alkenes Aim: Is cyclohexane more or less reactive than cyclohexene in the presence or absence of light Hypothesis The cyclohexene will reactive the fastest because being an "ene" it has a electron rich area making it more reactive than cyclohexane but neither one of the will react without light Materials * 4x 250ml conical flasks * 2 rubber stoppers * Aluminium foil * Cyclohexane * Cyclohexene * Bromide water * Measuring cylinder Risk assessment
Premium Erlenmeyer flask Oxygen Color
Alkene Synthesis from Alcohol: Preparation of Cyclohexene From Cyclohexanol 5/29/14 Abstract: A 42.89% yield cyclohexene was successfully synthesized from 10.0 mL cyclohexanol by unimolecular elimination (E1) through the dehydration of cyclohexanol and confirmed via a bromine test and the IR spectra. Introduction: Alkenes are hydrocarbons that have carbon–carbon double bonds and are one of the many functional groups in organic molecules. Alkenes are sp2 hybridized
Premium Alkene Alcohol Oxygen
Dehydration of Cyclohexanol Introduction In this experiment cyclohexene‚ an alkene‚ was prepared by the dehydration of cyclohexanol‚ an alcohol‚ using phosphoric acid‚ an acid catalyst. The reaction is as follows: [pic] The dehydration of cyclohexanol was performed in a simple distillation apparatus. As cyclohexene formed‚ it was distilled out of the mixture. Background Dehydration is an elimination reaction of an alcohol that takes place in the presence of an acid catalyst
Free Distillation
hydrocarbons or arenes. The different between these groups is in the bond types between the carbons. Objective: 1- To observe the flame of cyclohexane and cyclohexene. 2- To observe the effect of adding sulphuric acid on cyclohexane and cyclohexene. Apparatus Needed: Test tubes and rack‚ watch glass‚ and matches. Chemical Needed: Cyclohexane‚Cyclohexene‚ 1M of sulphuric acid. Procedures: A. Combustion (to be performed under fume hood) 1. 2-3 drops of liquid cyclohexane are dropped onto a watch glass
Premium Carbon Chemical bond Oxygen
CHM 337 | Dr. Pettit Abstract: A solution of cyclohexene‚ aqueous sodium hydroxide‚ and benzyltriethylammonium was used to synthesize 7‚7 – dichloronorcarane by the following reaction: + CHCl3 + OH - H2O + + Cl - After completion of the experiment‚ the percent recovery was calculated to be 46.21% Introduction The purpose of this experiment was to form 7‚7-dichloronorcarane by means of carbene trapping. Cyclohexene‚ aqueous sodium hydroxide‚ and benzyltriethylammonium
Premium Chlorine Sodium hydroxide Sodium chloride
Dehydrating Cyclohexanol • Introduction The purpose of the lab experiment is to prepare cyclohexene from cyclohexanol through an acid-catalyzed dehydration. In order to produce the cyclohexene from cyclohexanol‚ an elimination reaction was performed. First by protonating the oxygen of the alcohol and creating an oxonium ion we replaced the poor leaving group (OH) into a better leaving group (OH2+). Second‚ dehydrating the cyclohexanol using phosphoric acid and sulfuric acid as acid catalysts
Premium Distillation Oxygen Water
Cyclohexanol can be produce through several methods‚ which include the oxidation of cyclohexane‚ the hydration of cyclohexene‚ or the hydrogenation of phenol (Zhang‚ et al‚ 2002). Problem with oxidation of cyclohexene is poor selectivity‚ extremely large recycles and explosion hazards. (Suresh‚ Sridhar‚ Potter‚ 1988). The purpose of this experiment was to synthesis cyclohexanol by hydration of cyclohexene using concentrated sulphuric acid as an acidic catalyst. In hydration reaction‚ C=C B bond is replaced
Premium Management Marketing German language
Dehydration of Alcohols Abstract The dehydration of cyclohexanol to cyclohexene can be done through fractional distillation. Once the fraction has been collected it must then be dried. The dried distillate is finally tested to determine whether or not it has been dehydrated. The three tests used were infrared spectroscopy‚ Bromine chemical test and Bayer’s chemical test. The infrared spectroscopy showed a large narrow peak at 3062.12(cm-1) and 3020.71(cm-1) which indicates that there is a double
Premium
Mario Troncoso 20025019 Dehydrating Cyclohexanol Structure/MSDS: Anhydrous calcium chloride—irritant and hygroscopic (calcium chloride) cyclohexanol—irritant and hygroscopic (cyclohexanol) cyclohexene—flammable and irritant (cyclohexene) Sulfuric acid—toxic and oxidizer (Sulfuric acid) phosphoric acid—corrosive (phosphoric acid) Results/Data: End product weighed 0.109g of cyclohexane and tested positive with bromine test Discussion: In order to perform
Premium Sulfuric acid Laboratory glassware Distillation
Cyclohexanol Cycle. The cyclohexanol was first converted to cyclohexene and water by simple distillation (product: 6.5395g‚ 79.75% recovery). The cyclohexene then underwent a bromination reaction by addition of concentrated HBr and a 30% H2O2 solution‚ followed by an extraction of the aqueous phase. This produced trans-1‚2-dibromocyclohexane (product: 12.8886g‚ 67.34% recovery). The trans-1‚2-dibromocyclohexane was reduced by zinc metal to cyclohexene. The reaction was conducted in water‚ first allowing
Premium Chemistry