The final temperature was 76. The time duration for the bromination was 3:30 pm to 4:28 pm, which was 58 minutes. The flask was set out to cool. No changes occurred while it cooled. The next task was to precipitate the brominated hydrocinnamic acid from the solution. Even though BHCA has a polar carboxyl group, it has only a slight polarity due to its 9 carbon atoms. To precipitate it out, the solution was mixed added to 100 mL of ice water in a 250 mL flask. This flask was in an ice bath because low temperatures reduce solubility. The solution was added to a flask with a plastic pipette. The mixture was stirred at high speed. The mixture turned cloudy and white. The temperature was 3. The mixture was then poured through a Buchner funnel using vacuum filtration. The water and succinimide (the other product formed) collected in the flask below the funnel. This was the filtrate. BCHA stayed on top of the filter paper in the funnel. This was the precipitate. It was observed as a white powder. A beaker was pre-weighed at 14.40 g. The beaker was labeled and then the precipitate was added. The beaker was stored with no lid so the water will evaporate for the next lab…
In this experiment, the percent composition and empirical formula of silver oxide will be determined.…
9) Put 4mL of stock solution and 1mL of water in a test tube to make the second solution.…
2. To determine the densities of water, an unknown liquid, a rubber stopper, and an unknown rectangular solid.…
The purpose of this experiment was to be able to apply our knowledge of chemistry to identify 10 unknown elements that were presented to us. We were allowed to use Bunsen burners, hydrochloric acid, use PH paper to test if the unknown solution is an acid or a base, and precipitate each unknown solution with each other.…
Purpose: In this experiment I will determine the mass, density, volume, lengths and temperatures of different objects and liquids to help me better understand the importance of Chemistry and how Chemistry plays a big role in our everyday lives.…
.2400 grams of the unknown compound. This is done in duplicate and purple-tinted precipitates are placed in Gooch crucibles. The precipitates are suction dried using ethyl alcohol then acetone to…
5) For each of the reactions list the physical evidence that a chemical change was taking place (Please refer to the order in #3)…
The overall goal of experiment four was to determine the identity of unknown cations presented to the student. But in order to know the identity of these unknowns, in part 1, Ag+, Pb+, and Hg22+ were presented to the student in aqueous solutions and then precipitated through experimentation. In part 2, the same procedure was enacted to determine which substances precipitated through qualitative analysis. Solubility rules were also a major theme as solubility is important in determining whether a reaction will produce a precipitate.…
Conclusion: In this experiment we had to find the heat capacity of the calorimeter cup using two trials of hot and cold water. When we obtained the data after 10 minutes of recording 30 second intervals of the calorimeter cup temperature, we created a…
2). Did any of the liquids conduct an electric current? If so, which one(s), and please explain why or why not thoroughly?…
Three titrations were carried out: Acetic acid/NaOH, Tris/HCl and Gylcine/NaOH. 25ml of the weak acid or weak base was put into a beaker and its pH measured. Then it was titrated with the strong acid or strong base respectively while measuring the pH of the buffer (using a pH probe) on addition of every 1 ml of acid or base from the burette. Two point calibration was carried out prior to each titration using the three calibration solutions of pH 4, 7 and 9.2; for the Acetic acid/NaOH the calibration solutions used were: 4 and 7, for the Tris/HCl and for the Gylcine/NaOH the solutions used were 7 and 9.2. When carrying out the titration plot a rough graph in real time to immediately highlight any anomalies. For comparison carry out a similar experiment with strong acid and strong base where the acid is in the beaker and base is in the burette.…
An aqueous solution containing 0.050 M of ion and 0.072 M of is prepared, and the progress of the reaction followed by measuring []. The data obtained is given in the table below.…
There are three main sections to this module: terrestrial coordinates, celestial equatorial coordinates, and understanding how the ecliptic is related to seasons on the Earth. Each of these sections has its own simulator(s). The background material necessary to utilize these tools is contained in each section.…
Introduction: Gravimetric analysis is based on the measurement of mass. Gravimetric analysis involves isolation of an ion in solution by a precipitation reaction, filtering, washing the precipitate free of contaminants, conversion of the precipitate to a product of known composition, and finally weighing the precipitate and determining its mass by difference. From the mass and known composition of the precipitate, the amount of the original ion can be determined. Theodore W. Richards (1868-1928) and his graduate students at Harvard developed or defined many of the techniques of gravimetric analysis of silver and chlorine. These techniques were used to determine the atomic weights of 25 of the elements, decomposing known weights of the compounds, and determining the chloride content by gravimetric methods.…