Experiments 4A-C: Synthesis and Component Analysis of an Iron (III) Oxalate Complex My Name TA‚ Section B## Work Performed on 10/23‚ 10/30‚ & 11/4‚ 200# Report due Tuesday‚ November ##‚ 200# 1. Abstract This experiment initially involved the synthesis of an iron (III) oxalate complex with the general formula Kw[Fex(C2O4)y]·zH2O. The variables x‚ y‚ and z were determined through the duration of the entire experiment. From 1.2000g of Fe(NH4)2(SO4)2 were synthesized 1.1###g of K3[FeIII(C2O4)3]·3H2O
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Title: Experiment 28: Nitration of Methyl Benzoate Objective: The students will learn to nitrate methyl benzoate through electrophilic aromatic substitution reaction. They will learn the importance of regiochemistry in chemical reactions. They might experience disubstitution through a high temperature. Reactions: Observation: The crystals started to form when added 2 g of crushed ice. The addition of hot methanol dissociated the crystals. The crystals reappeared when cooled down in
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Introduction: A balanced chemical equation has reactants and product that has to represent a formulae. The amount of each element‚ number needs to be the same in either side of the equation. (E.g.‚ HCl(aq)+NaHCO3(s) reacts to produce NaCl(aq)+H2O(I)+CO2(g)‚ this is the equation given for this lab). This help us view the study of Law of Conservation of Mass‚ when either side of equation is equally balanced. The calculation for formula mass helps determine if you need to convert grams to a particular
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Extraction and Quantitative Determination of B-Carotene Introduction The study of B-Carotene is important because it is good for vision‚ immunity‚ and overall health. The purpose of this experiment is to extract and find quantitative amount of Beta-carotene from a carrot sample. The raw product(carrots) was extracted using simple distillation. The purity of the product will be characterized using percent yield‚ thin layer chromatography‚ Beer’s Law‚ and UV-vis. Beer’s law is used because in this
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Thiamine-Catalyzed Benzoin Condensation I.Conclusion Benzoin was produced by reacting 2 mols of benzaldehyde with the catalyst thiamine to form a new C-C bond. A total of 2.626 grams were recovered. There was a 33% recovery of benzoin. The low percent recovery could be due to the purity of the limiting reactant‚ benzaldehyde. Upon filtration‚ the mother liquid appeared oily making it more likely that the low recovery was due to the solution ‘oiling out.’ This could be avoided in the future
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Create a data table to record your data from the procedure. Be sure that the data table is neat and organized and that all measurements have the correct significant figures and units. (3 points) Events Masses Empty Dish 24.35 g Dish with NaHCO3 37.06 g Dish with NaHCO3 and HCI 40.06 g Dish after burning 31.52 g Write the complete balanced equation for the reaction that occurred in this lab. Hint: H2CO3 is not a final product of the doublereplacement reaction; it breaks down (decomposes) immediately
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Determination of the mole ratio of a chemical reaction The method of continuous variations is a means of determining the stoichiometric mole ratio of the reactants in a chemical reaction. The stoichiometric ratio‚ as given by the coefficients in the balanced chemical equation‚ represents the ratio at which chemicals must be combined to produce all product with no excess reactant. Since there is no “wasted” reactant‚ the maximum amount of product is made for the given amount of both reactants
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wavelength Percentage concentration (methanol: water) Peak H value (height equivalent to a theoretical plate) (mm) 230nm 80:20 Phenol 0.0373 Benzophenone 0.0196 Naphthalene 0.0164 235nm 80:20 Phenol 0.0327 Benzophenone 0.0203 Naphthalene 0.0147 260nm 80:20 Phenol 0.0318 Benzophenone 0.0202 Naphthalene 0.0146 Figure 11: table for the height equivalent of the theoretical plates. It can be observed that the H values or height equivalent to a theoretical plate for phenol at the three wavelengths
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I. Introduction The Percent Yield lab is designed to further the students’ understanding of percent yield by having them predict how much material will be produced from a reaction; specifically a double replacement reaction. In order to perform the lab‚ a solid understanding of percent yield is necessary. According to Prentice Hall Chemistry book‚ percent yield is comprised of two main components. The first is the theoretical yield. The theoretical yield is what is calculated and predicted. It is
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In the Stoichiometry Challenge Lab we compared the theoretical results of the reaction between sodium carbonate (Na2CO3) and sulfuric acid (H2SO4) with the actual data we found. I hypothesised that If the mole ratio between Na2SO4 and H2SO4 is 1:1 then when I react 0.5 grams of Na2SO4 (reactant with H2SO4) I should get 0.669 grams of Na2SO4. The actual reaction between .05 grams of Na2CO3 and 5 mL of of H2SO4 produced 0.79g of Na2SO4. When I were testing the reaction‚ I measured out the reactants
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