Preview

The Effect of Ph on a Food Preservative

Satisfactory Essays
Open Document
Open Document
690 Words
Grammar
Grammar
Plagiarism
Plagiarism
Writing
Writing
Score
Score
The Effect of Ph on a Food Preservative
The Effect of pH on a Food Preservative

September 18, 2012

Objective:
To study the affect of pH on a food preservative.

Chemical Equation: C6H5COONa + HCL ------ C6H5COOH + NaCl
Procedure:
This experiment was started with a clear solution of sodium benzoate and HCl was added to it, ultimately producing benzoic acid. First, .3395 g of sodium benzoate was weighed, then it was dissolved in water, causing it to disassociate into ions. Next, 3M of HCl were added drop wise to the solution until it reached a pH of 2, thus introducing the hydronium ion. This addition caused a white, solid benzoic acid to precipitate out of the solution. A vacuum filtration system was used to separate the solid from the liquid. What was once water soluable became insoluable.
Calculations:
Theoretical yield and Percent yield 0.3995 g of sodium benzoate x 144.1 g/mol sodium benzoate= 0.0028 mole of sodium benzoate = 0.0028 mole benzoic acid 0.0028 mole sodium benzoate x 122.1g/mole benzoic acid = 0.34 g benzoic acid (theoretical yield) % yield = (0.45g benzoic acid /0.34g benzoic acid) x 100 = 132.352%
Results:
A clear solution became a precipitate when HCl was added. What was once water soluable became insoluable. Sodium benzoate was converted into benzoic acid. The Theoretical yield of benzoic acid was found to be .34 g and the percent yield was 132.352%.
Conclusion:
To study the affect of pH on a food preservative. Sodium benzoate changed into benzoic acid once the 3 M of HCl was added making it a pH of 2, making the solution acidic. The hydronium ion concentration was high enough that it gave a yield of benzoic acid, which, is very insoluble in water and it formed a precipitate in the solution. The end percent yield was 132.352%, this was due to a few flaws in the experiment. During the filtration process of the experiment the funnel was not working properly and not all the

You May Also Find These Documents Helpful

  • Better Essays

    orgo lab

    • 993 Words
    • 4 Pages

    The results of the experiment show a percent yield of 34.34% for the first trial (Part A), and a percent yield of 84.0% for the second trial (Part B). The methods for both trials were generally the same, so the large difference is attributed to the fact that the beaker broke before the gravity-filtering step in the first trial. The beaker was attempted to be picked up by the beaker tongs, but as the hot solution was being poured into the filter, the beaker slipped out of the beaker tongs and shattered, leaving some of the product unfiltered and thus not accounted for in the final product. Although the methods were generally similar in both steps, the gravity filtration step was skipped over in the second trial, which may have accounted for the missing 16% in trial 2, but may have also accounted for the overall relatively high percent yield for this trial. Luckily, the actual melting point of benzoic acid fit within the recorded average…

    • 993 Words
    • 4 Pages
    Better Essays
  • Good Essays

    Hydrocinnamic acid underwent bromination using N-bromosuccinimide and AIBN. As one lab partner set up the reflux apparatus, the other measured the chemicals used in the lab experiment. 2.10 g of hydrocinnamic acid was used. It was observed as white and had a slight cinnamon smell. The amount of NBS was 2.49g and was measured in the fume hood. AIBN was measured at .030 g. 10 mL of acetic acid was also obtained. The reflux apparatus consisted of a 25 mL flask with a stir bar in a water bath. The chemicals were added in the following order: hydrocinnamic acid, NBS, AIBN, and acetic acid. After they were added, the temperature was turned up to come to a constant temperature around 80 C. A condenser was placed on top of the flask so if any evaporated…

    • 449 Words
    • 2 Pages
    Good Essays
  • Satisfactory Essays

    Organic Lab 2583-4

    • 503 Words
    • 3 Pages

    In another reaction tube, I dissolved 0.080mg of benzoic acid in the minimum volume of hot methanol; I added drops of water to the hot solution.…

    • 503 Words
    • 3 Pages
    Satisfactory Essays
  • Satisfactory Essays

    The benzoic acid may not have fully dissolved and been counted in as sand particles…

    • 288 Words
    • 2 Pages
    Satisfactory Essays
  • Good Essays

    The purpose of this experiment was to investigate a competitor’s claim that the food preservative, sodium benzoate (C6H5COONa), made by Fresh Foods International (FFI), changed into a new substance in stomach acid. Stomach acid has a pH between 1 and 3 due to the hydrochloric acid content. Based on the net equation given in the book as well as the solubility of the product our hypothesis is that a new substance will form.…

    • 683 Words
    • 3 Pages
    Good Essays
  • Good Essays

    benzoate was added, the cold nitric acid/sulfuric acid mixture was added to the conical vial…

    • 768 Words
    • 3 Pages
    Good Essays
  • Satisfactory Essays

    4) The benzoic acid formed crystals after the cooling bath and was obtained through filtration…

    • 522 Words
    • 3 Pages
    Satisfactory Essays
  • Better Essays

    Lab 2

    • 931 Words
    • 4 Pages

    The purpose of this lab was to produce benzoic acid by mixing sodium benzoate with hydrochloric acid. The Hydrochloric acid used in the experiment was a stock solution made by mixing HCl Acid and deionized water. HCl acid, historically called, muriatic acid or spirits of salt, hydrochloric acid is produced from sulfuric acid and common salt, NaCl (Princeton.edu). Since the early 1900 's, sodium benzoate has been used as a food preservative (SolarNavigator). It is utilized in a wide range of preservative applications due to its antimicrobial action combined with its low toxicity and low taste (SolarNavigator).…

