The first step in the procedure was to obtain and label ten test tubes and also three 50 mL beakers with the labels of sodium thiosulfate, potassium iodine, and hydrogen peroxide. Then 20 mL of sodium thiosulfate, 25 mL of potassium iodine, and 35 mL of hydrogen peroxide were added to their respective beakers. Next, 2.0 mL of sodium thiosulfate was added to test tubes 1-9 using a volumetric pipet. After that, potassium iodine and distilled water were added to the test tubes 1-9 with their respective amounts given by Table 1 in the lab manual. Sodium molybdate, a catalyst, was added to test tubes 6-8, and 10 mL of peroxide solution was added to test tube 10. An ice bath was also prepared for test tubes 8-10 to chill in for approximately 20 minutes. Part B of the experiment served to determine the reaction rates. Hydrogen peroxide was added to each test tube and the reactions were observed one by one. Once the hydrogen peroxide was added, an online stopwatch was started and a temperature probe was placed in the test tube to monitor the reaction. The timer was stopped when the solution turned blue and the temperature and time were recorded. This procedure was repeated for test tubes 2-7. For test tubes 8 and 9, the chilled hydrogen peroxide from test tube 10 was used instead of the room temperature hydroxide. Clean up protocols were then
The first step in the procedure was to obtain and label ten test tubes and also three 50 mL beakers with the labels of sodium thiosulfate, potassium iodine, and hydrogen peroxide. Then 20 mL of sodium thiosulfate, 25 mL of potassium iodine, and 35 mL of hydrogen peroxide were added to their respective beakers. Next, 2.0 mL of sodium thiosulfate was added to test tubes 1-9 using a volumetric pipet. After that, potassium iodine and distilled water were added to the test tubes 1-9 with their respective amounts given by Table 1 in the lab manual. Sodium molybdate, a catalyst, was added to test tubes 6-8, and 10 mL of peroxide solution was added to test tube 10. An ice bath was also prepared for test tubes 8-10 to chill in for approximately 20 minutes. Part B of the experiment served to determine the reaction rates. Hydrogen peroxide was added to each test tube and the reactions were observed one by one. Once the hydrogen peroxide was added, an online stopwatch was started and a temperature probe was placed in the test tube to monitor the reaction. The timer was stopped when the solution turned blue and the temperature and time were recorded. This procedure was repeated for test tubes 2-7. For test tubes 8 and 9, the chilled hydrogen peroxide from test tube 10 was used instead of the room temperature hydroxide. Clean up protocols were then