Thin Layer Chromatography of Unknown Samples and Paprika By: Uyen Huynh Date: June 18‚ 2014 Lab Partners: Philip Murray Professor and section: M. Pandey‚ CHM2210L.601 Data: Analysis of Drug Store Items Knowns Rf Values Aspirin .91 cm Acetaminophen .85 cm Ascorbic Acid .86 cm Unknown .97 cm Identity of unknown mixture Acetaminophen Analysis of Paprika Pigments Spot Number Rf Color 1 1 Red-orange 2 1 Red-orange Calculations
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Ever since I was a little girl I dreamed about traveling overseas. Strange lands‚ exciting places‚ and new cultures have always fascinated me. I’ve always wondered what it would be like to speak another language‚ to grow up learning different customs‚ or to live in a completely different way than I do now. This past summer my dream finally came true. I got to travel to England‚ France‚ Switzerland‚ and Germany with Mme. Kelly and five other girls‚ and suddenly the world was at my fingertips. <br> <br>England’s
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Experiment 5- Standardization of NaOH and determination of Molarity of an unknown Acid Objectives 1. Preparation and standardization of a 0.1M NaOH solution 2. To learn the technique of titration 3. Determination of the concentration of an unknown diprotic acid. Introduction Titration can be traced to the origins of volumetric analysis‚ which began in the late eighteenth century. Study of analytical chemistry began in France and the first burette was made by Francois Antoine Henri
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Carlie Haeffner Qualitative Analysis March 20‚ 2015 The purpose of this lab is to identify unknown ions in a solution by using a type of chemical reaction called precipitate reactions. The key to finding which ions are present in a solution is to form a precipitate which makes the ions “come out” in a reaction (McNeil‚ 2013-2014). Water is used in these experiments to act as a solvent. Since water is a polar molecule‚ the slightly positive and negative charges will sometimes pull apart molecules
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Determining the Unknown Concentration of NaHCO3 (aq) Through Titration Introduction Titration is the accurate addition of a titrant- solution in a burette- into a measured volume of a sample (Kessel‚ 2003). There are many different types of titration‚ such as acid-base reaction‚ redox reactions‚ precipitation reaction and more (Dohrman). In this lab an acid base titration will be explored. In an acid-base titration‚ the concentration of an acid or base is unknown and is determined by the adding
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The 13C NMR spectrum was useful to help finding the structure of the unknown. It showed six different signals in the spectrum. Signal 1 had an observed peak value of 19.242 ppm‚ and its peak calculated value was 19.1 ppm. This signal was first to most upfield and shielded in the spectrum because of the high electron density of carbon. This signal was agreed to a literature value for a CH3 group between 5-30 ppm. Signal 2 was branched to signal 1‚ and had the same value‚ but it was agreed for the
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Sally Jessica Smithers: The Case Of The Unknown Assassin Sally Jessica Smithers was a slender‚ beautiful‚ smart‚ and talented cop. She was investigating eleven serial killings of important men when she got a call‚ there was another murder. When she went‚ she took no time at all at the scene. As Sally left the crime scene in the park‚ with one hand in her long dark brown hair‚ she called out to a few units to make three immediate traffic stops and went to the last one to read off people’s IDs. When
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Scheme of Analysis for Lab 2 Unknown Sample Description Phase‚ color‚ odor‚ crystalline or gel-like? If crystalline‚ what is crystal shape – needle-like or powdery? Does it look like a pure substance or a mixture? How many components appear to be present? Tests on original sample Flame Test Bushy yellow‚ orange flame – Na+ is present and possibly K+ and NH4+. Pink-purple flame – K+ is present and Na+ is not. (Possibly NH4+) No color or faint trace Na+ - NH4+ is possible‚ K+ and Na+ are
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Experiment #9 – Identification of Aldehydes and Ketones Introduction Aldehydes and ketones share the carbonyl functional group which features carbon doubly bonded to oxygen. In the case of ketones there are two carbon atoms bonded to the carbonyl carbon and no hydrogens. In the case of aldehydes there is at least one hydrogen bonded to the carbonyl carbon; the other attachment may be to a carbon or a hydrogen. In all cases the carbon(s) that are attached to the carbonyl group may be aliphatic (not
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Identification of A Mixed Culture Unknown An experiment such as this one serves the purpose of allowing us‚ the students‚ to apply what we already know about any organism and any laboratory procedure to the difficult task at hand. It is possible to identify a mixed culture by running familiar experiments on the unknown bacteria and taking information already known about specific bacteria and applying it to the results. This helps to slowly eliminate any bacteria that do not correspond with the
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