Microscale Crystallization of Sulfanilamide Purpose The purpose of the experiment was to use the crystallization technique to purify the solute sulfanilamide using 95% ethanol as the solvent‚ to calculate the amount of sulfanilamide that was recovered‚ and to determine the purity of the final product. Introduction In this experiment‚ recrystallization will be the method used to purify the solute sulfanilamide using ethanol as the solvent. Based on the solubility curve on the solubility
Premium Solubility Temperature Solid
temperatures. "Most‚ but not all‚ substance are more soluble at higher temperatures". 1 Crystallization is a delicate procedure that involves the slow formation of a crystalline solid. Rapid formation of an amorphorous solid is called precipitation‚ which can contain many impurities. "The purest crystals are obtained when crystallization occurs slowly from an undisturbed solution".2 In general‚ crystallization is the easiest process to purify a solid substance to an acceptable quality for basic laboratory
Premium Chemistry Solid Crystal
The experiment is carried out to: 1.1 Conduct the synthesis of aspirin 1.2 Reinforce the skills of recrystallization 1.3 Reinforce the technique of melting point determination 2. Procedure: 2.1 Preparation of Aspirin 2.2 Recrystallization of Aspirin 2.3 1.4Melting Point Determination of Aspirin 3. Results: 3.1 Mass of dried‚ recrystallized aspirin: 1.62g 3.2 Percent yield: 51.75% yield 3.3 Temperature range: 138.2 – 140.0°C
Free Aspirin Acetic acid Acetic anhydride
order to evaluate this effectiveness‚ the yield and purity of only the ice product is investigated before and after a number of wash cycles. A 1000g solution of 5 wt% CuSO4 underwent crystallization for one hour with the use of ice crystal seeding and the agitation of a stirrer at 500rpm. After the crystallization process‚ the mass of the ice product and filtrate were recorded. The ice product was then washed with de-ionised water under Buchner vacuum filtration‚ before the masses were recorded
Premium Water Crystal Concentration
Experiment 2&3 Recrystallization and Melting Points Determinantion of Benzoic Acid Abstract In experiment 2‚ recrystallization was used to purify the crude benzoic acid extracted from a mixture during experiment 1. Then a percent recovery for this recrystallization process was calculated. In experiment 3‚ the melting point ranges of the crude and purified benzoic acid were both determined by using Melt Temp Apparatus. Introduction Recrystallization is a purification technique for non-volatile
Premium Chemistry Liquid Water
Microscale Crystallization – Craig Tube For this experiment‚ we had to find the percent recovery and melting point of pure sulfanilamide from impure sulfanilamide using the crystallization technique. To start‚ .1004 grams of impure sulfanilamide was put into a Craig tube with enough ethyl alcohol to barely pass the top of the sulfanilamide. The Craig tube was put into a stone block until boil‚ then check to see if the solid material had dissolve. With the addition of two more drops from a supply
Premium Solubility Ethanol Crystal
mixture and is cooled in a solution.In this experiment‚ acetanilide‚ the crude product of acetylation of aniline and acetic anhydride‚ was used as the pure organic compound. Crude acetanilide underwent crystallization process using the preferred recrystallizing solvent‚ water. The crystallization process was when crude acetanilide was placed in hot water bath and was cooled after in an ice bath which would then yield to the formation of crystals of pure acetanilide. The percentage yield form the
Premium Solvent Solubility Oxygen
is done by observing the melting point. This is important because if there is an impure substance the melting point would be depression and the melting range would be broader. By finding the melting point of a known substance one can then observe an unknown substance’s melting point to see if the points are the same and try to figure out the unknown. Experimental Section: The first known substance we used was Biphenyl. 68 degrees Celsius is the known melting point. We used the capillary method
Premium
Summary Purpose To purify the component (unknown) of Pancetin from last experiment and then compare its melt point to the two other possible substances. Theory Panacetin should be made up of about 50 percent of the unknown component that we previously separated out of Panacetin for testing. We suspect that this unknown compound is either acetanilide or phenacetin. From the solubility of acetaminophen and phenacetin‚ we could know both of them are relatively soluble in boiling water but insoluble
Premium Solubility Chemical substance Temperature
Aim: To determine the water of crystallization in washing soda crystals (Na2CO3.xH2O) Research Question: What is the percentage composition and the amount (in moles) of water in the given ionic hydrate? (Na2CO3.xH2O) Background Information: Sodium Carbonate also known as Washing Soda (Na2CO3.xH2O) is a sodium salt of carbonic acid. Sodium carbonate is domestically well known for its everyday use as a water softener. It is also used to remove grease‚ oil and wine stains. It can be extracted from
Premium Hydrochloric acid Sodium carbonate Sodium chloride