Chem 21 Fall 2009 Experiment 9 — Recrystallization _____________________________________________________________________________ Pre-lab preparation. (1) Read the supplemental material from Zubrick‚ The Organic Chem Lab Survival Manual. (2) Draw the structure of acetanilide and report relevant physical data. Be sure to cite the source of the data. You should be able to figure out what’s relevant by reading the procedure. (3) Find and report the boiling points of the solvents you will be using
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artificial flavoring. Data: Conclusion: Different dyes are shown when separated by different concentrations of isopropyl alcohol. Discussion of Theory: Chromatography‚ resolution and selectivity played major roles in making the experiment work. The experiment demonstrated a common use of chromatography‚ and works to explain a way to separate mixtures. The dyes were successfully separated and analyzed in the cartridge. Experimental Sources of Error: We could have produced better results if
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CHEM 2204 Chromatography Lab by wyk.wong » Fri Jul 11‚ 2014 10:25 am Results and Calculations Rf values Rf=(Distance moved by the spot (cm))/(Distance moved by the solvent front (cm)) Toluene: Rf=2 cm/3.8 cm=0.53 (Fluorenone) Rf=1.1 cm/3.8 cm=0.29 (Fluorene) Hexane: Rf=1.8 cm/2.2 cm=0.82 (Fluorene) Rf=0 cm/2.2 cm=0 (Fluorene Table 1: Experimental IR peaks compared to literature IR peaks for fluorenone Functional group Experimental peak (cm-1) Literature peak (cm-1) C-H 3010.5 3013
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Hannah Herbert BioL121 9/16/14 Density and Making Solutions Objective and Background/ Theory of Experiment: The objective of the experiment was to determine the density of a metal along with the density of distilled water. In an attempt to help the experimenters more thoroughly understand the relationship between concentration and density. Archimedes a Greek mathematician in the third century B.C. originally determined the relationship between the amount of matter that is within a particular space
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Purposes of Experiment: To synthesize a transition metal complex‚ potassium tris (oxalate)ferrate(III) trihydrate in a two step process‚ to learn new laboratory techniques such as decantation‚ recrystallization‚ gravity and suction filtration. Also the purpose of the experiment is to determine the actual‚ theoretical‚ and percent yields of product‚ and characterize the final compound by determining the number of waters of hydration by gravimetric analysis List of Observations: After adding
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Chem 31.1 Post Lab 3 CARBONYL COMPOUNDS AND CARBOHYDRATES HYDROLYSIS OF POLYSACCHARIDES - - Susceptible to both nucleophiles and electrophiles Presence of C=O TEST FOR ALDEHYDES AND KETONES - - Reaction with 2‚4-DNP (Dinitrophenylhydrazine) Positive: Formation of yellow precipitate IODOFORM TEST - Carbonyl compounds: Methyl ketones will give a positive result Postive: Yellow precipitate (CHI3) MOLISCH’S TEST for carbohydrates - TOLLEN’S TEST – for aldehydes
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Give brief answers to the following questions : 1. What happens to a molecule when it absorbs UV light ? rvv’ill occra’’ 6e cfr’oh fvhan ?- rr.ote c ulQ a$c‚ovb r4V t;g hl ‚ ?*rltdfi’oh o{ olQelraq ofc pronrottd potn *h’Qhr lraur1 dt *q‚fe to erc;feC‚ slst<‚Th<;6bSotb1 ) qh’:o&s ih n^olf c’‚la g r.in9 qb‚olal ob{‚1tr.ira :Lind c o1 et<cif l‚pln+t qt"d QqCh W-qrtr\ve 1t5 ou‚ 4iSfictlre ancvcry.0rl+yorvi6lst: qnI vrstblC t;Jht brin3 lboql rrrovc tbq\i v orl{rrro e.tCclro tts t5 Ricorlt5 fu o rv
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Majed Al Dhwaihi Chem 151 Lab Prelab Assignment for week 3 Chemical Separation Procedure: Separating the sample: First place a small amount of the spinach provided in the mortar‚ just enough to cover its bottom; combined with the sand provided to break down the call walls. A 1:1 mixture of hexane and acetone was determined to best solvent for this extraction. Knowing this add one mL of the pure hexane and one mL of the pure acetone to the mortar. Grind the contents until the cell walls
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Patel Chem 101 10-13-09 Introduction The objective of this lab was to show how stoichiometry is applied to a specific chemical reaction. Stoichiometry is pretty much the math behind chemistry. Doing stoichiometry can calculate masses‚ moles‚ and percents with a chemical equation. The use of stoichiometry is how we were able to find the limiting reagent in this lab. A limiting reagent is the chemical that will be used up first. Many calculations had to be made throughout this lab. Some
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Pre-Laboratory Assignment 1. What are the hazards associated with sodium hydroxide (NaOH) solution? Sodium hydroxide solutions‚ especially in high concentrations‚ are toxic and corrosive. 2. (a) What buret reading should you record when the liquid level is as shown in Figure 2? In Figure 2‚ the lower meniscus lies below the 3 mL line and 4 minor gradations that signify 0.1 values. Estimating the uncertain digit to be 0.04 mL‚ the reading we record for this particular buret is 3.44 mL.
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