Experiment 1: Study of Solubility Equilibrium Data Treatment and Analysis Section 1: Solubility Product Constant Temperature (˚C) | Volume of NaOH used (mL) | | | | Titration 1 | Titration 2 | Average | 28 | 12.7 | 12.8 | 12.75 | 9 | 10.5 | 10.5 | 10.5 | 19 | 11.3 | 11.2 | 11.25 | 40 | 16.2 | 16.2 | 16.2 | 50 | 22.8 | 22.9 | 22.85 | Table 1: The volume of NaOH used in the titration at various temperatures. No. of moles of KHC4H4O6 = 1.45 g ÷ 188.177g/mol = 7.71 x 10-3mol
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082 g/mL | Irritant (eyes/skin). Toxic by inhilation‚ Flammable (fp 49 ºC). | Discussion: Recrystallization is a widely-used technique to purify a solid mixture. The desired product is isolated from its impurities by differences in solubility. Insoluble impurities and colored impurities can be removed from hot solvent through the use of activated carbon and filtration. Soluble impurities remain in the cold solvent after recrystallization. The desired product should be as soluble as
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Charles Michael Te Herrera Date Performed: November 18‚ 2010 2009 – 14077 Ma’am Rea Abuan Experiment # 1 SOLUBILITY OF ORGANIC COMPOUNDS State what types of intermolecular forces are present in solutions formed due to intermolecular attractions between the solute and the solvent. Compound 1 Compound 2 Intermolecular Forces Class S (Water-soluble) Compounds Acetone Water Hydrogen Bonding & London Dispersion Forces Diethyl Ether Dipole – Induced
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Experiment 1: Solubility of Organic Compounds (Answers to Questions) Q1. State what types of inetmolecular forces are present in solutions formed due to intermolecular attractions between the solute and the solvent. A1. For Water-Soluble Compounds: Acetone – Water: Hydrogen bonding and van der Waals forces Acetone – Diethyl Ether: Dipole – (induced) dipole and van der Waals forces Sucrose – Water: Hydrogen bonding and van der Waals forces Ethyl alcohol – Water: Hydrogen bonding
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In part 1 the results of the solubility do not agree with the with rules of solubility most likely because we put too much solid in the test tubes and not enough water to dissolve it. They should have dissolved because the anything with nitrate should be soluble. With the pH‚ when the mixture where compared with the chart all of them except NaCl where a shade of blue which means that they have a pH of 8-14‚ depending on the darkness of the shade‚ meaning that they are a basic solution. When reacting
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The solubility of calcium hydroxide Aim: to find out the solubility of a substance that only partially dissolves in water. Method: place about 100cm3 of distilled water in a flask and add about one spatula of solid calcium hydroxide. Stopper the flask and shake well for one minute. Leave to stand for at least 24 hours. Titrate 10cm3 samples against 0.05 mol dm-3 hydrochloric acid solution using methyl orange as an indicator. Obtain enough results to calculate an accurate average‚ and then
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Solubility of CO2 in water Aim: To decarbonate a bottle of soft drink and find out the amount of CO2 in the drink. * Principle: The reaction between carbon dioxide and water is an example of an equilibrium reaction: Materials: * * 3 soft drink bottles (300ml) * 6g of salt (NaCl) * Triple beam balance scale * Thermometer * Digital scale * Watch glass * Electric hotplate Method: Standing up method 1. An unopened bottle of carbonated drink
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The primary focus of experiment 4 was to teach a student the basic solubility rules of salts in aqueous solutions. After developing and using a scheme for the qualitative analysis of three cations in an aqueous mixture‚ a student would use a centrifuge to identify‚ precipitate‚ and separate the three ions in the mixture. After becoming familiar with all three cations‚ the student would use the scheme again to identify at least two of the cations in an unknown solution. In order to begin the separation
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FACTORS AFFECTING SOLUBILITY There are three main factors that control solubility of a solute. (1) Temperature (2) Nature of solute or solvent (3) Pressure EFFECT OF TEMPERATURE Generally in many cases solubility increases with the rise in temperature and decreases with the fall of temperature but it is not necessary in all cases. However we must follow two behaviours: In endothermic process‚ solubility increases with the increase in temperature and vice versa. For
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concentrations of a miscible liquid (ethanol) on the solubility of KNO3 in water. The results of the investigation support the hypothesis that water‚ which exhibits greater polarity‚ is able to dissolve a greater mass of KNO3 at lower temperatures compared to tested concentrations of Ethanol ranging from 12.5% to 30%. Furthermore‚ the results of the graph 1 show correspondence to the dielectric constant of each solvent as both the starting solubility of the solubility curves and the dielectric constant of the
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