Experiment 8: Hydrogen Phosphate Buffer Systems Purpose The purpose of the lab was to create a buffer solution and observe the capacity of the phosphate buffer system. Also‚ the experiment was meant to provide experience with the calculations and mathematics involved in creating the buffer solution. Finally‚ the lab was designed to provide an insight and appreciation for the necessity and complexity of buffers in our physiology and in the environment. Procedure No deviations were made from
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The goals of this experiment are to determine if the products derived from amide synthesis and Williamson Ether Synthesis are identical‚ and if one of the synthetic routes is more advantageous than the other. In Part 1‚ an attempt to synthesize acteophenetidin crystals by amide synthesis was made. We began by removing the colored impurities from the p-Phenetidine (reddish-brown) by placing 2g of the sample in 38 mL of hydrochloric acid and heating the solution to boiling point. Upon reaching just
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Objective: The objective of this experiment is to use acid-base extraction techniques to separate a mixture of organic compounds based on acidity and/or basicity. After the three compounds are separated we will recover them into their salt forms and then purify them by recrystallization and identify them by their melting points. Procedure: Extraction of Carboxylic Acid A pre-weighed (0.315g) mixture of Carboxylic acid‚ a phenol‚ and neutral substance was placed into a reaction tube (tube 1)
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An Experiment to find the Concentration of a Sample of Acid Rain Plan Aim When a metal is extracted from its ore often sulphur dioxide is produced. When sulphur dioxide is dissolved in water it forms a strong acid called sulphuric acid. Sulphuric acid is often sold as a useful by-product‚ but also gets into the water cycle and forms acid rain. In this experiment‚ I have been given a sample acid rain of concentration between 0.05 mol dm-3 and 0.15 mol dm-3 and my aim is to find out exactly what
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Acid-Base Titration Using a pH Meter Bradley Holloway and Jennifer Parker Period 6 April 16‚ 2013 Introduction: In chemistry‚ the ability to find molarities of acidic and basic solutions is a convenient way to convert between moles of solute and the volumes of their solutions. Through the process of titration‚ the molarity of these acids and bases can be found to a high level of precision. To begin titration‚ one solution is added to a second solution slowly until a certain point
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Abstract The bromination of trans-cinnamic acid was completed to determine dibromide’s stereochemical structure and its mechanism. After the addition of bromine to trans-cinnamic acid‚ the product was identified by its melting point and infrared spectrum resulting in erythro-2‚3-Dibromo-3-phenylpropanoic acid after comparing similar properties. Introduction In this lab‚ the bromination of trans-cinnamic acid was completed to determine dibromide’s stereochemical structure‚ and from there determine
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Chemistry 521 Exam I‚ Spring Quarter 7:30 - 9:00 PM‚ 25 April 2000 NAME 1. [10 points] What are the concentrations of HSO− ‚ SO2− ‚ and H+ in a 0.20 M KHSO4 solution? (Hint: 4 4 H2 SO4 is a strong acid; Ka = 1.3 × 10−2 for HSO− .) 4 2. [15 points] Calculate the pH of 1.00 L of the buffer 1.00 M CH3 COONa/1.00 M CH3 COOH (pKa = 4.74) before and after the addition of (a) 0.080 moles NaOH and (b) 0.12 moles HCl. (Assume there is no change in volume). 3. [10 points] The following reaction
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Abstract A buffer is a solution that resists changes in pH when H+‚ OH-‚ or H20 is added. By using standard lab equipment‚ a lab pro diagnostic tool‚ and acidic and basic solutions‚ the pH can be found. By recording the pH while adding a base or an acid gradually to a buffer solution you can find the capacity of each buffer to resist drastic changes in pH. The best buffers will keep a solution from becoming either too acidic or basic with the addition of a strong base or acid. Introduction The
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The Equilibrium Constant of an Ester Hydrolysis Reaction Jesus Flores March 30th‚ 2015 Abstract: This experiment was conducted in order to discover the Kc‚ equilibrium constant‚ of a hydrolysis reaction of an unknown ester #2‚ unknown acid‚ and alcohol #2 products. The first week consisted of creating the reaction mixtures in bottles‚ next was preparing a NaOH solution while neutralizing with KHP. The final week consisted of titrating the bottles with the NaOH solution prepared previously
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Identifying Pb+2: 1) Took 2mL of my unknown solution and added 2 drops of HCl and got white ppt which correlates with the positive control. 2) Centrifuged the ppt and soln‚ then discarded soln and washed ppt and centrifuged again. 3) I added 2mL of H2O‚ put the test tube in the hot water bath and stirred for 3 minute with a stirring rod. 4) I then decanted the solution into another test tube. 5) I added one drop of 6M acetic acid and 3 drops of 1M K2CrO4‚ which formed a positive confirmation where
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