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Aspirin Preparation

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Aspirin Preparation
Preparation and melting point of Aspirin
Aspirin is a painkilling drug and is produced worldwide to reduce and stop pain. Aspirin is made up of ehtanoylation of 2-hydroxbenzenecarboxylic acid in a presence of phosphoric acid.
AIM: The aim of the experiment is to prepare and produce aspirin as pure as possible. I will do this threw preparing the aspirin and purifying the product threw recrystallization. I will then obtain a melting point of my product to get an estimate of its purity. By the end of the experiment the target is to produce aspirin as pure as possible. Apparatus for synthesis of aspirin Materials for synthesis of aspirin * Pear shaped flask * 2.0 g of hydrobenzenecarboxylic acid * Fume cupboard * 4 cm3 of ethanoic anhydride * Flask with reflux condenser * 5 drops of phosphoric acid * Water bath * ice * 100 cm3 beaker * distilled water* Pipette * boiling water* Funnel * Filter paper* Spachelor * Kettle*Weighing boat*Boiling tube | Apparatus for melting point Materials for melting point*Capillary tube *Tesco aspirin*Melting apparatus * synthesised aspirin |
Apparatus for chromatography Materials for chromatography *Chromatography tank *Ethanol dichloromethane
*Capillary tubes * Tesco pure aspirin
*Weighing boat *
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