the wrong spot was chosen. If the RF values were used to determined which spot to choose‚ results may yield a smaller presence of pure naphthyl ether and a larger presence of dichloromethane in the IR spectrum. The spot that is most visible on the TLC plate is the solution that needs to be chosen. For this lab‚ the forth sample was chosen because the spot showed up the most under the UV light. An IR spectrum was obtained for this sample‚ and peaks for dichloromethane and 2-naphthol were signaled
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study conducted by Mallek-Ayadi‚ Bahloul‚ and Kechaou‚ (2017)‚ phytochemical composition of Cucumis melo L. peels was analyzed. High performance liquid chromatography was performed for standardization. Peels consisted of carbohydrates‚ ash‚ phenols‚ flavonoids and dietary fibers. Main phenolic classes were flavones and hydroxybenzoic acid where 3-hydroxybenzoic acid was the major phenolic compound followed by apigenin-7-glycoside. Another study on preliminary phytochemical screening of methanolic seeds
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Purpose: The purpose of this experiment was to identify one ketone with Thin Layer Chromatography and one using NMR spectrometry. We will do this by making 2‚ 4 a DNPH derivative and checking the melting points. Theory: By Using specific methods of compounds detection‚ we can match an unknown compound with a known compound because similar compounds will display similar characteristics. In this experiment‚ identifications of the unknown ketone was accomplished using thin layer chromatography
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information (Petersen‚ 2007). The talking and listening process is complicated. Petersen explains each communication process of listening and talking individually to better understand. In this section he introduces the Talker-Listener Card (TLC). The TLC allows the person talking or listening to have their time to so do without interruption in order to facilitate a open dialogue (Petersen‚ 2007). The talker is either most
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they are also significantly lower in nitrates and pesticide residues. In addition‚ with the exception of wheat‚ oats‚ and wine‚ organic foods typically provide greater levels of a number of important antioxidant phytochemicals (anthocyanins‚ flavonoids‚ and carotenoids). Although in vitro studies of organic fruits and vegetables consistently demonstrate that organic foods have greater antioxidant activity‚ are more potent suppressors of the mutagenic action of toxic compounds‚ and inhibit the
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dietary fiber‚ which cuts down cholesterol and fats from the body and to help in smooth defecations and in addition offer alleviation from obstruction illnesses. Natural products make out of numerous against oxidants‚ for example‚ poly-phenolic flavonoids‚ vitamin-C‚ and anthocyanins. These mixes‚ firstly‚ help human body shielded from oxidant anxiety‚ ailments‚ and malignancies‚ and furthermore; help the body create ability to battle against these infirmities by boosting our invulnerability level
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CHEM 2018 Organic Lab Part 2 Experiment 7: Diethyl n- Butylmalonate Lab Partner: Reference: Williamson K.L.‚ & Masters
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SYNOPSIS: *INTRODUCTION *FOOD SOURCES *ORAC IN FOODS *VITAMINS *CAROTENOID TERPENOIDS *FLAVONOIDS *PHENOLIC ACIDS AND THEIR ESTER *OTHER NONFLAVONOID PHENOLICS *POTENTIAL ORGANIC ANTIOXIDANT *ANTIOXIDANT IN FRUITS *CONCLUSION ANTI-OXIDANT INTRODUCTION: *An antioxidant is a molecule that inhibits the oxidation of other molecules. * Oxidation is a chemical reaction that transfers electrons or hydrogen from a substance to an oxidizing agent. Oxidation reactions can produce
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from a group of others with acquired data. Experiment Summary: In this experiment‚ we use TLC to identify components of an unknown analgesic drug. We prepare a solution of the drug by dissolving part of a tablet in 1:1 ethanol/dichloromethane‚ then spotting a TLC plate with the solution along with standard solutions of all active substances the drug tablet is likely to contain. Once the TLC plate develops and dries‚ it is viewed under ultraviolet light to properly visualize and mark the
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and the crystals formed where powdery in texture. On the other hand‚ the pure recrystallized product gave a shiny white colour appearance‚ with its crystals being needle like in texture. TLC results: Legend: i= acetaminophen standard ii= phenacetin standard iii = Recrystallized product Figure 1: TLC
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