Introduction In a Grignard reaction‚ a Grignard reagent (R–MgX) adds to the carbonyl group in an aldehyde or ketone to form an alcohol (Figure 1). The reaction of a Grignard reagent with formaldehyde can be to synthesize a primary alcohol‚ with any other aldehyde can be used to synthesize a secondary alcohol‚ while the reaction with ketone is useful in the synthesis of a tertiary alcohol. Figure 1. General reaction mechanism of a Grignard Reaction The preparation of the Grignard reagent involves
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Micro-Reactions: Predicting the Products of Double Replacement Reactions Introduction – A double replacement reaction is a chemical reaction between two compounds where the positive ion of one compound is exchanged with the positive ion of another compound. If you have the reactants of two reaction solution that you can determine the products. All you need to do is pair the positive parts of the compounds with the other compounds negative part. Once you find the products you can determine their
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The progress of the reaction was monitored in my case using two TLC plate. It first started off with the spotting of Standard benzoin and benzil which were provided in the lab and followed by the addition of the reaction mixture at once it starts changing colour/boiling‚ then at 10 and 20 mins into the reflux. Once all the necessary steps were spotted‚ the TLC plate was placed in in a beaker containing CH₂Cl₂(methylene chloride)‚ which was used as the developing solvent in this experiment. To check
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Grignard Reaction: Synthesis of Triphenylmethanol Hai Liu TA: Ara Austin Mondays: 11:30-2:20 Abstract: In this experiment‚ phenylmagnesium bromide‚ a Grignard reagent was synthesized from bromobenzene and magnesium strips in a diethyl ether solvent. The Grignard reagent was then converted to triphenylmethanol‚ a tertiary alcohol with HCl. The reaction for phenylmagnesium bromide was: The reaction for Grignard to triphenylmethanol was: In the formation of the Grignard reagent
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Summary This experiment will measure the rate of oxidation of iodide ions by persulphate ions to derive the rate law for the reaction. Starch will be added to the reaction to facilitate the measure of time during the reaction. The reactant solutions will contain (NH4)2SO4 and KI‚ represented as: (NH4)2S2O8 + 2KI -> I2 + (NH4)2SO4 + K2SO4 This can be simplified to: S2O82- + 2I- -> I2 + 2SO42- These equations can only be carried out and be visible after the iodine has completely
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factors affecting the kinetics of reaction between peroxodisulfate (vi) and iodide d. del prado1 and j. belano2 1 department of food science and nutrition‚ college of home economics 2 department of food science and nutrition‚ college of home economics university of the philppines‚ diliman‚ quezon city 1101‚ philippines date submitted: january 7‚ 2013 ------------------------------------------------- ------------------------------------------------- ABSTRACT -------------------------------------------------
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Aim During this experiment I will be investigating if heating limestone and changing the concentration of the acid will affect the rate of reaction. Preliminary work Before doing our main experiment‚ we will have to conduct another experiment‚ to see what concentration of acid we will have to use. We done this using 0.1M‚ 0.5M and 1M of Hydrochloric acid‚ and 0.1g of powdered limestone‚ we used powdered limestone‚ as it would be a fairer test‚ I think this as all the particles of limestone will
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The Grignard Reaction Abstract Through the use of the Grignard reaction‚ a carbon-carbon bond was formed‚ thereby resulting in the formation of triphenylmethanol from phenyl magnesium bromide and benzophenone. A recrystallization was performed to purify the Grignard product by dissolving the product in methanol. From here‚ a melting point range of 147.0 °C to 150.8 °C was obtained. The purified product yielded an IR spectrum with major peaks of 3471.82 cm-1‚ 3060.90 cm-1‚ 1597.38 cm-1‚ and 1489
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The E2 reaction performed began by dehydrohalogenating the 3-chloro-3‚ 7-dimethyloctane with potassium hydroxide in aqueous ethanol. The 3-chloro-3‚ 7-dimethyloctane will lose a hydrogen from three different carbons that cause the formation of three constitutional isomers. If the hydroxide ion attacks a hydrogen on the 3-methyl carbon‚ then 2-ethyl-6-methyl-1-heptene will be the product. If a hydrogen on the carbon-2 was attacked‚ then the product would be 3‚ 7-dimethyl-2-octene. If a hydrogen was
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the majority of his time to his dog-racing activities‚ he feels it should be considered a business and should be allowed to deduct his losses against their other income. Issues Is Larry’s professional gambling considered a business or a hobby by the IRS? Would Larry be able to deduct the loss he incurred in his “business” against their other income? Conclusions Larry’s professional gambling is considered a business since he has no other income and spends 50 to 60 hours a week on his gambling studies
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