Amanda Jornd Experiment 7- Synthesis and Reactivity of tert-Butyl Chloride Via an SN1 Reaction Introduction/Background: Alkyl halides are compounds in which a halogen atom replaces a hydrogen atom of an alkane. Alkyl halides are classified as primary‚ secondary or tertiary depending on the number of alkyl substituents directly attached to the carbon attached to the halogen atom. The purpose of this lab was to properly prepare t-butyl chloride from t-butyl-alcohol in a concentrated hydrochloric
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counters. Our toaster competes for space with a collection of funnels made from 2-liter plastic beverage bottles and rubber stoppers (1). Baking soda from my shelf joins citric acid from a natural foods shopping trip‚ to be molded into bath bubblers using plastic eggs left over from Easter (2). My young children view this as normal. They like to help with mom’s “chemistry experiments”‚ as I refer to them. They pour water into the funnels. They try out the bath bubblers in their evening bath. They are
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An experiment was run to determine which enzyme (pectinase‚ and cellulase or combinations of the two enzymes) maximizes juice production and would be most cost effective. The proposed hypothesis was if the enzyme‚ pectinase‚ is added to apple juice‚ then the more juice will be extracted than if cellulase were added because pectinase holds the cell wall together and if it is separated apart from each other‚ then the more juice would be able to flow out. The experimental data show that during the ten
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Apparatus: Safety spectacles Weighing bottle Balance capable of weighing to within 0.01g Spatula Stirring rod with rubber end Dropping pipette Wash bottle of distilled water Funnel Volumetric flask‚ 250 cm3 Beaker‚ 250 cm3 Retort stand Burette clamp Burette‚ 50cm3 Pipette‚ 25cm3 Pipette filler Beaker‚ 100cm3 White tile Conical flask‚ 250cm3 Reagents used: Distilled Water Hydrated Sodium Borate 1.0 M Hydrochloric acid Screened methyl orange Sodium Borate solution
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test tubes‚ 4.0 mL of 5.0% NaHCO3‚ micropipette (glass with rubber suction top)‚ a stirring rod‚ and a vial. A 50 mL beaker‚ 2 x 1.0 mL of 6.0 M HCl‚ pH paper‚ a vacuum chamber‚ a test tube rack‚ scooper‚ ice bath‚ hot water bath‚ hot plate‚ Hirsche funnel‚ and a rubber tube are all necessary to perform the
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the listed tablet ingredients. This time we used a 150mL beaker‚ analytical balance‚ forceps‚ a 50mL graduated cylinder‚ a glass rod‚ beaker tongs‚ a hot plate‚ two 16 x 125-mm test tubes‚ centrifuge‚ a medicine dropper‚ a filter paper‚ a filter funnel‚ a 250-mL Erlenmeyer flask‚ a watch glass‚ a drying oven‚ a spatula and a red litmus paper. The chemicals we need were 20mL of 2.0M HCl‚ a calcium-enriched tablet and 25mL of 1.0M Na2CO3 solution.
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experiment. Make sure to thoroughly wash the instruments used and put them in the correct place after use. Procedure: 1) Put on safety goggles 2) Gather all the materials necessary to perform this experiment 3) Measure 5 mL of the system using the funnel into the graduated cylinder (25mL) 4) Pour the 5mL into the 40mL vile 5) Shake the content in the vile for 30 seconds 6) Record the time it takes for the system to turn from blue to colorless 7) Repeat steps 4‚5‚6‚7 with the following measurements:
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acetate. By using Fischer reaction‚ Isoamyl acetate was produced by refluxing isoamyl alchol and acetic anhydride with the presence of sulfuric acid for 30 minutes. After cooling the mixture‚ cold water was added and it was transferred in a separatory funnel. It was then extracted with immiscible saturated sodium bicarbonate to hasten separation. The sodium bicarbonate layer was discarded and the organic layer was again extracted with sodium chloride to remove the acid. The sodium chloride layer was discarded
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purify acetanilide by crystallization method from water c) Purity check by melting range Equipment / Materials and Hazars: hot plate beakers(150‚250mL) ice stirring rod spatula Büchner funnel aniline weighing paper digital scales rubber tubing (hose) acetic anhydride filter paper Mel-temp apparatus
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Extraction of Caffeine from Tea Leaves Marc Tugaoen‚ Kristine Vanzuela‚ Rafael Villanueva‚ Justeen Wong Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines Abstract This experiment has been divided into 4 set-ups‚ first was the solid-liquid extraction‚ next was the liquid-liquid extraction‚ then the sublimation and last was the melting point determination. The solid-liquid and liquid-liquid extraction were both done during the first meeting‚ the DCM layer was filtered and
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