expected melting point. After its temperature reached the plateau‚ the temperature increment was set at 1°C per minute‚ and the melting point range of 152°C-154°C was recorded. After standardizing the melting device‚ a small sample of unknown carboxylic acid was placed in a capillary tube‚ and an arbitrary plateau of 200°C was set. When the sample started to melt at 150°C‚ another capillary tube containing a small amount of unknown sample was placed in the melting device‚ and the plateau was set to 135°C
Premium PH Titration Laboratory glassware
Affects of Hydrogen Peroxide Equivalents on Green Synthesis of Adipic Acid. Andrew R. Glessman*‚ Chase W. Turner‚ Audra Cokain‚ Jacob Kindred‚ Darryl Watkins Department of Chemistry and Chemical Biology‚ IUPU‚ 402 N. Blackford St‚ Indianapolis‚ IN 46202 aglessma@umail.iu.edu April 25‚ 2014 Figure _______________________________________________________________Abstract- The synthesis of adipic acid has been a growing topic of discussion due to the harmful impact it has on the environment
Premium Hydrogen peroxide Hydrogen Oxygen
Extraction of R’-NH2 For both of the organic acid and organic base extraction‚ the addition of the respective inorganic acid or inorganic base (HCl or NaOH) to the three-component mixture caused an immiscible appearance of the solution in the separatory funnel. By briskly shaking the separatory funnel with the mixed components created a build up of pressure which was released through the stopcock forming small disappearing bubbles within the tip of the separatory funnel. Once the funnel was placed
Free Acid Chemistry Laboratory glassware
How Acetylsalicylic Acid was Discovered Acetylsalicylic Acid in its earliest form was a powder for the bark and leaves of the willow tree. Hippocrates‚ who lived sometime between 460 B.C. and 377 B.C‚ founded it. This “Miracle Drug” that was able to relieve pains was later looked into with further detail by Johann Buchner. He isolated a tiny amount of bitter tasting yellow‚ need- like crystals‚ and called salicin. By 1829 French Chemist Henri Leroux had improved the extraction procedure to
Premium Salicylic acid Aspirin
April Goodson CHEM 242L-002 February 20‚ 2013 Oxidation of Cyclohexanone to Adipic Acid Abstract The cyclic ketone cyclohexanone was oxidized to adipic acid using the oxidizing agent nitric acid. The experiment yielded 0.2667 grams of adipic acid‚ giving a percent yield of 113.97%. Although the product was allowed to dry for one week‚ residual moisture was still present in the sample and a melting point could not be obtained. This error in the experiment either resulted from adding too much
Premium Oxygen Oxidizing agent Chemistry
Jarrett Sears Dr. Hummel Chem 121 2/7/13 A Chemical Reaction between Tin and Nitric Acid Introduction: Finding the products made from the components of tin metal and nitric acid is the ultimate objective of this lab; the formula of the products will be found in the CRC handbook thereafter. Procedure: First‚ obtain a clean crucible‚ and heat it under a Bunsen burner until it is as hot as possible‚ about 15 minutes within a fume hood unit. The Bunsen burner will be used under the fume
Premium Oxygen
9.1 Manufacture of Sulphuric Acid 1. State uses of sulphuric acid in daily life. - lead acid batteries in automobiles and for home use - extraction of elements from ores - manufacturing of fertilizers 2.The following shows an incomplete flow chart of the Contact process. a) b)Chemical equation A. B. C. D. 3. Briefly explain the sources of sulphuric dioxide gas in atmosphere. -Sulphur dioxide is produced mainly from the combustion of fossil fuels
Premium Glass Sulfuric acid Ammonia
Punished by Acid Several people from the third world become a victim of an acid attack. The victim’s life has changed tremendously‚ which is what the photographer shows with his world-known pictures. On Ebrahim Noroozi’s photoseries you see a mom named Somayeh and her daughter‚ Rana and what acid has done to their faces. Now they most stay by themselves and take care of themselves. It is hard for me to understand some people will walk up to you to pour acid on you. Somayeh looked like an average
Premium Victim Maslow's hierarchy of needs Attack
Properties of Acids and Bases Diagram: A B C D E F Bromothymol Blue Universal Indicator Phenolphthalein Litmus Paper Analyze: 1) F‚ C‚ D‚ B‚ A‚ E 2) D is neutral because it turned to the colour of green when it came in contact with the indicator Bromothymol Blue. The acid or base is green between 6.0-7.6 pH. 3) Solution E is more alkaline (more basic) than solution A because when E came into contact with the indicator Bromothymol Blue it turned
Premium PH indicator Atlantic Ocean PH
The purpose of this experiment was to study the effect acid rain has on seed germination and after performing this experiment is can be concluded that acid rain has a negative effect on seed germination. When seeds are soaked in an acidic solution the process of germination slows. Acidic solutions‚ while do slow growth of a seed‚ they do not kill the seed. A seed can be dormant for a majority of its lifespan‚ seeds watered with acid solutions stayed in a dormant condition. For example‚ trial three
Premium