1. Standarization of NaOH with Potassium Hydrogenphthalate (KHC8H404) The hygroscopic nature of NaOH requires its solution to be standardized with a stable primary standard such as potassium hydrogen phthalate. The exact molar concentration of NaOH solution can then be accurately determined. 1.1) Prepare the stock NaOH solution by dissolving about 4 g of NaOH pellet in 100 mL of deionized water. Note that NaOH is a hazardous chemical which is corrosive to skin and irritant to eye‚ be cautious and
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versus the volume in milliliters of 0.1 M NaOH‚ a strong base‚ added to the solution. The initial pH reading of the solution was a pH of 2.60. Although the pH of the ½ equivalence point was unknown‚ it could be estimated by halving the volume of NaOH used at the first equivalence point. At the first equivalence point‚ 13.63 milliliters of NaOH had been added to the unknown acid solution. Once divided by two‚ that value ended up being 6.815 milliliters of NaOH added at the ½ equivalence point pH. In
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Volume of NaOH Required to Neutralize 10.00mL of Unknown HCl Molarity of NaOh | Trial 1 | Trial 2 | Trial 3 | Trial 4 | Initial Volume of NaOH(mL) | 0.00 | 11.00 | 20.85 | 30.45 | Final Volume of NaOH(mL) | 11.00 | 20.85 | 30.45 | 39.98 | Volume of NaOH used(mL) | 11.00 (Cancel out) | 9.85 | 9.60 | 9.53 | Average Volume of NaOH = (9.85+9.60+9.53)/3 = 9.66mL Sample Calculations: (9.85+9.60+9.53)/3 = 9.66mL The average volume of NaOH used. Calculations: 1. Moles NaOH = M x V = (0
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The aim of this experiment was to calculate the concentration of an unknown solution of Sodium Hydroxide (NaOH) by titrating it with Hydrochloric Acid (HCl) and to identify any possible sources of error. A colour change from pink to yellow signified the end of each individual titre as the NaOH had been neutralised. Experimental: Method: Firstly two solutions were prepared to show the colour of the Phenol Red indicator in acid and alkaline conditions. These colours were then used to determine the
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Indicator 1. Fill the 50-milliliter buret with a 0.25 molar NaOH solution. 2. Record volume. 3. Measure out between 20 milliliters and 40 milliliters of the unknown HCl solution. 4. Record volume. 5. The amount of unknown HCl is then added to the 100-milliliter Erlenmeyer flask. 6. Add two drops of the indicator‚ phenolphthalein‚ to the acid in the flask. 7. Using the slider on the right hand side‚ add NaOH to the HCl in the Erlenmeyer flask (This action is known as titrate)
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ABSTRACT In the majority field of chemical processes‚ the reactor vessel in which the reaction process take place is the key component of the equipment.The design of the reactors is very important to the success of the production. In this experiment‚ sodium hydroxide and ethyl acetate react in tubular flow reactor.Both of the reactants fed to the reactor at equimolar flowrate for a certain time.The reaction is carried out at different volumetric flowrate.The conductivity value of outlet stream
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9 Experiment A Volumetric Analysis A titrimetric analysis requires the careful addition of titrant. • To prepare and standardize a sodium hydroxide solution • To determine the molar concentration of a strong acid Objectives The following techniques are used in the Experimental Procedure Techniques 2 4 16b 16a 90 80 5 16c 6 13c 15a 15b ! A chemical analysis that is performed primarily with the aid of volumetric glassware (e.g.‚ pipets‚
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The kinetics of the reaction can be monitored due to the carbocation form of the dye by measuring the decrease in absorbance at the wavelength corresponding to the absorption maximum(λmax). The hydrolysis is carried out by using a large excess of NaOH (more than 10-fold) with respect to the substratecrystal violet such that the reaction (CV+ + OH-↔ CVOH) obey the pseudo-first order reaction rate equation -d[CV+]/dt = kw[CV+][OH-]=k[CV+] Where k=kw[OH-] is the pseudo-first order rate constant and
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Overview • • • • after calibration of the pH electrode and determination of the flow rate for the automatic titration‚ a NaOH solution is standardized against HCl. a pH titration curve for acetic acid is obtained and its pKa is determined. an unknown sample of Lysol is analyzed for its HCl content using the standardized NaOH. an unknown sample of Liquid Plumr is analyzed for its NaOH and NaOCl content using HCl of known molarity. 7 Name ______________________________ Section _______ Date ____________________
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By: Andrew Hoitt CHEM 105 Lab 11/29/2012 Lab # 11 – Acid - Base Titration Introduction: The purpose of this lab is to determine the molarity (M) of an unknown HCl solution. A NaOH solution will be made and its molarity calculated. A sample of the NaOH solution will be titrated against the unknown HCl solution to calculated the volume needed to neutralize it. With these volumes the unknown molarity can be calculated. Theory: Solutions are made up of
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