Quantitative Analysis Gravimetric Determination of Iron as Fe2O3 Laboratory Experiment 2 February 19‚ 2013 Abstract: In the Gravimetric determination is the measurement of mass in two different forms precipitation and volatilization. In our experiment we will be using the precipitation form which isolates an ion in a solution by a precipitation reaction‚ filtering‚ purifying by wash method‚ conversion to product of known composition‚ and final weigh of the product comparing the mass
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Laboratory #16: Analysis of Grease in Water by Solvent Extraction Experiment Date: 2/19/10 Due Date: 2/26/10 II. Objective The goal of this lab was to determine the amount of impurity‚ in the form of oil‚ in water using the method of solvent extraction‚ also known as liquid-liquid extraction‚ a method of separating two materials with different physical and/or chemical properties. Two methods of evaporation will be used to finally determine the concentration of impurity- one using an explosion-proof
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------------------------------------------------- Liquid–liquid extraction From Wikipedia‚ the free encyclopedia Liquid–liquid extraction also known as solvent extraction and partitioning‚ is a method to separate compounds based on their relative solubilities in two different immiscible liquids‚ usually water and an organic solvent. It is an extraction of a substance from one liquid into another liquid phase. Liquid–liquid extraction is a basic technique in chemical laboratories‚ where it is performed
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Chemistry 112: Anion Analysis Page 7 ANION ANALYSIS M uch of the work you will be doing in the Chemistry 112 laboratory will be concerned with identifying positive and negative ions‚ that is‚ cations and anions‚ in solutions whose composition is unknown. This procedure is called QUALITATIVE ANALYSIS. The modern chemist frequently wishes to identify the constituents in a very small amount of substance‚ and so he depends heavily on instrumental methods of analysis. While the procedures
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experiment as if all 3 compounds are present. In this particular experiment‚ the compounds are benzocaine‚ salicylic acid‚ and naphthalene. An appropriate organic solvent is used to create the ether phase. Diethyl ether is used because it has low solubility in water but will dissolve the components of the mixture (creating liquid layers)‚ is not acidic or basic‚ is less dense than water‚ and can be easily removed by evaporation. To begin the separation‚ the student needs to produce a salt that is water-soluble
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Thus‚ the comprehension of phase diagrams for system is very important. Besides‚ phase diagrams provide important information regarding the melting‚ casting‚ crystallization and other information [1]. 1) Binary Systems with Partial Solid Solubility This is the case of the alloy Aluminum and Copper‚ which solute atoms of another metal can be dissolved in the solvent in a solid state. In such diagrams‚ three single phase regions are found on the diagram: α‚ β‚ and liquid. The α phase‚ a solid
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Isolation‚ purification and characterization of alkaloid caffeine from tea leaves Date Submitted: September 3‚ 2014 Abstract Caffeine is one of the main constituents of tea leaves. In this experiment‚ 0.0039 g of pure caffeine was isolated from tea leaves. This was done through solid-liquid extraction followed by multiple liquid-liquid extraction. Then crude material obtained was then purified by sublimation. The isolated caffeine was subjected to thin layer chromatography (TLC) together
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Identification and characterization of model drug 7.1.1 Description: A pale yellow‚ crystalline powder having bitter taste. 7.1.2 Melting point: The melting point of model drug was found to be 318ºC which confirmed the purity of model drug. 7.1.3 Solubility: Solubility of model drug in distilled water was found to be 10 mg/ml. 7.1.4 Ultraviolet spectrum: The λ max of model drug in 0.1N hydrochloric acid 278nm. Figure 7.1: UV Spectrum of model drug in 0.1 N HCl The λmax selected for the further analysis
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Extraction of caffeine from Lipton tea leaves Maria Gianna Beatrice L. Cancio*‚ Joe Mari Isabella B. Caringal‚ Rowena A. Chiang‚ Patricia Deanne del Valle Department of Biological Sciences‚ College of Science‚ University of Santo Tomas‚ España‚ Manila‚ Philippines Abstract Caffeine was extracted from Lipton tea leaves by multiple extraction techniques namely solid to liquid extraction and liquid to liquid extraction; the purification by sublimation and melting point determination. Three
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INTERNATIONALE PHARMACEUTICA SCIENCIA | Jan-March 2011 | Vol. 1 | Issue 1 | Available online http://www.ipharmsciencia.com ©2011 IPS REVIEW ARTICLE Phytochemical screening and Extraction: A Review ABSTRACT Plants are a source of large amount of drugs comprising to different groups such as antispasmodics‚ emetics‚ anti-cancer‚ antimicrobials etc. A large number of the plants are claimed to possess the antibiotic properties in the traditional system and are also used extensively by the tribal people
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