restrained as appropriate at one end and under an axial tensile load of 500 KN applied to the other end face. It has been initially designed with a thickness of 50 mm. This gives a hand calculated stress value of 25 MN/m2‚ which is 1/8 of the material’s Yield Stress‚ of 200 MN/m2‚ giving a factor of safety of eight‚ which is deemed to too conservative. The flat bar now requires stepped down in size from W to h‚ forming a shoulder with fillet‚ at the middle of the bar along its length. For a given radius
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Chem 201 Lab October 21‚ 2011 Lab #6: Preparation of 2-chloro-2-methylbutane – an Sn 1 Reaction Purpose The purpose of this experiment was to prepare an alkyl halide‚ 2-chloro-2-methylbutane by reacting 2-methyl -2-butanol (t-amyl alcohol) with hydrochloric acid. Alkyl halides are of wide interest because they are widespread and have diverse beneficial and detrimental impacts .The overall reaction is given below: Procedure 1 ml of 2-methyl-2-butanol was measured using 1 ml syringe and
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reactions will occur to yield alum. Calculations: Aluminum foil: 0.5035 grams Alum & Watch Glass: 21.7691 grams Watch Glass: 15.1560 grams Alum: 6.6131 gram Theoretical Yield of Alum: 2Al(s) + 2KOH(aq) + 4H2SO4 + 22H20 -> 3H2(g) + 2KAl(SO4)2 + 12H2O(s) 0.5035gAl x 1molAl/ 26.98gAl = 0.0186 mol Al 0.0168molAl x 2molAl / 2mol KAl(SO4)2 = 0.0186mol KAl(SO4)2 0.0186mol KAl(SO4)2 x 258.2g/ mol KAl(SO4)2 = 4.8 gKAl(SO4)2 Theoretical yield = 4.8g KAl(SO4)2 Percent Yield Alum: 6.6131gKAl(SO4)2
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(oxalate)ferrate(III) trihydrate in a two step process‚ to learn new laboratory techniques such as decantation‚ recrystallization‚ gravity and suction filtration. Also the purpose of the experiment is to determine the actual‚ theoretical‚ and percent yields of product‚ and characterize the final compound by determining the number of waters of hydration by gravimetric analysis List of Observations: After adding (15 mL distilled water/5 drops of 3 M H2SO4) to ferrous ammonium sulfate hexahydrate
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Williamson Ether Synthesis specializing in producing ethers‚ it was ideal for this lab because of the alcohol and the alkyl halide used. After the synthesis and isolation of Gauifenesin was completed‚ the melting point ranges were observed and percentage yields were calculated to compare with the values of authentic guaifenesin and guaiacol. Reflux was used to synthesize Guaifenesin. Guaifenesin is an expectorant‚ meaning it helps loosen congestion in one’s chest and throat‚ making it easier to cough
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Name: David Kennedy Date: 11/5/14 Project No: 131 Title: Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate Abstract: The targeted trisubstituted ethylene compound Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate and its copolymer with styrene was prepared in this lab. The base catalyzed Knoevengael condensation of butyl cyanoacetate and corresponding aldehyde led to the forming Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate. The analyses that were used to prove its composition and structure
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Surface Area Formulas In general‚ the surface area is the sum of all the areas of all the shapes that cover the surface of the object. Cube | Rectangular Prism | Prism | Sphere | Cylinder | Units Note: "ab" means "a" multiplied by "b". "a2" means "a squared"‚ which is the same as "a" times "a". Be careful!! Units count. Use the same units for all measurements. Examples |Surface Area of a Cube = 6 a 2
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soluble in the solution. The yield is calculated to look at how well the reaction has been completed. This reaction is simplified to: C7H6O3 + C4H6O3 → C9H8O4 + C2H4O2 To work out the yield; 0.917g of 2-hydroxybenzoic acid (0.917/138) * 180 138 (the molar mass of 2-hydroxybenzoic acid) 180 (the molar mass of aspirin) Theoretical yield: 1.196g 3 d.p. Percentage yield is worked out by Actual yield of synthesised aspirin:
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Surface Waves: Understanding its movements I. Introduction We treat here an important wave phenomenon‚ the surface wave. It occurs in many physical systems both mechanical and electromagnetic. Mechanical surface waves can exist at the interface between two media with different densities such as the oceans and air. Ordinary sea waves and tsunamis are surface waves. Seismic events can produce both longitudinal and shear waves at the earth’s surface‚ resulting in earthquakes. Electromagnetic surface
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Microsoft’s Surface Pro laptop-in-disguise1 tablet is no different‚ a “flawed”2 device which has seen improvements to its design and structure over the past few years making it slowly approach perfection. Microsoft’s Surface Pro is one of the newer innovative devices that was initially introduced in February 20133 and has seen a much shorter succession cycle than that of any other popular tablet manufacturer‚ namely Apple. Adoption rate was not at its best with the initial introduction of the Surface Pro
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