CHM 3120L ANALYTICAL CHEMISTRY I LABORATORY REPORT EXPERIMENT: SPECTROPHOTOMETRIC DETERMINATION OF IRON IN DRINKING WATER Name: Steven Adrien Section: 3 Date Experiment Completed: Wednesday‚ July 17‚ 2013 1. Complete the following table Fe(II) stock solution | mass‚ g | 0.1756 | volume‚ mL | 500.0 | MW(Fe(NH4)2(SO4)2 x 6H2O)‚ g/mol | 392.14 | AW(Fe)‚ g/mol | 55.85 | conc. Fe(II)‚ ppm | 50.0 | Use Equation Editor to show how you calculated the concentration of Fe(II)
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changes in temperature. The changes in temperature were to be used to find the amount of heat released or absorbed. EXPERIMENTAL Reference """""""""""your website with your information""""""" RESULTS Calculation Calculation for determination of q: q = ms∆T Hess’s Law-type calculation ΔH = ΔHproducts – ΔHreactants J = g x [ J / ( g x ° C ) ] x ° C Calculation for Heat Change q=60g(160g*4.4c) =(60g*4.18J)/4.4j =1104.56 Joules CLASS TABLE part I
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and Potentiometric Determination of its Purity and Dissociation Constant ------------------------------------------------- Abstract The purpose of the study is to synthesize salicylic acid from the ester‚ methyl salicylate‚ and determine the acid’s dissociation constant and purity. The ester was converted to salicylic acid by base hydrolysis. The products were refluxed and recrystallized‚ to ensure maximum purity‚ and filtered‚ dried‚ and weighed. The melting point of the product was determined using
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Reviewer’s Name: Sanjeev Mishra UMN ID Number: 4585009 The Photoelectric Effect: A Determination of Planck’s constant Ian E. Jaeger School of Physics and Astronomy‚ University of Minnesota – Twin Cities 116 Church St. S.E.‚ Minneapolis‚ MN 55455 Abstract The photoelectric effect was explored to determine an experimental value of Planck’s constant‚ h. Included is a brief introduction to the history leading up to Einstein’s discovery of the photoelectric effect as well as the theory behind
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Experiment 19 - Determination of the equilibrium constant for the reaction Fe3+ (aq) + SCN( (aq) = FeSCN2+ (aq) Object: To determine the equilibrium constant by a colorimetric method Theory: Colorimetric methods of analysis are usually applied to the determination of small concentrations of either inorganic or organic materials in a solution. The constituent sought must be coloured or must be capable of reacting with a reagent to produce a substance having a suitable colour. Beers Law‚ which
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Emilia Monroe August 27‚ 2014 Experiment #01 The Determination of the Percent of Water in a Compound CHEM 1315-022 For experiment one‚ The Determination of the Percent of Water in a Compound‚ the sole purpose of conducting this experiment was to determine the percent of water found in compounds such as Magnesium Sulfate‚ Copper Sulfate‚ and so on. Along with determining the percentages of the hygroscopic compounds the experiment allowed for the exploration of separation of hydrogen bonds
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2.4.4. Direct determination of saliva proteins Protein contaminated with nucleic acids absorbed the light at wavelength 280 nm and it absorbs much strongly at wavelength 205 nm when it is free from nucleic acids. The UV-visible spectrophotometer was used in determination of saliva proteins (Figure 2.2). Cold trichloroacetic acid (10 % w/v ) was added to the sample‚ centrifuged for 10 minutes to precipitate protein. The absorbance of a known volume
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LAB REPORT Introduction: In a chemical change‚ the identities of substances change and new substances form. In an equation the substances on the left are the reactants. The substances on the right are the products. In this experiment the objectives are to observe evidence that a chemical change has taken place. Infer from observations that a new substance has been formed. Identify and record observations that show energy is involved in chemical change observe the color‚ solubility of some substances
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SPECTROPHOTOMETRIC DETERMINATION OF THE EQUILIBRIUM CONSTANT OF A REACTION Methodology The following stock solutions were prepared: 1.0 M HCl‚ 0.1 M HCl‚ 0.1 M KSCN‚ 0.002 M KSCN (in 0.1 M HCl)‚ 0.2 M FeCl3 (in 0.1 M HCl)‚ and 0.002 M FeCl3(in 0.1 M HCl). Using the prepared stock solutions‚ the standard (Table 1) and Unknown (Table 2) solutions were prepared. Table 2. Preparation of Standard Solutions 0.10 M KSCN 0.002 M FeCl3 0.1 M HCl Blank 2.0 ml 0.0 ml 8 ml S1 2.0 ml 0.1 ml 7
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Name SOLUBILITY CURVES Answer the following questions based on the solubility curve below. Which salt is least soluble in water .. at 2O° C? 2. How many grams of potassium chloride can be dissolved in 200 g of water at 80° C? IO 3. At 40° C‚ how much potassium _ __nitrate coin be dissoiu$tl ^n 30D.g of water? ------W- ’1 80 70 ...- O --60 0 5© 40 4. Which salt shows the least change 30 In solubility from 0° - 100° C? 20 10 At 30° C‚ 90 g of sodium
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