Feasibility trails were carried out by melt granulation method. Method: Drug was passed from 40# sieve. Weigh accurately drug‚ polymer and other excipients. Wax was melted at 60-65°C. After that drug and other ingredient were added to wax and mixing of drug and wax was done. Prepared lump was passed from 10# sieve. Granules were dried at 40°C. Lubricant was added to granules. Granules were compressed to prepare tablets. Table 4.6: composition of trail F1 and F2 Ingredients F1 F2 Metformin Hydrochloride
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Objective: The purpose of the lab is to learn filtering techniques. Specifically‚ to form and filter a calcium carbonate precipitate using a Buchner funnel. Procedure: a.) Prepared a mixture of .5 M calcium nitrate (45 mL) and .01 M sodium carbonate by combining and stirring the two liquids in a beaker. Allow the mixture to stand. b.) Prepare the filtration assembly. The assembly consists of a tapered flask with a buchner funnel inserted in the top. The funnel has a rubber stopper attached
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OBJECTIVE The main objective of this experiment is to carry out qualitative analysis to identify metal cations in unknown solution 1. INTRODUCTION An unknown material can be determined by using simple chemical tests and separations which is called as inorganic qualitative analysis. The separation of cations depends on the difference in their propensity to form precipitates. Separation scheme is used to classify cation into five groups on the basis of their physical and chemical behavior opposed
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Non-Tradional Machining What is the principal cause of tool wear in ECM? There is no tool wear to speak of in ECM as the tool is protected cathodically during the process. There may be some chemical reaction between the tool and the electrolyte when the power is off‚ depending upon the materials involved. What is the nature of the surface obtained by electro discharge machining? The surface is heated by the sparks to either melt or even vaporize metal. The melted metal is washed away
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How does a catalyst in the form of a metal ion affect the rate of reaction in an iodide clock reaction with potassium peroxydisulphate ions? Background When peroxydisulfate ions (S2O82-) react with iodide ions (I-) in the presence of a starch indicator‚ they produce a dark blue solution. Reaction (1) S2O82- + 3I- I3- + 2 SO42- (peroxydisulfate ion) (iodide ion) (iodine ion) (sulfate ion) To determine the rate law for this reaction a series of changes
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Lab 3: Stoichiometry of a Precipitation Reaction NOTE: All photos should be taken so the reading on the electronic balance is readable. Photo 1: filter paper being weighed on electronic balance‚ along with your student information card. Photo 2: beaker with precipitate slurry in it (after step 5) ‚ along with your student information card Photo 3: dried precipitate/filter paper being weighed on electronic balance‚ along with your student information card Additional Question Guidelines:
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Abstract There are many methods employed to precipitate proteins out of solution. In this experiment we manipulated many physical and chemical variables in order to achieve purification of a protein via precipitation. In the first part of the experiment we purified the protein casein by modifying it’s pH. In the second part of the experiment we manipulated the ionic strength of albumin in egg whites‚ in a process called salting out. By manipulating these chemical properties we were able to
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To resolve this and to design an ultrasound-enhanced process that would lead to homochirality in the absence of glass beads‚ we employed seeding during ultrasound-enhanced deracemization. We theorized that by introducing larger seed crystals to the system after the establishment of the monodispersed sized crystals (~2 hours)‚ we would broaden the crystal size distribution and thus allow the deracemization process to resume. To test this idea we performed seeded experiments using ultrasound‚ in which
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Step 1: Pb (NO3) 2 (aq) + CaCl2 (aq) PbCl2 (aq) + Ca (NO3) 2 (aq) (double displacement reaction) According to the solubility guidelines lead (II) chloride (PbCl2) is a possible precipitate. This is because even though most chlorides are soluble‚ lead chloride is considered insoluble (p.2‚ Lesson 17). Step 2: PbCl2 ↔ Pb2+ + 2Cl- Q = [Pb2+] [Cl-] 2 Step 3: Ksp = 1.2 x 10-5 (from table 17.1‚ p.5) Step 4: V2 = 20.0 mL (volume of Pb (NO3)2) + 45.0 mL (volume of CaCl2) = 65.0
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The objective of this lab was to identify an unknown compound by determining the melting point range using fast and slow ramps. Also‚ to determine the eutectic point of Urea and Cinnamic Acid. An unknown compound that was numbered 8 was chosen. A small amount of the unknown compound was placed in a weighing paper using a spatula. The weighing paper was folded in half twice and then was grinded using a spatula. After the unknown compound was grinded about 1-2mm was added into a capillary tube. A
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