Preparation Of Triphenylmethanol Objectives 1. To study the preparation of triphenylmethanol using through Gridnard reaction 2. To study the operations of anhydrous reaction‚ water vapor distillation. Principles Alcohol is widely used in organic chemistry‚ not only as solute but also as intermediate to synthesize halide‚ alkene‚ ether‚ aldehyde and ketone etc. In laboratory‚ an important method of synthesizing alcohol is though the addition reaction of Gridnard reagent and carbonyl compound‚ whereas
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The first days in the lab will be used to practice with collecting bare footprints from different individuals using the bare footprint reagent cream. To get access to the lab‚ a Practical Risk Assessment must be made (see appendix I)‚ and three Health & Safety courses must be completed (see appendix II). After practicing with collecting bare footprints‚ the study starts with collecting footprints from six specific participants‚ whose footprints have already been collected by two other investigators
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ions Reagent/ Condition; Reaction | Explanation | Oxygen supply; Combustion | Limited supply of oxygen: CO formed.Even less Oxygen: C is deposited as soot. Excess Oxygen: Complete combustion (giving CO2 and H2O) | Al2 O3 and vaporisation of alkane at 500°C; Cracking of Alkanes | Al2 O3 is used as a catalyst. Heat provides energy for breakage of C-C bonds. | UV light; Initiation step of FRS of alkanes by halogens * Not required for electrophilic addition reaction btw Halogens and alkenes
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The purpose of this experiment was to prepare the Grignard reagent methylmagnesium iodide and react it with benzoin to form the 3o alcohol 1‚2-diphenyl-1‚2-propanediol‚ through an addition reaction pathway. Introduction: Grignard reagents are alkyl or aryl-magnesium halides that act as the nucleophile in Grignard reactions‚ where ketones are reacted with the reagent‚ then treated with acid to produce an alcohol. In the case of this experiment‚ methylmagnesium iodide was created from methyl
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– ethyl methyl ether Physical Properties of Ethers: Ethers have much lower boiling points compared to alcohols of comparable MWs. BPs of ethers increases with increasing MW. BPs of isomeric ethers increase with increasing alkyl chain length. BPs of ethers are about the same as those of alkanes of comparable MWs. Solubility of ethers in water is comparable to that of alcohols. As chain length of ethers increases‚ solubility in water decreases. Branching of the alkyl chain results
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Stoichiometry and Limiting Reagents Theodore A. Bieniosek I. Purpose and Theory The purpose of the experiment is to study and apply the processes of stoichiometric calculation on a controlled chemical reaction. We will be adding variable amounts of reactants in a chemical reaction in order to demonstrate the effect of limiting reagents. Based on the volumes of the reactants‚ and their respective molarities‚ we can calculate the theoretical yield of the reaction and compare it to the
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Mona Vaidya April 8‚ 2014 Professor Diaz Chem 317 Section: 20711 Lab Experiment: Nitration of Bromobenzene Introduction: The chemical reaction of nitration consists of a nitro group being added to or substituted in a molecule. Nitration can basically be carried out by a mixture of concentrated nitric acid and sulfuric acid; this mixture is useful to obtain the active nitronium ion. Electrophilic aromatic substitution is a method used when a functional group is needed to be substituted on
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compound which acts as a reference in all titrimetric volumetric analysis. A secondary standard is titrants that is standardized against a primary standard or another standard solution and are used for certain types of analysis. A primary standard is a reagent that is extremely pure‚ stable‚ it’s not a hydrate/has no water of hydration and has high molecular weight. A primary standard is used to calibrate other standards referred to as working standards. Examples of primary standards for titration of acids
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Objectives * Be able to prepare cyclohexene from the dehydration of cyclohexanol * Understand the mechanisms of the dehydration reaction (acid-catalyzed dehydration). * Know how to use the necessary equipment for this reaction‚ such as the fractioning column. * Obtain positive results in unsaturation tests for the presence of carbon-carbon double bond (cyclohexene). II. Background Cyclohexanol‚ the reagent of this experiment‚ is used in the production of nylon‚ paints
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Limiting Reagents and Percentage Yield Worksheet 1. Consider the reaction I2O5(g) + 5 CO(g) -------> 5 CO2(g) + I2(g) a) 80.0 grams of iodine(V) oxide‚ I2O5‚ reacts with 28.0 grams of carbon monoxide‚ CO. Determine the mass of iodine I2‚ which could be produced? 80 g I2O5 1 mol I2O5 1 mol I2 1 333.8 g I2O5 1 mol I2O5 28 g CO 1 mol CO 1 mol I2 253.8 g I2 1 28 g CO 5 mol CO 1 mol I2 b) If‚ in the above situation‚ only 0.160 moles‚ of iodine‚ I2 was produced
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