The result of the total plate count of Adlay vinegar fortified with iron in different concentrations was shown in Table 13. The analysis was performed using 1:100 dilution in triplicates and the data gathered substantially varies. The differences could be explained by the fermentation temperature‚ and other environmental conditions of the samples. Since the fermentation of the samples were done in uncontrolled environmental conditions. According to the study of Millet and Lonvaud-Funel (2000)‚ the
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details) (Date Abstract The aim of the lab was to separate and analyse analgesic drugs in a drug tablet. The method used to separate the components was Thin Layer Chromatography (TLC) with silica adsorbent as the stationary phase and 0.5% glacial acetic as the mobile phase. In one plate‚ five known samples were used as the reference‚ that is: Aspirin; Caffeine; Ibuprofen; and Salicylamide. Aspirin and Salicylamide were the only samples that fluoresced. On a second plate‚ the tablet sample was developed
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Preparing Esters by esterification method using carboxylic acid to an alcohol‚ which is 1.0 ml of ethanoic acid to the ethanol‚ and ethanoic acid to the propan-1-ol‚ also adding H2SO4 as a catalyst for the reaction Abstract: Esters are a group of organic compound‚ famous for their interesting odours and smells. In this investigation student used ethanoic acid and ethanol with sulfuric acid as catalyst to produce ester‚ which was known of its smell. However it was expected to have a pleasant smell
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experiment and shows the possible identities for the product. II. Key experimental details‚ observations‚ and results: Table 1: Exactly how much of each reagent was used Reagent | Amount added to flask | (E)-stilbene | .201g | Glacial Acetic Acid | 4.1mL | Pyridinium Tribromide | .391g | A. Observations: 1. The 10mL round-bottom flask weighed 17.690g. 2. The flask was heated and stirred at ~95 C until the (E)-stilbene dissolved. 3. 4mL of cold Deionized water was run
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Experiment 1: TLC Analysis of Analgesic Drugs 1/23/2011 Purpose: The goal of this experiment is to test our knowledge and understanding of TLC analysis by having us do a TLC analysis of analgesics to figure out their main chemical components. Calculations: 1.) Rf = Distance spot traveled/ distance solvent traveled Results: Table 1: TLC Analysis Analgesic Drugs | Rf Value | Acetaminophen | 0.323 | Aspirin | 0.597 | Caffeine | 0.081 | Unknown 154 (Plate 1) | 0.081‚ 0.306‚ 0.597
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Assignments in Science Class X (Term II) 4 Carbon and its Compounds IMPORTANT NOTES 9. Unsaturated organic compounds : Organic compounds in which a double or a triple bond exists between two carbon atoms in a carbon chain‚ are called unsaturated organic compounds. 10. Hydrocarbons : Organic compounds which contain only carbon and hydrogen atoms are called hydrocarbons. 11. Straight chain hydrocarbons : Hydrocarbons‚ in which all the carbon atoms are linked to one another in a straight chain
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Synthesis of p-Toulichydrazone and Resacetophenone Schiff base (RAPPTH): p-Toluic hydrazide (1.5018g) and Resacetophenone (2‚4Dihydroxyacetophenone)(1.5215g) were dissolved in methanol and Refluxed in the presence of few drops of acetic acid for 7 hours on water bath with constant stirring. The resultant mixture was transferred in a china dish and allowed to cool naturally. Light brown crystals were obtained. The compound was recrystalized from water. The % of yield was 80% and
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5. Melting point determination. Crude Aspirin Recrystallized Aspirin Melting point 118-130°C 134-136°C Literature value 135°C 135°C Table 6. Differentiation of starting materials. Substance Sol’y in water +/- Fecl3 test +/- KMnO4 +/- Acetic Chloride Dissolved acetyl chloride. Clear colorless liquid. + Boils upon addition of acetyl chloride. Cloudy yellow solution. --
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Viktoria R. Beltran RELATIVE RATES OF ELECTROPHILIC AROMATIC SUBSTITUTION I. Objective(s) In this Experiment‚ the relative reactivities of different substituted benzenes towards bromination will be determined‚ where bromine is dissolved in acetic acid. Materials and apparatus Test solutions: 0.2 M solutions in ethyl acetate: Benzene‚ chlorobenzene‚ phenol‚ nitrophenol‚ aniline and acetanilide. Measuring pipettes (5 mL) micro test tubes 0.05 M Br2 in 90% CH3COOH Pasteur
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Lab Report: Stoichiometry Lab Oct. 27‚ 2011 Claire Elizabeth Lab Partners: Hannah Signature:___________________ Introduction- Baking soda and vinegar are two common materials found in almost every household. That‚ plus the fact that all the starting and finishing materials are non hazardous and safe‚ is why this is one of the first chemical reactions that many people are exposed to The purpose of this experiment tests which of the two reactants (vinegar and baking soda) is the limited
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