QUALITY CONTROL LABORATORY Mam Dawn Assay of HCL Aqueous Alkalimetry Direct titration 0.1N NaOH Methyl Red TS HCL + NaOH NaCl + H2O Assay of Diluted H3PO4 Aqueous Alkalimetry Direct titration 0.1N NaOH Thymolphthalein TS H3PO4 + 2NaOH Na2HPO4 + 2H2O Assay of H3BO3 Aqueous Alkalimetry Direct titration 0.1N NaOH Phenolphthalein TS H3BO3 H+ + BO2- + H2O
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Discovering the Mystery of Eleven Test Tubes Karen Radakovich Ph.D. Mohammad Farhad Brittany Cina CH 223‚ Spring 08 Abstract: Eleven mystery test tubes labeled from K-1 to K-11 contained: 6M H2SO4‚ 6M NH3‚ 6M HCl‚ 6M NaOH‚ 1M NaCl‚ 1M Fe(NO3)3‚ 1M NiSO4‚ 1M AgNO3‚ 1M KSCN‚ 1M Ba(NO3)2‚ 1M Cu(NO3)2 respectively. The contents of the test tubes were determined by chemical experiments. Solution K-1 contained NiSO4 because when solution K-9‚ ammonia which was identified by its pungent odor
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Guide Questions Experiment 1 Calibration of the calorimeter: 1. Give the net ionic thermochemical equation of the reaction used to calibrate the calorimeter. a. Is the reaction endothermic or exothermic? b. Which is the limiting reactant? c. How much (in moles) limiting reactant was used? d. How much heat was generated (or absorbed) by the reaction? 2. Relate the sign of the ΔT to the ΔH of the reaction used for calibration. 3. What is the heat capacity of the calorimeter? Relate
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recorded and compared to controlled results from previous studies. Results of the preliminary and confirmatory tests have shown that the solution contained calcium (Ca2+)‚ ammonium (NH4+) and thiocyanate (SCN-) in all replications. Keywords: unknown analysis‚ cations‚ anions‚ calcium‚ ammonium‚ thiocyanate‚ preliminary tests‚ confirmatory tests Introduction Analytical chemistry has two divisions‚ namely: qualitative analysis and quantitative analysis. Qualitative analysis concerns the identity
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adjust to 50 μL of double-distilled water. 35. Lysis Buffer: to prepare 50 mL of buffer dissolve 23.6 g of Guanidine thiocyanate (118.16 g/L) in 25 mL of double-distilled water. Once dissolved add: 2.5 mL of 1 M Tris-HCl pH 7.0 (121.14 g/L)‚ 2 mL of 0.5 M EDTA pH 8.0 (186.12 g/L) and 0.05 mL of Triton X-100. Add double-distilled water to 50mL (final concentrations: 4 M guanidine thiocyanate‚ 50 mM Tris-Hcl pH 7.0‚ 20 mM EDTA and 0.1 % Triton X-100). 36. DNA Binding Solution: First‚ wash diatomaceous earth
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EXPERIMENT # 14: Exothermic and endothermic reactions Date: 25/06/2012 Name: Meagen Reyes Year 11 PARTS A‚ B and C * For the procedures and equipment needed in these experiments‚ refer to page 73-74 in the STAWA Exploring chemistry stage 2 book Part A: solution process (dissociation) Solutions and their chemical equations | Initial temperature (in Celsius) | Final temperature (in Celsius) | Classification(exothermic or endothermic) | Sodium hydroxide NaOH(s) Na+(aq) + OH-(aq) + Energy
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form a co-ordination complex”( Miessler‚ Gary L‚ 1999). This usually involves donation of one or more of the ligands electron pairs. Ligands that can bind via two or more atoms to form linkage isomers like thiocyanate (NCS-). Some ligands are better than others by having faster rates of equilibrium and exchange ligands very quickly. Examples of linkage isomerism are cobalt (III) complexes pentaamminenitro-kN-cobalt (III) and pentaamminenitro-kO-cobalt (III) which will be chemically prepared and investigated
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make it easily identifiable among other substances. The chemical property of cocaine is that it is reactive to cobalt thiocyanate and as a result it produces a blue-colored product (Girard‚ 2007). There are some other substances that also produce the same colored residue with reaction to the chemicals used for substance identification. For example; in reaction to cobalt thiocyanate‚ a blue-colored product similar to that of cocaine is produced by lidocaine‚ benzocaine‚ and procaine. Therefore‚ the
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Ammonium sulphate (NH4)2SO4. FW = 132.14‚ Eq. = 66g/l. 250ml 0.05M = 1.325g = 0.1N | Adipic acid HO2C(CH2)4CO2H‚ FW = 146.4‚ Eq. = 73.03g/l 250ml 0.05M = 1.83g = 0.1N | Barium hydroxide Ba(OH)2.8H2O‚ FW = 315.48‚ Eq. = 157.5g/l 250ml 0.05M = 3.94g = 0.1N | Benzoic acid C6H5COOH‚ FW = 122.12‚ Eq. = 61g/l 250ml 0.05M = 1.52g = 0.1N | Calcium carbonate CaCO3‚ FW = 100.00‚ Eq. = 50g/l 250ml 0.05M = 1.25g = 0.1N | Furroic acid FW = 112.08‚ Eq. = 112g/l 250ml 0.1M = 2.8g = 0.1N |
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N12/4/CHEMI/SPM/ENG/TZ0/XX 88126104 CHEMISTRY standard level Paper 1 Friday 9 November 2012 (afternoon) 45 minutes INSTRUCTIONS TO CANDIDATES • Do not open this examination paper until instructed to do so. • Answer all the questions. • For each question‚ choose the answer you consider to be the best and indicate your choice on the answer sheet provided. • The periodic table is provided for reference on page 2 of this examination paper. • The maximum mark for this examination
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