"Williamson ether synthesis lab" Essays and Research Papers

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    blue green dihydrate. Copper (II) Chloride is highly soluble in water and will produce a blue solution. solutioAluminum is the compound that has a chemical formula of Al. This is a silver solid that can be easily formed‚ machined‚ or cast. In this lab‚ we will be finding the limiting reactant between Copper(II) Chloride and Aluminum. The limiting reactant is‚ reactant is‚ the reactant in a chemical reactant that limit’s the amount of the product that can be formed. We will also need to find the molarity

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    High Performance Liquid Chromatography Analysis of Aspirin Problem: Was aspirin (acetylsalicylic acid) successfully synthesized? Are there impurities or by-products present in the synthesized aspirin? How pure is the synthesized aspirin? Introduction: In the last experiment‚ aspirin was synthesized followed by characterization of the product using several different techniques. Melting point was a test that provided information about the identity and purity of the aspirin product. The iron(III)chloride

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    The goals of this experiment are to determine if the products derived from amide synthesis and Williamson Ether Synthesis are identical‚ and if one of the synthetic routes is more advantageous than the other. In Part 1‚ an attempt to synthesize acteophenetidin crystals by amide synthesis was made. We began by removing the colored impurities from the p-Phenetidine (reddish-brown) by placing 2g of the sample in 38 mL of hydrochloric acid and heating the solution to boiling point. Upon reaching just

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    Examples of synthesis reactions: 1. Metal  +  oxygen  →   metal oxide EX. 2Mg(s)  +  O2(g)  →    2MgO(s) 2. Nonmetal  +  oxygen  →    nonmetallic oxide EX. C(s)  +  O2(g)  →    CO2(g) 3. Metal oxide  +  water  →    metallic hydroxide EX. MgO(s)  +   H2O(l)  →    Mg(OH)2(s) 4. Nonmetallic oxide  +  water  →    acid EX. CO2(g)  +  H2O(l)  →    ; H2CO3(aq) 5. Metal + nonmetal  →    salt EX. 2 Na(s)  +  Cl2(g)  →    2NaCl(s) 6. A few nonmetals combine with each other. EX. 2P(s)  +  3Cl2(g)  →

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    “The Synthesis of Zinc Chloride”‚ what a peculiar name for a lab that does not even involve synthesis. Synthesis‚ by definition‚ is when two elements are combined in a chemical reaction‚but that is not the case. In this lab we are combining zinc‚ an element‚ and hydrochloric acid‚ a compound‚ but combining a compound and an element is not synthesis‚ it is single replacement. We are taking zinc and hydrochloric acid and making zinc chloride and hydrogen‚ a single replacement‚ but what occurred during

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    Alum Synthesis Lab Report

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    system to isolate the alum. 2 Al(s) + 2 KOH + 22 H2O + 4 H2SO4 → 2 KAl(SO4)2●12H2O(s) + 3 H2(g) Its composition was analyzed using two precipitation tests and two flame tests. Three methods for growing crystals were then set up for observation next lab. Theoretical yield and percent yield: The theoretical yield for alum was 4.55g and the percent yield was 139%. The percent yield was above 100% because the alum was saturated with ethanol and water. KOH test: The KOH test identified the presence of

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    Pa Synthesis Lab Report

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    Materials & Methods Synthesis Procedure of PDA@MT Polydopamine is synthesized through covalent polymerization similar to melanin biosynthesis‚ with DA oxidized to dopamine quinone‚ then further oxidized to DHI‚ which undergoes deprotonation and cross-linking via Michael addition to form PDA. A solution was prepared to synthesize PDA by mixing 90 mL of water‚ 40 mL of ethanol‚ and 3 mL of ammonia solution in a 300 mL beaker. After stirring for 30 minutes at 37°C‚ a solution of 500 mg of DA dissolved

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    CHEM 1474-E01 Chemistry for Everyday WEEK5 Lab Report Spring 2017 Instructor: Kyoung Nan Kim Office: SI3076 Email: kyoung.kim@ucdenver.edu Office hour: M/W 1:00p-2:30p (SI3076) T/Th 12:30p-1:30p (SI3076) • All communication should be done via school email (xxxx@ucdenver.edu) • The work will be submitted through canvas assignments. You can simply upload doc/pdf files under “Lab report” assignment tap. • Review: Ch2‚ Ch3.5‚ Ch 4.2‚ Ch6.1 and Ch7.1-Ch 7.3 in your text book (21st

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    Photolytic Degradation of Flupentixol-Melitracen Chapter One Introduction 1 Photolytic Degradation of Flupentixol-Melitracen 2 1. ANTIPSYCHOTIC 1.1 Antipsychotic An antipsychotic also known as neuroleptic is a tranquilizing psychiatric medication which is used to treat psychosis‚ schizophrenia and bipolar disorder. Now it is increasingly being used to treat the non-psychotic disorders. Psychosis disorder included delusions or hallucinations. Delusion is the pathological condition

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    Abstract – The synthesis of 4-hydroxy-4‚4-diphenylbutn-2-one was a three week multi-step project. The steps involved protecting the ketone of ethyl acetoacetate with a ketal group‚ followed by preparation and reaction with Grignard‚ then purification by extraction and recrystallization. The yield was 78.5%‚ but there are impurities present suggested by 1H-NMR‚ IR‚ and TLC. However‚ the results do indicate the desired hydroxyketone was formed. Introduction: The purpose of this multi-step lab was to synthesize

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