| |concentrated HNO3 (4 – 6 mL) |6.0 M H2SO4 (15 mL) | |graduated cylinder |granular zinc | |3.0 M NaOH (30 mL) |methanol | |carborundum boiling chips |acetone | |stirring rod
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Like any titration‚ neutralization titrations depend on a chemical reaction between the unknown solution and a standard reagent. The point of chemical equivalence is indicated by a chemical indicator or an instrumental measurement. When the color changes to the specified color‚ the titration has reached endpoint. The mole ratio and volume relates the concentration of the solutions. The more the number of moles of the base is used the more number of moles are needed to neutralize. To increase the
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Introduction Table of Contents Introduction Materials Chemicals Equipment Safety Containers Measuring Devices Other Equipment Procedure Synthesis of Aspirin Crystalizing the Aspirin Recrystallizing the Crude Aspirin Finding the Melting Point Range Safety Precautions Acetic Anhydride Sulphuric and Salicylic Acid Heating Observations Mass of Aspirin Synthesized Melting Point Calculations Percentage Yield Maximum Yield Crude Product Final Product Melting Range Percentage
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Observations Test tube was hot after reaction; exothermic reaction took place; sodium was malleable; when sodium was added to diH2O it popped and fizzled; solution turned pink when phenolphthalein was added. Reactants: Na and H2O Products: H2 and NaOH Balanced chemical equation 2Na + 2H2O 2NaOH + H2 Table 8.4- Single replacement reaction of lithium Observations Test tube was hot after reaction; exothermic reaction took place; lithium was not malleable; when lithium was added to diH2O it
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1. Clean‚ rinse‚ and fill a buret with NaOH solution just as you did in last week’s experiment. Record the molarity of the NaOH and the initial NaOH volume reading from the buret (+0.02 mL). 2. Weigh an antacid table in a weighing boat and record the mass (+0.01 g). Transfer the tablet to a clean mortar and crush the tablet into a fine powder using the pestle. 3. Weigh about 0.2 grams (+0.01 g) of the ground up tablet powder and transfer it to a clean 250 mL Erlenmeyer flask. 4. Transfer
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Keywords acid value vegetable oils indirect titration A new method of acid value determination in vegetable oils has been developed. The method is based on (a) simple‚ rapid and complete extraction of acids from an oil test portion into reagent (0.05 mol dm–3 triethanolamine (B) in the mixture of 50 % H2O + 50 % 2-PrOH) and (b) indirect titration of acids in BH+ form against aqueous alkali in the presence of a phenolphthalein indicator. Suitable metrological parameters of acid value determination
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Partner: Camille Dupiton Lab #1 Purification of a Solid: Crystallization and Melting Point Section: A61 Laboratory Exercise #1 Purification of a Solid: Crystallization and Melting Point Introduction In this lab exercise‚ we will be learning experimental techniques using glassware and other apparatuses. In order to successfully complete this lab‚ we will use techniques 1.0‚ 1.1‚1.2‚2.0‚2.1‚2.2‚ and 2.3 that are described in the Lab Manuel. In addition‚ we will
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cheese. Lactic acid bacteria(LAB)‚ a bacteria that can be found in the production of cheese‚ its stress gene was investigated in the experiment by using various biochemical and genetic techniques to identify and extract. The characterisation of the strain illustrates how identification of strains differ using different methods‚ such as gram stain and 16s rRNA screening. After the characterisation‚ the stress gene isolation assist the further understanding of the gene on LAB be giving different stress
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[pic] Drops |Water(HcL) |Water(NaOH) |Liver(HcL) |Liver(NaOH) |Egg White(HcL) |Egg White(NaOH0) |Potato(HCl) |Potato(NaOH) |Buffer(HCl) |Buffer(NaOH) | |0 |7 |4 |7.4 |5 |8.2 |7 |6.9 |4 |10.7 |10 | |5 |4.5 |7 |6.9 |6 |7.5 |8 |6.2 |5 |10.5 |10 | |10 |2.7 |9 |6.3 |6 |7 |9 |5.7 |5 |10.4 |11 | |15 |2.6 |12 |5.8 |6 |6.4 |9 |5.3 |6 |10.3 |12 | |20 |2.5 |12 |5.4 |6 |4.5 |10 |4.9 |7 |10.2 |12 | |25 |2.4 |13 |5.1 |6 |3.5 |10 |4.6 |8 |10.1 |13 | |30 |2.3 |13 |4.8 |6 |3.3 |11 |4.2 |8 |10 |13 | | 1.
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Investigation and Preparation of Esterification Lab Introduction Esters are classified as organic compounds commonly derived from carboxylic acids. They are compounded from the reaction of a carboxylic acid with an alcohol in the presence of a strong acid to be used as a catalyst. The formula that represents an ester is R-COO-R where both Rs’ are alkyl groups‚ one which is bonded to an oxygen‚ and the other to a carbon which is double bonded to 1 oxygen and single bonded to the other. Esters
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