(Maserton‚ p. 15). Because even small amounts of impurities systematically affect observed chemical reactions‚ the first step to determine the identity of an unknown is to purify the substance. One technique often used to purify solids is recrystallization from a selected solvent. Because of the variable solubility of different compounds in various solvents and at various temperatures‚ it is possible to remove impurities by dissolving the unknown and then immediately cooling the solvent. The
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benzene ring in salicylic acid reacts with acetic anhydride to form an ester functional group. The acetylsalicylic acid crystallizes as the solution cools and begins to come out of the solution. The acetylsalicylic acid is further purified through recrystallization with ethyl acetate. MATERIALS USED: Test Tubes Pasteur Pipette Salicylic acid acetic anhydride Sulfuric acid 125 mL Erlenmeyer flask Scale Water Hot water bath Ice Bath Buchner Fünnel 1% Ferric Chloride Ethyl acetate Glass Rod Iodine
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Quiz #1 Attempt 1 Written: Jul 7‚ 2012 9:48 AM - Jul 7‚ 2012 9:50 AM Submission View Your quiz has been submitted successfully. Question 1 1 / 1 point At what time do you have to complete your online prelab assignment to be allowed to participate in the lab? Question options: A week before the lab Day before the lab at 10 pm The morning of lab day at 8 am One hour before the lab Question 2 1 / 1 point Which materials/chemicals belong in the desiccator? Question options: Drying
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thirty minutes. The crystals were then washed with water three times and recrystallized using ethanol. It was then characterized using melting point analysis. The percent yield for this reaction was 59.84%. This was due to loss of crystals during recrystallization and during solvent removal from the reaction mixture. The observed melting point was 104 – 107.5°C‚ compared to a literature value of 110°C. The lower and broader observed melting point may have been due to the product still being wet. It may
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methyl m-nitrobenzoate. The product was then isolated and recrystallized using methanol. This reaction is an example of an electrophilic aromatic substitution reaction‚ in which the nitro group replaces a proton of the aromatic ring. Following recrystallization‚ melting point and infrared were used to identify and characterize the product of the reaction. Purpose: The purpose of this experiment is to synthesize methyl nitrobenzoate from methyl benzoate‚ concentrated nitric acid‚ and concentrated
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1. Introduction Ice cream is a favorite of millions‚ because a delicious‚ attractive and relatively inexpensive food item (Marshal and Arbuckle‚ 1996)P2‚7. The protein content of ice cream has an excellent biological value because it contains the essential amino acids such as tryptophan and lysine. So target groups such as elderly can get their required protein from ice cream(Goff and Hartel‚ 2013)P35. In the modern diet‚ here is a concern that excessive usage of fats leads to increasing propagation
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Synthesis of Aspirin and Oil of Wintergreen INTRODUCTION: Synthesis and use of organic compounds is an extremely important area of modern chemistry. Approximately half of all chemists work with organic chemicals. In everyday life‚ many if not most of the chemicals you come in contact with are organic chemicals. Examples include drugs‚ synthetic fabrics‚ paints‚ plastics‚ etc. Synthesis of Aspirin and Methyl Salicylate. The two compounds we will be preparing‚ aspirin (acetylsalicylic acid) and oil
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Sourav Sett National institute of technology‚ durgapur. ------------------------------------------------- Plate Mill project report Sourav Sett National institute of technology‚ durgapur. ------------------------------------------------- Plate Mill project report Project Report Plate Mill Jindal Steel and Power Ltd. Raigarh Name: Sourav Sett College: National Institute Of Technology‚ Durgapur Introduction I am very grateful to Mr. N.Rajkumar and Mr.S.S.Kumar for
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LAB REPORT! EXPERIMENT#5‚6! MANPREET KAUR KHAIRA! LAB PARTNER: VIAN RAIES! The purpose of this lab exercise was to perform the bromination of (E)-1‚2-diphenylethene (trans-stilbene) by addition reaction in which bromine was added across the double bond to yield a vicinal dibromide. The next step was to perform a double elimination reaction by product gained to synthesize an alkyne‚ that is‚ 1‚2-diphenylacetylene. The two major techniques used in this lab were TLC analysis and UV-vis spectroscopy
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the unknown D liquid and solid by using its acidic and basic characteristics in a chemically active extraction then to identify the unknowns by analyzing the physical properties on IR and NMR spectrums. The neutral solid was purified through recrystallization and the melting point range was determined to be 47.5oC to 48.9oC. The basic liquid was purified with simple distillation and the boiling point of 135oC was concluded. Through the analysis of IR spectrum of each unknown the structures for each
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