Yield Data The reaction of 0.139 grams of trans-cinnamic acid‚ 0.8 mL of glacial acetic acid‚ and 1.0 mL of 1.0 M of Bromine in acetic acid was recrystallized to form a solid‚ clear‚ crystal- like product. The melting was taken from the recrystallized product to determine what had been obtained. The melting point was found to be 130.5°C-133.7°C. Concluding that the product formed from the addition of bromine was a mixture of the erythro-2‚ 3-dibromo-3-phenylpropanoic acid‚ which has a known melting
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acidification of salicylic acid and acetic anhydride. The objective was to convert a specific amount of salicylic acid into the same amount of aspirin that was high in purity. Furthermore‚ the other objectives were to enable students to conduct the synthesis of aspirin‚ reinforce skills or recrystallisation and the technique of melting point determination. The amount of each compound should be the same because there is a 1:1 ratio between them. The purity of the synthesized aspirin was measured by determining
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CHAPTER 6 QUESTIONS : 8‚13‚14‚15 QUESTION 8 Akira Numata –UIA Japan Assumptions | Value $ | Yen equivalent | Arbitrage funds | 5‚000‚000 | 593‚000‚000 | Spot Rate (¥/$) | 118.60 | | 180-days forward Rate | 117.80 | | Expected spot Rate | 118.00 | | 180-days U.S dollar interest rate | 4.80% | | 180-days Japanese Yen Interest Rate | 3.400% | | Calculations Calculating forward Rate (i= interest rate) F180 sf/$ = S sf/$*1+ (isF*180/360)/ (i$*180/360)
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Name Period Date The Synthesis of Aspirin Background Pharmaceutical research labs perform chemical reactions between organic molecules that contain mostly carbon. Since the atoms in organic molecules tend to be nonmetals‚ then the bonds that hold them together are covalent bonds. Only a few elements on the periodic table are nonmetals: C‚ N‚ O‚ S‚ Cl‚ and F. This small number of elements can be bonded together in different quantities‚ bonding types (single‚ double‚ triple bonds)‚ and structural
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In modern day‚ man does not truly think about how much the earth means to life. On the contrary‚ humans aspire to cease Mother Nature’s beauty with the replacement of modern day cities made up of synthetic nature. Since the dawn of the twentieth century‚ a major theme in the American Arts has been the protest against man’s destruction of the natural world. With this in mind‚ as very well argued in Chief Seattle’s article “Respect”‚ humans fail to be conscious of the physical and sentimental value
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Lab Report Synthesis and Characterization of Aspirin (Acetylsalicylic Acid) The Synthesis and Characterization of Aspirin (Acetylsalicylic Acid). Summary: In this experiment‚ we produced 4.21 g of acetylsalicylic acid. Our theoretical yield was calculated to be 5.22 g. Therefore our % yield was determined to be 80.6%. The experimental boiling point range of acetylsalicylic acid was found to be 130-132° C. The true melting point of acetylsalicylic acid is 135° C‚ therefore our percent
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Revealing Trans Fats Informative Abstract Trans fats are fats resulting from the process a product undergoes in adding hydrogen to vegetable oil by turning liquid oils into solid fats and based on evidence supported‚ if consumed it would increase the risk of coronary heart disease and promote bad cholesterol at an high rate especially among Americans; it is therefore one of the leading causes of death in the United States. As a precautionary measure to counter this mass effect of trans fat the
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Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
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SYNTHESIS AND CHARACTERIZATION OF POLYANILINE/POLY (P-HYDROXYANILINE)/Fe3O4 MAGNETIC NANOCOMPOSITE M. R. SABOKTAKIN‚ A. M. MAHARRAMOV‚ M. A. RAMAZANOV Baku State University‚ Baku‚ Azarbaijan E-mail: mamed_r50@mail.ru Several composites have been studied for static dissipationand microwave absorbing materials based on polyaniline with metallic oxides. These composites which are conducting polymers have been widely used because of their lower density as well their good environmental stability as in
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Lab Report Macrocyclic Synthesis (Heme Analog) I. Purpose of Experiment and Introduction The purpose of this lab experiment is to prepare meso-tetraphenylporphin (TPP) and its copper‚ cobalt or zinc complex by condensing benzaldehyde with pyrrole in boiling propanoic acid. II. Introduction and Background There are two types of proteins that function as oxygen carriers: myoglobin (stores the oxygen) and hemoglobin (present in red blood cells and is responsible for oxygen transport)
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