experiment‚ there was a total of 2.25g of caffeine (the net weight of the tea bag). After preparing the tea solution‚ extracting‚ drying and evaporating the weight of crude caffeine was .0321g‚ making the percent recovery before sublimation 1.43%. After sublimation the weight of pure caffeine was .0027g‚ making the percent recovery of caffeine after sublimation .12%. The percent recovery of caffeine is less in the second half of the experiment because the crude caffeine had some impurities in it which were
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and Sublimation of Caffeine from Tea Leaves By: Ashley Barnes CH 236 – P8 Experiment 4 & 4.5 Due: 10/15/2014 Table 1. Table of Reagents Discussion The extraction yield refers to the percent of caffeine in the tea leaves at start of the extraction experiment. Tea leaves had 0.55 grams of mass per eight ounce serving. The weight of the extracted crude caffeine was 0.264 grams. Therefore‚ the extraction yield was 48%. This means that we pulled out almost half of the caffeine in tea
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SUBLIMATION Sublimation is a technique used by chemists to purify compounds. Typically a solid is placed in a vessel which is then heated under vacuum. Under this reduced pressure the solid volatilizes and condenses as a purified compound on a cooled surface‚ leaving the non-volatile impurities behind. This cooled surface often takes the form of a "cold finger" (shown in the diagram above). Once heating ceases and the vacuum is released‚ the sublimed compound can be collected from the cooled surface
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Purpose of the Experiment: The intention of the experiment is to use solvent extraction methods to separate a mixture containing a carboxylic acid and a neutral compound. Once recovered‚ the solids were purified by recrystallization and examined by thin-layer chromatography‚ and their identities were derived by melting point and infrared (IR) spectroscopy. Extraction is a procedure that selectively dissolves one or more of the mixture compounds into a proper solvent. Extraction refers to
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1-1 EXPERIMENT 1 ISOLATION OF CAFFEINE FROM TEA In this experiment you will isolate caffeine from tea leaves and prepare the salicylate derivative. Introduction This experiment illustrates the isolation of a naturally occurring product from plant material -- caffeine from tea leaves. The experiment will provide experience in handling relatively small amounts of material and at the same time you will be exposed to several techniques and procedures which are fundamental for survival in an organic
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------------------------------------------------- Liquid–liquid extraction From Wikipedia‚ the free encyclopedia Liquid–liquid extraction also known as solvent extraction and partitioning‚ is a method to separate compounds based on their relative solubilities in two different immiscible liquids‚ usually water and an organic solvent. It is an extraction of a substance from one liquid into another liquid phase. Liquid–liquid extraction is a basic technique in chemical laboratories‚ where it is performed
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What is water purification? Water purification generally means freeing water from any kind of impurity it contains‚ such as contaminants or micro organisms. Water purification is not a very one-sided process; the purification process contains many steps. The steps that need to be progressed depend on the kind of impurities that are found in the water. This can differ very much for different types of water. In which ways is polluted water treated? Settling Before the purification process begins some
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Extraction of Caffeine from Tea Leaves Jaybee Balilea‚ Sharmaine Baysic‚ and Maria Anjelette Patricia Belen 3BIO7‚ Department of Biology‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Extraction is a technique for isolating and purifying organic substances. In this technique‚ a solution is combined thoroughly with a second solvent that is immiscible with the first solvent. The solute is extracted from one solvent into the other because it is more soluble in the second solvent
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Caffeine in the diet Email this page to a friend Bookmark & Share Printer-friendly version Caffeine is a substance that is found in certain plants. It can also be man-made (produced synthetically) and then added to food products. It is a central nervous system stimulant and a diuretic (substance that helps rid your body of fluids). Function Caffeine is absorbed and passes quickly into the brain. It does not collect in the bloodstream or get stored in the body. It leaves the body in
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Evidence Homework #1 Topic: Caffeine Preview: Every morning when I wake up the first thing I do after brushing my teeth is walk straight to the coffee pot. I pour myself a hot rich cup of coffee to start the day off. On my way out the door I grab my go cup and fill it up. When I finally get to school I get myself another cup of coffee. How many miller grams of caffeine do you think I have drank at this point? According to the Mayo Clinic a healthy amount of caffeine for an adult is 200 to 300 miller
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