Synthesis of Methyl Stearate The purpose of this lab was the convert liquid methyl oleate to solid methyl stearate by catalytic hydrogenation. Firstly‚ we produced hydrogen gas using solid mossy zinc and sulfuric acid. Using the hydrogen produced in the previous reaction‚ we were able to convert the liquid methyl oleate to solid crystals of methyl stearate. A mineral oil was also used to bubbler was used to maintain the hydrogen pressure slightly above the atmospheric pressure and to prevent back-diffusion
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2. Experimental 2.1. Experimental procedure for the synthesis of bone-like CS-PEG-HA-ZrO2 nanocomposites (BNC I-III). At first‚ ZrO2 nanoparticles (NPs) were synthesized by using the previously reported method [16]. Briefly‚ aqueous solution of sodium hydroxide (purchased from HiMedia Private Ltd.) (40 ml 0.05M) was slowly added in zirconium oxychloride octahydrate (purchased from Merck India Ltd.) solution (100 ml 0.01M) prepared in methanol-water (1:1) at 5 oC temperature. The mixture was stirred
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Lab #5: Refraction of Light Theory: Refraction can be defined as the bending of a wave when it enters a medium which causes it to have some reduced speed. In terms of light‚ refraction occurs when the ray passes through some medium which slows its speed; such as water or glass. In this instance the ray tends to bend towards the normal of the medium. The amount of bending or refraction which occurs can be calculated using Snell’s Law (). Objective: To measure the index of refraction of Lucite
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CHEM 3125 Experiment 4: Multistep synthesis of tetraphenylcyclopentadienone Overall Synthesis: CHEMICALS: wk 1: thiamine hydrochloride (1 g/student)‚ 95% ethanol (8 mls/ student)‚ 2M NaOH (5 mls/student)‚ benzaldehyde (4 mls/student) wk 2: 95% ethanol (30 mls/student) wk 3: acetic acid (6 mls/student)‚ ammonium nitrate (1 g/student)‚ 0.1g/ml cupric acetate (1.5 mls/student)‚ dichloromethane (6 mls/ student)‚ 30% acetone in heptanes (3 mls/student)‚ 95% ethanol (20 mls/student) wk 4:
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During the recess of the Chung case‚ Judge Moore motioned to move forward with the next case. The defendant Jeffrey Gaddy was presented to the court was along with Mr. Francisco. Once Mr. Francisco was sworn into court‚ defense attorney Clayton asked him to recall the incident. Mr. Francisco stated that the defendant Jeffery Gaddy was accused of burglary and breaking into the backdoor and two offices within ACE Tree Service. The officer on duty responded to the initially burglary call and found Mr
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4/27/11 SYNTHESIS AND CHEMILUMINESCENCE OF LUMINOL Abstract: Chemiluminescence occurs in nature and can be found in everyday products. For example‚ the light omitted by fireflies‚ deep sea fish and glow sticks is a result of this process. Luminol was synthesized from from 3-nitrophthalic acid and then combined with potassium ferricyanide and hydrogen peroxide to omit a blue light. The product of this reaction is very unstable and is made by losing a nitrogen and the electrons go from an excited
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Isopentyl Acetate Synthesis Results: Crude % Yield Calculation Reaction: H2SO4 C2H4O2(aq) + C5H12O(aq) ----> C7H14O2(aq) + H2O(l) (1 mole of acetic acid reacts with 1 mole of isopentyl alcohol to make 1 mole of isopentyl acetate and 1 mold of water) Volume of isopentyl alcohol (d=0.809g/mL; MW=88.15g/mol): 2.5mL Moles of isopentyl alcohol: (2.5mL)(0.809g/1mL)(1mol/88.15g) = 0.02294mol Volume of glacial acetic acid (d=1.06g/mL; MW=60g/mol): 3.5mL Moles of glacial
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Objective To synthesis methyl orange by coupling diazotised sulphanilic acid with N‚N-dimethylaniline. Materials (Chemicals) Sulfanilic acid‚ 2.5% aqueous sodium carbonate solution‚ sodium nitrite‚ concentrated hydrochloric acid‚ N‚N-dimethylaniline‚ glacial acetic acid‚ 10% aqueous sodium hydroxide‚ saturated sodium chloride solution Apparatus 50 mL Erlemeyer flask‚ 250 mL beaker‚ test tube‚ hot plate‚ Buchner funnels Procedure In a 50 mL Elermenyer flask 1.2 g of sulfanilic acid and
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Experiment #1: Synthesis of Salicylic Acid From Wintergreen Oil By: Asad Razzaq TA: Date: 18/01/2015 222/Lab Section 8 Introduction Salicylic acid‚ used in production of substances used worldwide such as commonly used analgesic drug aspirin(cite)‚ can be obtained from natural resources such as wintergreen oil or can be synthesized. Through a series of chemical reactions with cheap raw materials beginning with beginning with methyl salicylate and‚ it is a cheaper and more
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Abdulfatah Momen R/W class One of the basic components of the community is children. Some of families think that having children bring problems to their life. Some of these families decide to work off children by medical science before children come to the life. The way that they choosing is abortion. Abortion was made by women who are pregnant‚ and they don’t want to have children. Abortion is the termination of a pregnancy by the removal of the fetus. Rates of abortion increase to be very
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