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solution by taking a mole ratio of NaOH to KHP. 5. The main objective of Part 1 is to make sure all the students are paying attention to standard laboratory safety practices before they receive a vial of acid to work with. KHP is
In the experiment, standardization of NaOH with HC1 solution is carried out. Solid NaOH is hygroscopic where significant amounts of water vapor can be absorbed. Also, as NaOH is a strong base, significant amounts of atmospheric carbon dioxide can be absorbed too. It is also clear that NaOH cannot serve as a primary standard and thus it needs standardization by a primary or secondary standard. NaOH solutions can be directly titrated versus standardized HCl using phenolphthalein or methyl red indicator. In this case, methyl red is used as an indicator. The colours change from red to completely purple pink indicate the standardization is achieved. If reasonable concentrations of the acid and base are used, very sharp end points can be achieved. The…
10 ml of acid was used for all the three trials to keep a constant. During the first trial it took 3.700 ml of NaOH to titrate the HCl, in the second trial it took 3.750 ml, and in the third trial it took 3.750 ml. These differences in amounts of NaOH required to titrate the acid led to different molarities being calculated for the NaOH. The first being 0.270M and the other to being 0.267M. In order to calculate the total volume of base used, the readings from the burette from before and after titration were subtracted from each other. The average of the three molarities was found to be 0.268M for NaOH (Figure 2).…
In this experiment we experimented with titration. We saw the effects of titration on an acid and then on a base. The acid we used was hydro chloric acid and the base was ammonia. The acid turned pinkish red when properly titrated and the base turned clear. We used phenolphthalein as the titrate which turns red in acidic solutions and clear in basic solutions. The control aspects of this lab were the hydrochloric acid and ammonia. The independent variable was the titrate the phenolphthalein. We measured how many drops of the phenolphthalein it took to titrate the acid or the base.…
We will be using the LoggerPro and LabPro in order to help us determine our data. The purpose of this experiment is to follow the changes of pH during the titration of an acid and a base in order to determine the of the weak acid, . is a constant for a given acid at a given temperature. In this experiment we determined the Ka using two different methods: 1) the measurement of the pH of a solution containing a known concentration of a weak acid, and 2) measurement of the pH at the half-neutralization point in the titration of a weak acid and a strong base.…
The experiment began with the preparation and standardization of NaOH solution. It was calculated that 2.00 grams of NaOH pellets were needed to prepare 0.5 L of 0.1 M NaOH solution. The solution was then standardized by conducting three titration trials. It was calculated that 0.7148 grams of KHP were necessary to neutralize 35 mL of the 0.1 M NaOH. Three samples of KHP were weighed approximating this number (Table 1). Each sample was mixed with 40 mL of deionized water and 2 drops of phenolphthalein in 3 Erlenmeyer flasks. Each flask was then titrated with the NaOH to a light pink endpoint. The volumes of NaOH were recorded, averaged, and the standardized. The molarity of the NaOH was found to be 0.0981.…
6. Insert the pH meter into the Erlenmeyer flask and record the initial pH of the acid. Remember to record the pH of the solution after every 5 milliliters of NaOH added.…
7. Put 10 drops of 0.5 M nitric acid and 10 drops of 0.5 M phosphoric acid into separate test tubes. Add 1 drop of phenolphthalein to each test tube. Add drops of dilute (0.5 M) sodium hydroxide solution into each of the test tubes until a permanent color change is observed. (NOTE: Phenolphthalein is an acid-base indicator that is colorless in acidic and neutral solutions, but pink in basic solutions). HINT: When writing your net ionic equations: nitric acid is a strong acid while phosphoric acid is a weak…
Materials and Methods: A buret with NaOH solution was used to ensure an accurate measure of NaOH could be taken. A PH recording machine was used to measure the PH. To make sure 25.0 ml of the unknown was measured, we used a 25.0 ml pipet.…
This lab experiment covers the preparation of standard solution and the acid/base titration. The first part of the lab is to prepare a standard solution of Potassium hydrogen per. A standard solution is a solution of known concentration, in which it is prepared using exacting techniques to make sure that the molarity is to the highest accuracy. The stock solution on the other hand, which is also a base in this experiment, is a large volume of a common reagent prepared…
While our ecosystem does exist, without dramatic changes, we can speak of the objects without contradicting anything in it. The existence of the ecosystem is contingent on human society, it is very important that we acknowledge that. The people that play one of the most important roles are the environmental scientists. They describe the ecosystem and in the correct management of the ecosystem, but we miss the importance of the human role in the environment if we discretely see the objects of the ecosystem as independent of the human society. Just a few years ago we had an oil spill in the Gulf of Mexico that was caused by BP Oil Company. This impacted the whole gulf coast not just the animals. They had to pay almost 8 billion dollars to businesses and families. The spill caused major damage to marine, wildlife habitats, and to the Gulf's fishing and tourism industries. Being from Louisiana I seen firsthand the effect the spill had on the gulf coast. Seafood is one of the biggest markets we have in Louisiana and we could not eat, buy, or sell anything out of the gulf. Skimmer ships, floating containment booms, anchored barriers, sand-filled barricades along shorelines, and dispersants were used in an attempt to protect hundreds of miles of beaches, wetlands, and estuaries from the spreading oil. Scientists also reported immense underwater plumes of dissolved oil not visible at the surface as well as a "kill zone" surrounding the blown well.…
The goal of this lab was to correctly prepare a 0.2M solution of NaOH, identify highly acidic household cleaning chemicals, and determine their concentration (molarity) through titrations using the previously prepared 0.2M NaOH solution.…
2. Repeat the same steps 5-7 substituting the unknown acid for KHP. The unknown acids are in labeled jars A, B, and C. It will be indicated whether the acids are monoprotic, diprotic, or triprotic. 10 titrations should be completed for each unknown acid.…
Week One: the experiment started off by preparing 250mL of NaOH solution. About 0.5 grams of NaOH were measured and then inserted into a 250mL volumetric flask. Once the NaOH was in the flask, it was then filled up to the 250mL line using deionized water. After the water was put in the flask, the solution was then mixed well until the NaOH dissolved well in the water. The second solution that was prepared was KHP. This was done by measuring 1 gram of KHP. After that was completed, the KHP was put in a beaker and filled up using 50mL of demonized water and mixed well until the KHP dissolved well in the water. Three drops of the indicator phenolphthalein were put in the KHP solution.…
Fig 2: Titration of an acid to a base by using phenolphthalein as the indicator.…
In “Part B” experiment, we use a strong acid (HCl) and a weak acid (acetic acid) titrates with a strong base (NaOH). In both titrations, we will monitor the change in PH to determine the volume of 0.100 M NaOH required neutralizing both 10ml sample of HCl and acetic acid. And refer to the neutralization reaction of these two acid, H+ (aq) + OH-(aq) → H2O(l) for HCl, and CH3COOH(aq) + OH-(aq) → CH3COO-(aq) + H2O(l) . as we can see , in both case, two reaction have 1:1 stoichiometry, the moles of NaOH added = moles of acid present in the 10.00 mL sample , this will allow to calculate the concentration of acid in the original sample.…