quantity of solid dissolved in solution. It may also be used to calculate the molar mass of an unknown acid or base. Purpose: I. Prepare a standard solution of sodium hydroxide II. Standardize a sodium hydroxide solution by using potassium hydrogen phthalate (KHP) III. When given whether the acid is monoprotic‚ diprotic‚ or triprotic ‚ determine the molar mass of the unknown organic acid. IV. Calculate the Molarity of the Soft drink. Materials: * 50 mL Buret * Beaker
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Introduction Extraction is a purification technique used in organic chemistry to separate compounds from a mixture of two or more compounds. There are three different extraction techniques: liquid-liquid extraction‚ solid-liquid extraction and chemically active extraction. All three types of extraction follow the same principle. Organic molecules dissolve in organic solvents and polar molecules dissolve in aqueous solvents. This phenomenon is observed because of the intermolecular forces between
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Separation of a Carboxylic Acid from a Neutral Compound by Extraction Reference: Smith‚ Chapter 2 (Acids and Bases) Introduction Carboxylic acids and phenols are two families of organic compounds that contain carbon‚ hydrogen and oxygen‚ and also react with water to yield an excess of hydronium ions over hydroxide ions. Pure water has a pH of 7‚ which means it has a hydronium ion concentration‚ [H3O+] of 10-7 M (M = molarity‚ moles/Liter). The hydronium ions in pure water come from the self-ionization
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solution of an acidic and organic compound and purify its respective acidic product through the techniques of an acid base extraction‚ recrystallization‚ and use of Melt Temp (melting point range). The reaction of an unknown acid (3-chlorobenzoic acid) with diethyl and sodium hydroxide was observed‚ and the solution naturally separated into an aqueous and organic solution. The mixture of acid and organic solution was created and then separated through the Hirsch funnel into separate beakers of an aqueous
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Mabel M. Kimble September 21‚ 2014 Chemistry 234 Recrystallization of Benzoic Acid ABSTRACT The recrystallization of Benzoic Acid was performed to fully master the ability to purify a solid compound. This form of purification technique is especially important in chemical identification‚ where the melting point of the compound is taken to confirm its purity. In order to perform recrystallization a solubility test much be completed. Four solvents (95% Ethanol‚ Petroleum Ether‚ Acetone and distilled
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BUFFERS By: Luis P. Bazan‚ RPh.‚ Ph.D. A buffer solution is a solution of: 1. A weak acid or a weak base and 2. The salt of the weak acid or weak base Both must be present! A buffer solution has the ability to resist changes in pH upon the addition of small amounts of either acid or base. Consider an equal molar mixture of CH3COOH and CH3COONa CH3COOH (aq) H+ (aq) + CH3COO- (aq) Adding more acid creates a shift left IF enough acetate ions are present 16.3 Which of the following
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REPORT EXPERIMENT 9 CARBOXYLIC ACID AND DERIVATIVES Date: January 19‚ 2004 Objectives: 1. To understand the reactions of carboxylic compounds and derivatives. 2. To know the methods for preparing carboxylic acid derivatives. 3. To know the methods for testing the carboxylic acid derivatives. Experimental Procedures: 9.1 Solubility 1. Prepare 3 test tubes with 3 ml of water in each. 2. Place 3 drops of acetic acid‚ benzoic acid‚ and oxalic acid in separate test tubes. 3. Shake and observe
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Titration Lab How Much Citric Acid is in Your Soda? PURPOSE To determine the molarity (concentration) of citric acid (H3C6H5O7) in various different citrus flavored sodas. BACKGROUND PRINCIPLES Popular sodas all strive for a somewhat sour (’tart’) flavor and manufacturers utilize acids to impart this taste. While there are a vast variety of different brands of sodas on the market‚ they can be broken into two main categories: dark or clear. This differentiation is not only a simple color
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Crystallization of Benzoic Acid Purpose: The purpose of this experiment is to purify benzoic acid by crystallization. Procedure: 1. 0.5g impure benzoic acid was placed in a 50mL Erlenmeyer flask. 15mL of water was added and the mixture was heated to a boil on a hot plate. 0.5mL of water was added to the flask‚ while swirling the flask. The mixture was boiled until the benzoic acid completely dissolved. The total volume of water used was recorded. The black solid that remain in the dissolved
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Name: Citric acid Chemical Name: 2-hydroxypropane-1‚2‚3-tricarboxylic acid Chemical Formula: C6H8O7 Chemical Structure: pH: 4.18‚ 3.90‚ 3.57 Classification: Weak acid Uses: It is a natural preservative/conservative and is also used to add an acidic or sour taste to foods and drinks. It is also used mainly as an acidifier‚ as a flavoring‚ and as a chelating agent. Name: Vinegar acid Chemical Name: Acetic acid or ethanoic acid Chemical Formula: C2H4O2 Chemical Structure:
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