BTEC Chemistry – Titration experiment I – Standard Solution Prep Preparation of a standard solution of sodium carbonate Anhydrous sodium carbonate is a suitable chemical (primary standard) for the preparation of a standard solution. Standard Solutions are critical in chemistry because you need to have solutions with an EXACT known concentration and volume. Chemicals/Materials: solid sodium carbonate (Na2CO3) distilled water Apparatus: 250cm3 volumetric flask 250cm3 beaker Glass
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October 9‚ 2013 Partner(s): Acetylsalicylic Acid Synthesis Theory. This experiment was carried out to see how the hydroxyl group on the benzene ring in salicylic acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above
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My Reaction Paper This is my reaction paper on a movie that I watched entitled “The Wizards Of Waverly Place: The Movie”. Wizards of Waverly Place: The Movie follows the Russo family as they embark on a vacation to the Caribbean resort where Jerry and Theresa first met. Alex‚ upset that she was forced to accompany her family on the trip‚ conjures a spell that erases her parents’ fateful first meeting and puts the Russo family’s very existence in peril. In order to reverse the spell‚ Alex
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Objective: Using sodium borohydride as a reducing agent‚ the ketone 4-tert-butylcyclohexane is reduced to its corresponding alcohol. It is purified through extraction techniques to give the cis and trans diasteromer products. Procedure: The procedure was followed as outlined in Mayo’s book for Experiment 5B with the following modifications: 1. Reagents and Equipment – The reaction will be on a scale of 2X what is described in the text. 2. Reagents and Equipment – The progress of the reaction will be followed
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supplied food acid is citric acid (triprotic) or tartaric acid (diprotic acid) Materials 4 x 100mL conical flasks 50mL burette rubber bulb 1 x 200mL beaker white tile retort stand 20mL volumetric pipette volumetric flask stopper 300mL distilled water marker 40mL 0.3M food acid burette clamp 0.1M sodium hydroxide magnetic flea magnetic stirrer glass funnel 1 x 200mL volumetric flask phenolphthalein 4 x 50mL beakers Method Part A: Making the food acid Place distilled
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to the appropriate significant figures. 15-1 Molarity Problems: (M = moles/ liter ) 1. What is the molar concentration of a 415 ml solution containing 0.745 moles of HCl? (A: 1.80 M HCl) 2. What is the molar concentration of an acetic acid (CH3COOH) solution containing 3.21 moles in 4.50 liters? (A: 0.713 M) 3. How many moles of KI are present in 125 ml of 0.500 M KI? (A: 0.0625 mol KI) 4. How many moles of ammonia (NH3) are present in .360 L of 2.13 M NH3 solution in water
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9.1 Sulphuric Acid Sulphuric Acid is Manufactured in Industry 1. Sulphuric acid‚ H2SO4 is manufactured in industry through Contact Process. 2. The raw materials used are sulphur‚ air and water 3. The Contact process consists of three stages. Stage 1: The production of sulphur dioxide This can be obtained by two methods: 1. Burning of sulphur in dry air in the furnace S + O SO2 2. Burning of metal sulphide such as zinc sulphide or iron(III) sulphide in dry air. 2ZnS
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Acid-Base Calculations The Ion-Product Constant for Water‚ Kw Water undergoes ionization to a small extent: H20(l) H+(aq) + OH–(aq) The equilibrium constant for the reaction is the ion-product constant for water Kw: (1) This is a key equation in acid-base chemistry. Note that the product of [H+] and [OH–] is a constant at a given temperature (Eq(1) value is for 25oC). Thus as the hydrogen ion concentration of a solution increases‚ the hydroxide ion concentration decreases
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nitrogens on this station. Both of these methods rely on the repulsive electrostatic interactions between the positively charged axial component and the post-switching cationic nature of the benzidine station (Figure 5.4). Deuterated trifluoroacetic acid (d-TFA) was added in the solution which resulted in the protonation of the benzidine residue and shuttling of macrocycle in to the biphenol station of the Rotaxane. This was supported by NOESY 1H NMR that showed a shift in the peaks in retrospect to
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But-2-enedioic acid Introduction Cis-trans isomers are a kind of stereoisomers called geometrical isomers. Due to the inability of rotation about the C=C bond‚ some compounds possess cis and trans isomers. But-2-enedioic acid is an example of having both isomers. Maleic acid Fumaric acid Cis and trans isomers have different physical properties such as boiling point‚ solubility‚ density and stability. In this experiment some maleic acid is converted to fumaric acid by
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