"Calibration of volumetric glassware pipet buret" Essays and Research Papers

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    boils around 95ºC at 6600ft. Ice also has a significant effect on the temperature of water from the tap. Ice dropped the temperature about 15ºC. Volumetric measurements were the basis of the 3rd part of the experiment. It was displayed during this experiment that a pipet holds about 4mL and that there are approximately 27 drops/mL from a short stem pipet. Part 4 introduced the student to measuring mass using an electronic scale. Step 5 was about density measurements. If you have an objects mass and

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    volume of 6.00 M NaoH that is needed to prepare 250mL of an approximately 0.100 M NaOH solution. Transfer the calculated volume of the 6.00 M NaOH solution to a volumetric flask using a graduated cylinder. Obtain a 25mL buret‚ and rinse and fill it with the prepared base solution. Make sure there are no air bubbles trap within the buret. Calculate the amount of KHP required to reach equivalence point. Using a 125mL Erlenmeyer flask‚ place it on a balance‚ and add KHP to it until the balance reads

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    Determination of Pka

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    the PH changes very quickly. With the results‚ a titration curve should be produced. Experimental Section Materials and Methods: A buret with NaOH solution was used to ensure an accurate measure of NaOH could be taken. A PH recording machine was used to measure the PH. To make sure 25.0 ml of the unknown was measured‚ we used a 25.0 ml pipet. The buret was primed and filled with NaOH. The measured 25.0 ml of the unknown solution was placed into a beaker and the PH was measured. At this point

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    Abstract The purpose of this experiment was to determine the enthalpy of formation of magnesium carbonate in a lab setting. This was done using a calorimeter‚ which was calibrated by adding a known amount of both hot and cold water. Following the calibration of the calorimeter‚ HCl was placed into the empty calorimeter and then mixed with magnesium and then MgCO3 and the temperature changes were recorded. The heat lost by the hot water is thus equal to the heat gained by the calorimeter. Experimentally

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    Lab Techniques

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    and dissolved in 25 ml of deionized water. This solution was then quantitatively transferred to a 250ml volumetric flask. Proper technique is needed for quantitative analysis. This transfer was done to ensure that there was no detectable KCl left in the beaker. After transferring the solution add 3 drops of AgNO3 to the rinsed beaked to check the completeness of the transfer. Now take the volumetric flask and add deionized water till it is 6mm away from the etched mark on the neck of the flask. Place

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    1. Beakers (5ml markings) 2. 10ml graduated cylinder (0.1 markings) 3. 5ml vials (0.1 and 0.3 markings) 4. 1ml plastic pipets (0.1 ml markings) 5. 1ml syringes (0.1 ml markings) 6. 1ml graduated volumetric pipets (0.01 ml markings) B. A 1ml graduated volumetric pipet is the best to use if you want 0.15 ml of reactant C. 1ml plastic pipets (used 2 times) are best to use when you want 2 ml of solvent Safety Hazards: 1. Methanol is flammable and toxic. Don’t breathe

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    Determination of An Unknown Amino Acid From Titration Abstract Experiment 11 used a titration curve to determine the identity of an unknown amino acid. The initial pH of the solution was 1.96‚ and the pKa’s found experimentally were 2.0‚ 4.0‚ and 9.85. The accepted pKa values were found to be 2.10‚ 4.07‚ and 9.47. The molecular weight was calculated to be 176.3 while the accepted value was found to be 183.5. The identity of the unknown amino acid was established to be glutamic acid‚

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    Calibration:- A calibration curve is a mathematical tool used in analytical chemistry that provides a set of reference points that unknown chemical substances can be compared to. When analyzing certain substances‚ scientists are often unable to get a completely accurate understanding of the substance’s makeup. With a calibration curve‚ chemists can compare known information about unknown substances to make estimates

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    Titration of vitamin c

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    Determination of Vitamin C by an Iodometric Titration Purpose: The goal of this lab is to determine the concentration of vitamin C in juices and Real Lemon. A redox titration‚ involving an iodometric method‚ will be used to do the analysis. The samples will be classified by their Vitamin C content. Introduction: Although most mammals can synthesize vitamin C‚ or ascorbic acid (C6H8O6)‚ from sugars‚ man must ingest considerable quantities of this substance. The National Academy of Sciences recommends

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    cm3 – 14.7 cm3 = 235.3 cm3 1) Measure 14.7 cm3 of H¬2O2 using a 20 cm3 graduated pipette (with a pipette filler) and transfer to a 250 cm3 volumetric flask. 2) Rinse the pipette filler with distilled water and pour the washings into the volumetric flask. 3) To dilute the solution fill the flask with distilled water until it is 5mm below the calibration line. 4) Use a dropping to add the final quantity of distilled water until the bottom of the meniscus is level with the 250 cm3 mark. 5) Stopper

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