Prelab 5B Macrocyclic Synthesis OBJECTIVE: The objective this week is to produce Tetraphenylporphyrin and its metal complex. This will be carried out by condensation of 4 equivalents of Benzaldehyde and pyyrole in the presence of propanoic acid. The product will undergo UV/Visible Spectrum tests to determine its lambda max. The lambda max will show us the relationship between a conjugated system and the visible spectrum. PROCEDURE: Step 1: preparation of meso-tetraphenylporphyrin (TPP)
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Determination of Trace Amount of Copper and Zinc in an Aqueous Solution by Atomic Absorbance Spectroscopy Abstract: The purpose of this experiment is to analyze a sample containing copper and zinc in trace amounts‚ where standard addition method was used and the instrument used is the atomic absorbance spectroscopy. The amount of copper obtained was 0.569 ppm ± 0.015 and for zinc we obtained 0.42 ppm ± 0.0027. Introduction: This method implies the excitation of particles in the solution sample
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Microwave Synthesis of 5‚10‚15‚20- Tetraphenylporphyrin Abstract: In this green chemistry experiment of 5‚10‚15‚20-tetraphenylporphyrin was synthesized from benzaldehyde and pyrrole. using microwave irradiation to heat the reactants.‚ The liquid reactants are absorbed on a solid support‚ silica gel‚ which acts as a Lewis acid catalyst to facilitate the reaction. The reaction forms a porphyrinogen‚ which is then oxidized to the porphyrin product by atmospheric oxygen. Column chromatography is performed
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Synthesis With all the foreigners crossing the borders of the United States‚ America is considered to be a nation of immigrants. The United States has all kinds of immigrants who decide to relocate to America in order to pursue better opportunities for themselves than what they could find in their own country. Once the immigrants make it passed American borders‚ they begin living the "American way"‚ and doing what they think will help lead to a positive movement within the community. What the
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Synthesis Essay Reactions to death and tragedy range depending on the cause and effect of the situation. People react differently to every situation‚ but with tragedy and death‚ a common reactions can range from anger to depression to fear. All of these can be authentic responses‚ but the question is whether these reactions are appropriate. In circumstances of tragedy and death‚ emotional responses are appropriate when they are authentic and additionally evoke action. In times of death and tragedy
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Synthesis Paper Introduction Exercise can be very challenging to commit to. As a young adult my ideas and hopes were to always begin and maintain a routine that would help me to stay active and healthy. I regretfully report that I have not yet committed to this effort. In high school‚ I ran with the track team and was faithful the Reserve Officer Training Corps which helped me to stay in shape and remain fit with much effort. This was just a part of my life and I enjoyed it
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Two common theories about dreams are the Freudian theory that dreams are repressed desires and Hobson’s activation-synthesis theory that dreams are the result of random brain stem circuits actively overwhelming the cerebral cortex (Pinel‚ 2007). The two common sleep theories that attempt to address the purpose of sleep and sleep habits: recuperation and circadian. Recuperation
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Set 7 Ap English Set 7 Ap English Television in Presidential Elections Synthesis Essay The United States have adapted television into presidential elections since the 1960s. However the influence on America is not necessarily positive. The negative influence of television on the United States can be conveyed though the necessity of perfect image by candidates‚ sharing of too personal facts‚ and the brutality of the television debate. Television has negatively affected presidential debates
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Synthesis Essay The Puritans dream was to create a model society for the rest of the Christians. Their goal was to make a society in every way connected to god. But to really understand what the aspirations of the puritans were‚ we must first understand their beliefs. These beliefs were expressed through their writings which have been read through the years by American students. With this‚ American students were taught Puritan lessons of devotion‚ virtue‚ and conformity. Devotion can be defined
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Synthesis The Tell-Tale Heart‚ and The Cask of Amontillado “The Cask of Amontillado” and “The Tell-tale Heart”‚ has a setting in the mid 1800’s‚ where the narrator in each stories killed another character‚ hid their victims and leaving no evidence behind. But both of these stories don’t end the same‚ one of these stories‚ the murder gets away‚ and the other faces his consequences. In “The Cask of Amontillado”‚ Montresor tells the story of the day that he took his revenge on Fortunato‚ because
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