The 13C NMR spectrum was useful to help finding the structure of the unknown. It showed six different signals in the spectrum. Signal 1 had an observed peak value of 19.242 ppm‚ and its peak calculated value was 19.1 ppm. This signal was first to most upfield and shielded in the spectrum because of the high electron density of carbon. This signal was agreed to a literature value for a CH3 group between 5-30 ppm. Signal 2 was branched to signal 1‚ and had the same value‚ but it was agreed for the
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Case Study Report for Unknown #49 A new school for girls was opened in a larger village in Northern Pakistan‚ and the teachers were proud to have convinced many families in the surrounding villages to allow their daughters a basic education. The school was a success‚ and the 6-10 year olds girls quickly learned how to read and write and were even instructed in the sciences. However‚ 2 weeks before summer break‚ many of the girls and the teacher developed breathing problems that included severe coughing
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Sally Jessica Smithers: The Case Of The Unknown Assassin Sally Jessica Smithers was a slender‚ beautiful‚ smart‚ and talented cop. She was investigating eleven serial killings of important men when she got a call‚ there was another murder. When she went‚ she took no time at all at the scene. As Sally left the crime scene in the park‚ with one hand in her long dark brown hair‚ she called out to a few units to make three immediate traffic stops and went to the last one to read off people’s IDs. When
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MIC 206 Guidelines for Unknown Investigation Lab Report General Considerations: A. Papers must be typed‚ written in past tense‚ and in third person. (-50 if not typed) B. Paper Structure: Each section is to be headed with the appropriate heading. C. Format and Style 1. Format: a. Face Page: The face page should contain the title of the experiment‚ the author of the report‚ class section time‚ & date submitted. (1.5 points) b.
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1. Obtain 1 gram of an impure‚ unknown substance solid. Make sure to stir the mixture before measuring the sample; record the mixture’s code in the data section. 2. Add approx. 25-50 mL of water and several boiling chips to a 125 mL Erlenmeyer flask and heat the water to a gentle boil using a hotplate. 3. On a second hotplate‚ place a 125 mL Erlenmeyer flask containing the one gram of unknown solid along with a boiling chip. 4. Using a ring clamp‚ slowly pour approx. 5-10 mL of boiling water into
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Lab: Flame Test Purpose: to determine the ID of 2 unknown substances Background Information: Every atom consists of a nucleus with tiny electrons whizzing around it. The further away from the nucleus they are‚ the more energy the electrons have. If a metal atom is heated‚ the electrons get enough energy to jump higher away from the nucleus‚ they become “excited”. When they fall back closer to the nucleus (back to their ground state)‚ they give off this extra energy as light. Why is the
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The Unknown Struggles of Homeless Children Tammy R. Mathews Liberty University Abstract This research assessed the struggles of homeless children. The study compared the educational struggles of a random sampling of children living in stable environments to children who are considered “homeless.” Homeless refers to any child or youth who lack a fixed‚ regular‚ and adequate nighttime residence. The study revealed the number of homeless
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Spectrophotometric determination of Ascorbic acid Concentration in an Unknown Solution Introduction: The naturally occurring organic compound with antioxidant properties is Ascorbic acid shortly referred as (AA). Normally the color of Ascorbic acid is white‚ but in some cases of impure samples it appears yellow in color. Ascorbic acid is solid in state. In water it dissolves well to give mildly acidic solutions. Ascorbic acid is one form ("vitamer") of vitamin C [1]. So‚ Ascorbic Acid (AA)
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An Autobiography of an Unknown Indian by Nirad C. Chaudhuri. In this book the author has depicted his “Early Environment” in book -1 which he talks about his “ My birth place”‚ “ My Ancestral village” where he has pass his old days‚ “ My Mother place” where he had lived for sometimes and also describe about “England” as he was very fascinated of it. So as the same he talks about his “parents and early 12 days” and something about “Nationalism” in book -2.In book -3 he talks about “Calcutta” how
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Abstract Three tests were performed to determine the identity of unknown number 34‚ a gram stain‚ citrate utilization test‚ and a urease detection test. These tests are explained in detail‚ and the method of performing the tests is described. The tests showed that the bacterium was gram-negative bacilli that did not utilize citrate‚ and the ability to hydrolyze urea using urease. These results indicate that the identity of unknown number 34 is Proteus mirabilis. Introduction Proteus mirabilis is
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