Lab 3: Bromination of Acetanilide CHEM 2110 Hassan Alsaleh 0525970 Due date :11/02/2015 Q1: To find the limiting reagent we need to find the number of moles of acetanilide‚ and the number of moles of Bromine. Mass of Acetanilide used = 0.67g Molar mass of Acetanilide = 135.16g/mol[1] Number of moles of Acetanilide = (0.67g) / (135.16g/mol) = 0‚005 mols Volume of Bromine = 0.25ml Density of Bromine = 3.103 g/ml[2] Mass of Bromine = (0.25ml) X (3.103g/ml) = 0.78g Molar mass of Bromine
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Results and Calculations: Table of reagents Name Density (g/ml) Amount used Amount # moles Bromine (excess) Trans-cinnamic Acid 1.246 g/cm3 0.148g – do conversion Dichloromethane 1‚3266 g/cm3 - Table of Results Name Amount obtained Molar Mass (g/mol) Amount used (moles) Melting point (Celsius) Color/observations 2‚3-dibromo-3-phenylpropanoic acid 0.285g 307.97 200.4 – 205.1 White powder Limiting reagent: Trans-cinnamic acid (148.16g/mol) 2.5g/148.16g/mol=0
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Ice Calorimeter Determination with Mg June 18th 2013 Abstract: This experiment determines the amount of energy needed to melt ice. A spontaneous increase in enthalpy produce by combining 0.2036g Mg and 5.00mL H₂SO₄‚ ice was melted and readings were taken by using an ice calorimeter. Readings were taken before during and after the reaction were completed. The data taken shows a value of -405 KJ/mol while the theoretical value was -483.7 KJ/mol. Calculating the experimental
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Experiment 3: Stoichiometry of a Precipitation Reaction Abstract: In this experiment the objectives were to try and predict the amount of product that was produced in the precipitation reaction of calcium carbonate by using stoichiometry. Then learn how to figure out the actual yield‚ theoretical yield and percent yield of the experiment. Experiment and Observation: The first step in the experiment was to weigh 1g of CaCl2 +2 H2O‚ then pour it into the 100mL
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Experiment 11 Calorimetry and Hess’s Law Purpose- To determine the change in enthalpy for four reactions using calorimetry and Hess’s Law Procedures: A. Calibration of the Calorimeter 1. Obtain two copper cylinders and a Styrofoam cup with lid from your lab instructor. Check out a digital thermometer display from the storeroom window. 2. Set up a hot water bath using a 600mL beaker‚ ring stand‚ and Bunsen burner. Weigh the two copper cylinders
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For known amounts of reactants‚ theoretical amounts of product can be calculated in a chemical process. These calculated products are determined using the limiting reagent‚ (the substance that runs out first which stops the reaction) and are called the theoretical yield. The theoretical yield is the amount of product that should be acquired during the experiment if all aspects go perfectly. However‚ due to experimental errors‚ very few labs do so. These results are called actual yield. The percent
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07.04 Equilibrium: Hands-On Equilibrium Demonstration Lab Equilibrium Model Materials: • a minimum of 80 small candies‚ coins‚ or other objects • one blank sheet of paper • one notebook Introduction: For this lab‚ we will be using small items‚ such as candies‚ to represent chemical compounds undergoing a reaction. Draw a line down the middle of a sheet of paper and label the left side of the paper “R” for reactants and the right side “P” for products. R P To represent molecules that are
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Introduction The experiment is testing for the formation of precipitates caused by different limiting reactants. A precipitate results in a solid formed by an ionic compound. Calcium nitrate and copper sulfate will be added to separate beakers with approximately half of the solutions from the Büchner funnel system of each trial to test for the formation of precipitates. The limiting reactant is the reactant that will run out first in the chemical reaction. It is important to recognize which chemical
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Grignard reagent‚ and react it with benzophenone to give triphenylmethanol. Once made‚ the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone‚ benzophenone. The result is an alkoxide that is then protonated to give the alcohol‚ triphenylmethanol. The purity of the final product will then be considered by melting point and IR spectroscopy. Final purified triphenylmethanol weighed 8.02 grams and melted at 158.5-162 degrees Celsius. Introduction: Grignard reagents are
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products in a chemical reaction to determine desired quantitative data. Doing stoichiometry can calculate masses‚ moles‚ and percent’s with a chemical equation. The use of stoichiometry is how we were able to find the limiting reagent in this lab. We know that the limiting reagent is the chemical that will be used up first. Two factors affect the yield of product in a chemical reaction: the amounts of starting materials and the percent yield of the reaction. Under certain conditions such as temperature
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