Extraction (Ch # 07) Faraz Gohar Mr. Wayne Xie Chem 201 10/02/2012 Objectives : 1)To purify samples of organic compounds that are solids at room temperature. 2)To dissociate the impure sample in the minimum amount of an appropriate hot solvent Chemical Index : Naphthalene; mp 82 *C 1‚4-Dichlorobenzene; mp 56 *C 4-Chloroaniline; mp 68 - 71 *C; pKb 4.15 Ethyl 4-Aminobenzoate; mp 90 *C; pKb 4.92 Procedure :
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Technique of Water Evaporation Introduction When water evaporates from water storages it becomes a major issue that affects regions of agriculture in most lands leading to annual loss exceeding potentially to 40 precent and more of water storage. This water which is lost leads to reduction of productivity in agriculture affecting the environment adversely. Literature review has been developed on the same by various researchers in order to develop evaporation suppression techniques
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METHODS OF EXTRACTION FOOD PROCESSING PRACTICAL (TFT 709) BY GROUP THREE MEMBERS ISMAILA AYUBA RAMADAN Submitted to Department of Food Technology University of Ibadan Lecturer-in-charge Dr. Akinoso Febuary‚ 2012 Abstract Oil extraction was carried out using two different extraction method (water and solvent) and the yield for different method were obtained. The free fatty acid for different oil was also determined immediately after extraction and also
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Extraction is a method used for separating and isolating materials. A compound is pulled from solvent A to solvent B and in this case‚ both solvents are miscible. These two concepts are not capable of mixing together; when they are mixed together‚ they form a bilayer. This can be seen when mixing oil and water together. When thinking of extractions‚ one can picture how coffee gets extracted. The flavors‚ molecules‚ caffeine‚ etc. are extracted from the coffee beans. In this experiment‚ a solution
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TWO-BASE EXTRACTION OF BENZOIC ACID‚ 2-NAPHTHOL‚ AND NAPHTHALENE FROM UNKNOWN SAMPLE # 131 Douglas G. Balmer (T.A. Mike Hall) Dr. Dailey Submitted 11 July 2007 Introduction: The purpose of this experiment was to separate a sample of benzoic acid‚ 2- naphthol‚ and naphthalene of unknown proportions using a two-base extraction method. The three components of the mixture will react differently to sodium bicarbonate and sodium hydroxide because each of the bases’ conjugate acids has a different
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My hypothesis is that if I turn the water to vapor then I will be able to determine the ratio and the amount of moles of the salt and water. This is because by using evaporation I will be able to learn the mass of the salt and of the water needed for n=m/MM which states the amount of moles can be found by dividing mass of the moles by the molar mass. Experiment 1 First I took a crucible‚ a balance‚ and a Bunsen burner and placed them onto the workbench. Then I measured the mass of the empty crucible
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techniques of an acid base extraction‚ recrystallization‚ and use of Melt Temp (melting point range). The reaction of an unknown acid (3-chlorobenzoic acid) with diethyl and sodium hydroxide was observed‚ and the solution naturally separated into an aqueous and organic solution. The mixture of acid and organic solution was created and then separated through the Hirsch funnel into separate beakers of an aqueous and organic solution. The neutral compound was obtained through evaporation‚ while the unknown
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the quantification of albumin and casein were performed and analyzed after extraction of the said proteins from their respective sources. Isolation of proteins was initiated by the breakage of the cell wall / membranes in three different ways. Homogenization of invertase‚ albumin and casein were achieved via grinding process‚ addition of 1M acetic acid and acidification by 0.1M hydrochloric acid correspondingly. Extraction of invertase and casein involved precipitation through the utilization of 95%
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Kate Kirby June 6‚ 2013 Title: Extraction of an Unknown Compound Purpose: The purpose of this experiment was to separate a mixture of two or more unknown compounds and identify them based on their melting point and reactivity with an acid or a base. Compound studied/Reactions: The organic solvent used in this experiment was methyl t-butyl ether (MTBE‚ 2-methoxy-2-methylpropane). The unknown that dissolved in the MTBE‚ but was insoluble in water. MBTE is very volatile and flammable. It was
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Hiding the Truth In John Updlike’s short story‚ “Separating‚” the author focuses on the prevailing issue of divorce and the everlasting effects on the individual family members. The fifteen-year-old son‚ John‚ of divorcing parents Joan and Richard masks his true feelings by avoiding real issues with a careless attitude. At the beginning of the story‚ readers can sense the tension between the family when they are getting ready to sit down at the dinner table together. In detail‚ John is unaware of
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