as well as above other reactions of enolates has serious limitations to be overcome. In these reactions‚ a strong base NaOH is needed to transform the carbonyl compounds into their anion forms. Generally‚ the carbonyl compounds such as ketone and aldehyde have high pKa values (pKa ~ 20) [1]. It is difficult to make their − anion forms of carbonyl compounds by removing the hydrogens on the α-carbons because of their weakly acidic characteristics. Therefore‚ the product yields of acylation‚ alkylation
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Chemistry 3373F Lab Manual 2008 Modified 11/07 Table of Contents Chem 3373 Laboratory Schedule for Fall 2008.............................................................................2 The Benzoin Condensation of Benzaldehyde ..............................................................................3 Synthesis of Dilantin and Related Compounds (two weeks).........................................................6 Synthesis of an Alkaloid: Pseudopelletierine (two weeks) .............
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Elimination The Kidneys Primary function of the kidneys is to maintain correct balance of electrolytes in body fluids (water and salt) Filters 1 liter of plasma per min; produces 1 cobic cm of urine per min Filters everything out of the blood then selectively reabsorbs Blood passes into a nephron (a long tube) Bowman’s capsule which contains a clump of capillaries (glomerulus) Nephron connects with collecting tubes that empty into the bladder The nephron is the functional unit of the kidney
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Topic Acid-Base Theory (Unit 1) Acid-Base Theory (Unit 2) Isomerism (Unit 1) Isomerism (Unit 2) Nomenclature Reaction Mechanism (Unit 1) - Introduction to Mechanism Reaction Mechanism (Unit 2) - Nucleophilic substitution Reaction Mechanism (Unit 3) - Nucleophilic substitution Reaction Mechanism (Unit 4) - Nucleophilic substitution Reaction Mechanism (Unit 5) - Nucleophilic substitution Reaction Mechanism (Unit 6) - Nucleophilic substitution Reaction Mechanism (Unit 7) - Elimination Reaction Mechanism
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Distillation Alcoholic distillation is basically the process of separation the more volatile component‚ alcohol‚ from the less volatile component‚ water‚ from a water/alcohol solution‚ by heating the solution and condensing and collecting the alcohol rich vapours released‚ as a high alcohol strength liquid (spirit). The starting material for most distillations‚ such as wine for brandy and beer for whisky‚ are usually weak alcoholic solutions (5%-7% v/v ethanol) This seems counter intuitive
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2.4.General procedure for the synthesis of 2‚3-dihydriquinazolin-4(1H) ones derivatives: A stirred mixture of isatoic anhydride (1 mmol)‚ amines containing 2-aminobenzothiazole or 2-amino benzimidazole (1.1mmol)‚ aromatic aldehydes (1 mmol) and 0.045 g of H-ZSM-5 nanozeolite was reacted in an oil bath at 100 oC for the appropriated times. Completion of the reaction was indicated by TLC. After completion of reaction‚ the mixture was cooled to room temperature. The solid residue was dissolved in hot
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Test of Biological Molecules Tamari Manyengavana 5XVGXTJ96 Laboratory Report SCPB111 Principles of Biology Faculty of Applied Sciences Pearson Institute of Higher Education 14 March 2018 Abstract Biological molecules are part of Introduction Biological molecules are formerly known as macromolecules. Macromolecules are large molecules that are formed from smaller molecules called monomers (Ellisman‚ 2014). They are formed by dehydration reactions‚ in which a water molecule is
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Sample Lab Report for CHM 152 Name Lab Partner(s) Abstract: The physical properties‚ including the boiling point‚ density‚ and refractive index were measured for unknown liquid #16. The infrared (IR) spectrum of the compound was also taken. Based on the data collected‚ it was determined that the compound was likely to be salicylaldehyde. Introduction The purpose of this experiment was to determine the identity of an unknown organic liquid by measuring some of its physical
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DATE: 11/10/12 COURSE CODE: BIOL 2365 Comparative Biochemistry TITLE: Proteins and Amino Acids RESULTS: Table 1: The results of experiment 1; the Lowry Test Volume of Standard Protein/ Unknown (mL) Absorbance at 750 nm 0 0.000 0.1 0.017 0.3 0.135 0.3 0.155 0.5 0.230 0.7 0.323 0.7 0.310 1.0 0.457 1.0 Unknown 1a 0.463 1.0 Unknown 1b 0.433 1.0 Unknown 2a 0.237 1.0 Unknown 2b 0.159 Table 2: The results of Experiment 2; Ninhydrin Test Amino acid Color X
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Viresh H. Shah* Department of Chemistry‚ Saurashtra University‚ Rajkot (Gujarat)‚ India‚ Pin-360005 E-mail: shah_v_h@yahoo.com Abstract In the present investigation ethyl 2-(4-carboxyphenylazo)acetoacetate 1 on condensation with various aromatic aldehydes in ethanolic NaOH solution yielded the corresponding chalcones 2a-j. These chalcones were further reacted with urea in the presence of base in ethanol‚ which led to the formation of pyrimidine derivatives 3a-j. The newly synthesized heterocyles were
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