temperature Step 8: Cooled the solution in an ice bath for 5 minutes Step 9: Collected the crystalized solid by vacuum filtration Step 10: Measured the melting point for the crystalize solid Reagent Table: Table 1: The chemicals and properties used in the reaction Compound Quantity Molar Mass (g/mol) Melting Point (C) Boiling Point (C) Anthracene 0.5g 178.23 216-218 340 Maleic Anhydride 0.25g 98.06 54-56 200 Potassium Bromide 100 119 63.38 759 Xylene 6mL 106.17
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% by volume of the fat‚ a nitrogencylinder With flowmeter is connected to suction of feed pump 40 3-5 Crystallization System ( Refrigeration Load : 1T/ HR-50 TR) Average Composition of a General purpose Bakery Fat : High Melting Point Middle Melting Point Lower Melting Point Til Oil (Sesame) 43-44ºC 35-36ºC 28-30ºC 50% 35% 12% 3% 100% Equipment Fat Temp ºC RPM Residence In Out Time Seconds Performer I 47+2 34+2 400-500 20 Performer II 34+2 24+1 400-500 20 Maturator I 24+1 28+1 175-200 90-180
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by Actual yield of synthesised aspirin: 0.347g 0.347/1.196 * 100= 29 Percentage yield: 29% Melting Points Compound Began Melting (°C) Totally Melted (°C) Range (°C) Pure Aspirin 136 1-2 Crude Aspirin 125 130 5 Product from Willow Bark 120 125 5 The documented melting point for pure aspirin is 136°C. An impure compound will exhibit a lower melting point than this‚ which is what was observed in both the willow bark product and the crude aspirin. Pure aspirin has a narrow
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completes the statement or answers the question. ____ 11. The phase change that is the reverse of sublimation is a. deposition c. condensation. b. vaporization. d. melting. ____ 12. The phase change in which a substance changes from a solid to a gas or vapor without changing to a liquid first is a. melting. c. deposition. b. sublimation. d. vaporization. ____ 13. If a solid piece of naphthalene is heated and remains at 80°C until it is completely melted‚ you know that
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amount of heat required to convert a mass of a solid at its melting point into a liquid without an increase in temperature. As difficult as this may sound‚ this experiment can be carried out with minimal equipment. The following equipment was needed‚ a 100mL graduated cylinder‚ a calorimeter‚ a digital thermometer‚ a calculator‚ water‚ and ice cubes. Procedure: The procedure to find the heat of fusion for ice was measured by melting ice cubes in a known volume and temperature of water and carefully
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Lab 6: Organic Compound Analysis Isabella O’Toole CHY 116 Friday 1:15-4:00 Lab Conducted on 4-12-13 and 4-19-13 4-26-13 This lab was conducted in order to determine the chemical composition of an unknown organic acid. A known mass of acid was dissolved into 30mL of either water or methanol (depending on solubility) and titrated with standardized sodium hydroxide. Data from this allowed the molar
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Lab Name: Molar Mass by Freezing Point Depression Researcher: Isabella Cuenco Lab Start Date: November 9‚ 2012 Lab Completion Date: November 9‚ 2012 Table of Contents SECTION NAME I. Introduction II. Procedure III. Data IV. Analysis V. Conclusion PAGE NUMBER I. INTRODUCTION Purpose: The purpose of the lab is to find the molar mass of an unknown substance by measuring the freezing point depression of a solution of the unknown
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Polymer Essay: Plexiglass Many of the glass screens and windows we see today are not really made of glass. They are made of plexiglass. Plexiglass is not related to the chemical structure of glass at all. It is an organic polymer. Today this polymer is used in all sorts of applications. The formation of plexiglass was begun in 1930‚ at McGi11 University by William Chalmers‚ a research student. He polymerized methacrylic ethyl ester and methacrylic nitirile‚ creating a clear plastic paste
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temperature where the lowest melting constituent of steel starts to melt. The strength decreases and looses plasticity and tind to crumble under applied stress instead of flow. 2. Selection of temperature depends on a) Chemistry. b) Melting point of the lowest constituent. 3. Finishing temperatures. Lower the finishing temperature finer the structure of the piece but limited to mass and shape. The finishing temperature should be near the lower transformation point. SCALING 1. Not
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Physics Facts & TriviaA rubber band shrinks when heated and expands when cooled because of the change in its Entropy state.Submitted by: Emily (Awesome) - Helena‚ Montana‚ United StatesDue to the effect of Thermal Expansion‚ the Eiffel Tower is upto 15cm taller in summer.Submitted by: Muhaimin Mareum Khan - Dhaka‚ BangladeshRadar is an abbreviation ofRadio Detection And Ranging.Submitted by: Marvin Jadulos - PhilippinesIf an atom were the size of a stadium‚ its electrons would be as small as
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