    • 931 Words
    • 4 Pages
    Better Essays
  • Better Essays

    Chem Lab

    • 858 Words
    • 4 Pages

    There are millions of different organic compounds. Most of them are found in mixtures and in order to achieve a pure form they need to be separated, isolated, and purified. However, there are endless numbers of possible mixtures, which make it impossible to have a pre-designed procedure for every mixture. So chemists often have to make their own procedures. The purpose of this experiment was to prepare the student to the real world by them designing their own procedure which will help them understand the techniques of separation and purification better. The goal was to extract two of the components of the mixture that consisted of 50% benzoic acid, 40% benzoin, and 10% dibromobenzene. The benzoic acid was extracted by the use of base and extraction technique. Then a crystallization was performed in order to separate benzoin by the use of hexane a solvent, leaving the dibromobenzne in the mother liquor. The percent recovery for benzoic acid was 91.8% and 80.3% for the benzoin. The MP for benzoic acid was 119-122°C (1) and 135-136°C (2)for the benzoin. The high percent recovery and closeness of measured MP to the literature value indicate that the designed procedure was successful.…

    • 858 Words
    • 4 Pages
    Better Essays
  • Powerful Essays

    The purpose of the current experiment was to determine the pH of various hydrochloric acid and acetic acid solutions, to determine the pH of various salt solutions, to prepare a buffer solution, and determine the effects of adding a strong acid and strong base to the buffer solution versus adding a strong acid and strong base to water. The measured pHs for the hydrochloric acid solutions were 1.6, 2.2, 2.9, and 3.8. The measured pHs for the acetic acid solutions were 2.9, 3.9, 4.2, and 4.4. The pHs measured for the salts were 4.3 for sodium chloride, 7.3 for sodium acetate, 8.9 for sodium bicarbonate, 10.8 for sodium carbonate, 7.9 for ammonium chloride, and 6.9 for ammonium acetate. The pH for the buffer solution and the strong acid was 3.9 and the pH for the buffer solution and the strong base was 11.6. The pH of water with the strong acid added was 3.44 and the pH of water with the strong base added was 13.4…

    • 1669 Words
    • 6 Pages
    Powerful Essays
  • Good Essays

    Sodium Chloride Lab

    • 739 Words
    • 3 Pages

    In the experiment, we tested a sodium chloride solution. Along with the tested solution, control groups (water and sodium phosphate) were used to be help understand whether or not NaCl was a buffer. Water was the negative control group and sodium phosphate was the positive control group. If NaCl was a buffer than the pH would be stabled as the sodium phosphate buffer. If NaCl was not a buffer than the pH would fluctuate like the negative control, water. During the first trial and prior to the drops of 0.5 M of HCl acid, the pH of sodium chloride was 7.50. After the addition of 5 drops of 0.5 M of HCl, the pH decreased by 4.83 and ended at 2.67 on the pH scale. When comparing the results of the sodium chloride to the control groups, the total pH change of sodium phosphate was only…

    • 739 Words
    • 3 Pages
    Good Essays
  • Better Essays

    Therefore, the experiment was performed to conduct quality control analysis on two commercial products to determine the amount of acid or base active in these two products and then compare the results to those of the manufacture. This was done through the preparation of standardized acid solution and standardized base solution, and through titration. The purpose of titration was to determine the concentration levels of the commercial products being used.…

    • 1661 Words
    • 7 Pages
    Better Essays
  • Good Essays

    The primary focus of experiment 4 was to teach a student the basic solubility rules of salts in aqueous solutions. After developing and using a scheme for the qualitative analysis of three cations in an aqueous mixture, a student would use a centrifuge to identify, precipitate, and separate the three ions in the mixture. After becoming familiar with all three cations, the student would use the scheme again to identify at least two of the cations in an unknown solution. In order to begin the separation process, HCl is added to the mixture of cations to form the precipitates and separate the chlorides of Ag+, Pb2+, and HG22+. It is important not to add too much HCl because an excess would form the soluble complexes of AgCl and PbCl2. After the HCl is added, it is centrifuged to form a solid precipitate that contains all three cations and separate them from the supernatant liquid. Finally, another drop of HCl is added to test for completeness of precipitation and centrifuged again if the solution remains incomplete.…

    • 484 Words
    • 2 Pages
    Good Essays
  • Good Essays

    The benzoic Acid was dissolved in a very small amount of hot ethanol once dissolved water was added drop wise using a disposable pipet until it got cloudy. Once it reached this point the substance was removed from the steam bed and let cool down at room temperature. It is important to let this cool down slowly so impurities don’t get trapped in between the crystals. After 20 minutes the crystals were filtered out using a vacuum filter method. The crystals were carefully removed from the filter paper and weighted. These crystals were dried out for a period of 2 weeks, to later get a melting point. The MSDS value was compared with the experimental value to verify purity of the crystals…

    • 584 Words
    • 3 Pages
    Good Essays
  • Good Essays

    When the precipitate ion was added to ~1 mL of acetone there was a strong property of insolubility. Even when a stir rod was used to mix the precipitate in the acetone, the precipitate remained un-dissolved in the solvent.…

    • 971 Words
    • 4 Pages
    Good Essays