Intro In 1936 a scientist named Ruzika was the first ever to make a pure form of testosterone from cholesterol (steroid.com). It is then that steroids emerged as a performance enhancing drug. I am pretty sure we all have pre conceived ideas and notions about steroids and the people that use them. Today I would like to talk to you all about the fact and fiction of steroid usage. 1st I would like to talk about the History of steroids‚ 2nd the types of steroids‚ 3rd anabolic and androgenic affects
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separate vials‚ label and store. 13. Disassemble and clean the fractional distilling apparatus using hexane for the joints and acetone for the glassware. III. Observations O O O O Ethyl Acetate Butyl Acetate (boiling point ~ 78◦C) (boiling point ~ 120◦C) Initial temperature of fractional distillation apparatus:
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substitution happens when the initially formed intermediate expels one of the substitutes originally bonded to the carbonyl carbon leading to the formation of a new carbonyl compound. In this experiment‚ the specific nucleophilic acyl substitution is esterification. It occurs when a carboxylic acid in salicylic acid and an alcohol combine in a reaction to produce an ester. Figure 11.4. Mechanisms on the formation of aspirin Phosphoric acid protonates the carbonyl oxygen atom (C=O) of the anhydride
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being that Silica gel in TLC 2 was polar and the solvent ethyl acetate-hexane is non-polar it moved relatively with the solvent. The stationary phase in TLC 3‚ alumina is non polar and the solvent ethyl acetate is polar so from the ideal that polar does not attract non-polar benzophenone stick stronger to alumina non-polar rather than moving up with polar solvent ethyl acetate as it did in tlc2. 6. Ethyl acetate is polar and Ethyl acetate- hexane is nonpolar‚ use of polarity differences. Because the
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Preparation of Synthetic Banana Oil Eric Nelson Chem. 253-1: Deepali Rathore Lab 1: Preparation of Synthetic Banana Oil 9-24-10 Purpose To create Isopentyl acetate with no more than 10% isopentyl alcohol and no more than 2% acidic acid in its composition. Theory Esters are a chemical functional group that usually forms by loosing a hydroxyl group and having it replaced with an alkoxy group with the loss of hydrogen. Esters are most commonly produced by taking a carboxylic acid‚ and
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The reaction used for production of vinyl acetate using ethylene‚ acetic acid and oxygen over a palladium catalyst‚ in gas phase is shown below: 2 H3C–COOH + 2 C2H4 + O2 → 2 H3C–CO–O–CH=CH2 + 2 H2O Vinyl acetate synthesised is used for production of polyvinyl acetate. Acetic anhydride Acetic anhydride can be synthesized by condensation reaction of two molecules of acetic acid. The main process involves
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dried using anhydrous granular sodium sulfate. After dried‚ the sample was placed in a distillation apparatus and heated. This resulted in 1.8g of pure isopentyl acetate‚ a 44% yield. Introduction Isopentyl acetate is yielded by combining isopentyl alcohol with acetic acid using sulfuric acid as a catalyst. The product is isopentyl acetate also known as banana oil. Banana oil is an ester. Esters can be found in fruits and flowers’ scents. When water is added to an ester‚ the process can be reversed
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10mL pipet 2 aspirator 1 50mL graduated cylinder 1 10mL graduated cylinder 1 50mL beaker 1 100 mL beaker 1 glass stir rod 1 ring stand 1 clamp 1 250mL beaker Distilled water pH paper reagents: 10mL 6M acetic acid 10g solid sodium acetate 25mL 1M naOH NH3 NH4Cl 0.1 solution Safety: Acetuc acid‚ HCl and NaOH are corrosive. They attact the skin and cause permanent damage to the eyes. If one of these solutions splashes into your eyes‚ use the eyewash immediately. Hold your eyes
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|[pic] | | | | |UNIVERSITI TEKNOLOGI MARA | | | |FAKULTI KEJURUTERAAN KIMA | | | |CHEMICAL ENGINEERING LABORATORY III | | | |(CHE575)
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Oxidation of an Alcohol: Oxidizing Methoxybenzyl Alcohol to Methoxybenzaldehyde Using Phase-Transfer Catalysis PURPOSE OF THE EXPERIMENT Oxidize methoxybenzyl alcohol to methoxybenzaldehyde‚ using sodium hypochlorite as the oxidizing agent and tetrabutylammonium hydrogen sulfate as the phase-transfer catalyst. Monitor the progress of the reaction by thin-layer chromatography. BACKGROUND REQUIRED You should be familiar with extraction‚ evaporation‚ and thin-layer chromatography techniques
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