David Kennedy CHE 235 Lab 10/30/14 Scale-up Synthesis and Characterization of Butyl 2-Cyano-3-(3‚5-dichloro-phenyl)-2-propenoate‚ TSE Project #131 Introduction: This report describes the steps taken to create the scale-up of targeted trisubstituted ethylene‚ Butyl 2-Cyano-3-(3‚5-dichloro-phenyl)-2-propenoate compound (#131)‚ and also the characterization methods deployed to the results. This report serves as a critical step in the overall objective of the project; the synthesis of the copolymer
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Introduction The purpose of this lab is to synthesize Lidocaine from 2‚6-dimethylaniline‚ using diethyl amine‚ 2-chloroacetyl chloride‚ acetic acid‚ and toluene. The Lidocaine was made by adding 2‚6-dimethylaniline to 2-chloroacetyl chloride in acetic acid. Sodium acetate is added in order to make the compound soluble. The product is dried‚ then treated with diethyl amine and toluene. This is refluxed using a water-cooled reflux condenser. The vapor is condensed by the cold water as the compound
Free Solvent Acetic acid Ethanol
Value of Boiling Point: 1- methycyclohexene: 110oC 3- methycyclohexene: 104oC Balanced Chemical Equations Mechanism: Experimental Procedure: (as per lab handout) 1) Add 6 mL of 2-methylcyclohexanol‚ 5 mL of 85% phosphoric acid and a boiling stone to a 25 mL round bottom flask. 2) Set up the flask and also start setting up the distillation
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gures and units. (3 points) Events Masses Empty Dish 24.35 g Dish with NaHCO3 37.06 g Dish with NaHCO3 and HCI 40.06 g Dish after burning 31.52 g Write the complete balanced equation for the reaction that occurred in this lab. Hint: H2CO3 is not a final product of the doublereplacement reaction; it breaks down (decomposes) immediately into two products. (3 points) ___HCl___ + __NaHCO3___ → __H2O___ + __CO2___ + __NACl___
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100 Weight of the of 500ml RB flask before addition of sample: 206.43g Weight of 500ml RB flask after addition of sample solution: 212.79g Weight of sample = 212.79 – 206.43 = 6.36g Theoretical yield is calculated with the aid of a balanced stoichiometry of the reaction. 1. Theoretical yield of methyl salicyl weight of salicylic acid taken: 14g Moles of salicylic acid: 14.g/138 = 0.10moles Mass of methanol = Volume of methanol X Density of methanol. Volume of
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1.TITLE: To prepare isopentyl acetate (isoamyl acetate) 2. AIM: To make an ester referred to as banana oil from acetic acid and isopentyl alcohol 3.THEORY: This ester is often referred to as banana oil‚ since it has the familiar odor of this fruit O O CH3 H+ CH3 CH3C OH +
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Kennedy Date: 11/5/14 Project No: 131 Title: Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate Abstract: The targeted trisubstituted ethylene compound Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate and its copolymer with styrene was prepared in this lab. The base catalyzed Knoevengael condensation of butyl cyanoacetate and corresponding aldehyde led to the forming Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate. The analyses that were used to prove its composition and structure include; IR spectroscopy
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Percent Yield = Actual or experimental yield in grams (or moles) X 100 Theoretical or calculated yield in grams (or moles) Show all of your calculations! Graphs should be done on graph paper. Note: Our lab manual contains a "Data Report Sheet" for each experiment. You may record your results here and include this sheet at this stage of your report. The discussion part comes from you! Were your results what you expected? If‚ not‚ can you suggest reasons
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Title: Experiment 28: Nitration of Methyl Benzoate Objective: The students will learn to nitrate methyl benzoate through electrophilic aromatic substitution reaction. They will learn the importance of regiochemistry in chemical reactions. They might experience disubstitution through a high temperature. Reactions: Observation: The crystals started to form when added 2 g of crushed ice. The addition of hot methanol dissociated the crystals. The crystals reappeared when cooled down in
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Lab Report Macrocyclic Synthesis (Heme Analog) I. Purpose of Experiment and Introduction The purpose of this lab experiment is to prepare meso-tetraphenylporphin (TPP) and its copper‚ cobalt or zinc complex by condensing benzaldehyde with pyrrole in boiling propanoic acid. II. Introduction and Background There are two types of proteins that function as oxygen carriers: myoglobin (stores the oxygen) and hemoglobin (present in red blood cells and is responsible for oxygen transport)
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