technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol‚ then characterized using melting point analysis. Introduction: In this experiment we learnt on carbonyl compounds‚ enols and enolates. We also learnt two different techniques
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Separation and Identification of Organics from an Aqueous/Organic Environment through Physical Manipulation Date Lab Performed: Nov. 11/2013 Date Lab Submitted: Nov. 18/2013 Introduction We conducted this experiment to investigate the technique of liquid / liquid extraction‚ the miscibility of organics and water and the effect of a mixture of compounds in methylene chloride versus pure compounds retention time as introduced to a Gas
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International Journal of Advances in Engineering & Technology‚ July 2011. ©IJAET ISSN: 2231-1963 EFFECT OF PROCESS PARAMETERS ON MECHANICAL PROPERTIES OF THE INVESTMENT CASTINGS PRODUCED BY USING EXPANDABLE POLYSTYRENE PATTERN Nikhil Yadav1 and D. B. Karunakar2 1 2 M.Tech Scholar‚ Mechanical & Industrial Engg. Deptt.‚ IIT Roorkee‚ Roorkee‚ India Assistant Professor‚ Mechanical & Industrial Engg. Deptt.‚ IIT Roorkee‚ Roorkee‚ India ABSTRACT The present study is concerned with the investigation
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ethanol/acetone Recrystallize Characterization of aldol product Perform this test on both unknown compounds Add 1 drop of the unknown compound to a test tube and add 1 mL of acetone Then Add 1 drop of the chromic acid-sulfuric test reagent directly into the solution. Shake the mixture A green bluish green precipitate appears within 1 min if the unknown compound is an aldehyde (Aliphatic aldehydes give precipitates with 15 s whereas aromatic aldehydes usually take 30-60s. Acetone and other
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I found that among mentioned substances acetone and ethylene glycol are soluble in water‚ therefore we can say that they are polar substances. Besides‚ I observed that biphenyl‚ butyl acetate‚ glycerol and motor oil are nonpolar substance. These compounds were soluble in hexane. Meanwhile‚ magnesium
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Materials: ● ● ● ● ● ● ● ● ● ● ● 1000 ml beaker/2 gallon tank air pump air stone tubing eye droppers 10 ml pipettes graduated cylinders small petri dishes dissecting scopes/hand lenses beakers stopwatch live brine shrimp Lysol Bleach vinegar acetone (nail polish remover) Procedures: Place live brine shrimp in a small aquarium tank or a 1000ml beaker with an aerator. Place 2 petri dishes at each lab table. Three tables will be working on sample A and the other half working on sample B
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experimented on the reactions of the chemicals that undergoes SN1 or SN2 reaction. Nine different compounds were given to be examined with two reagents - NaI in acetone and AgNO3 in ethanol. The SN1 reaction happens in AgNO3 in ethanol reagents‚ and SN2 reaction is in NaI in acetone. Procedure: Following the lab manual. Results: compound NaI /acetone (SN2) AgNO3/ethanol (SN1) Bromobenzene NR NR Bromocyclopentane X 2 sec Bromocyclohexane NR 4 sec 2-bromobutane 5 min 2 sec 2-chlorobutane
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Methodology The reagents used for this experiment were the following: * Methyl red * 0.1M Nitric Acid * 0.5M Copper sulfate – sulfuric acid mixture * 0.1M Sodium hydroxide * Acetone * Distilled water The apparatus used were the following: * Phywe Transference Number Apparatus * Analytical Balance * Buret * Beaker * pipet The experiment starts off with the preparation of the set-up for the transference vessel. Fill the double U-tube with 0.1M Nitric acid
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in the Organic Laboratory. In Abstracts of Papers‚ 225th ACS National Meeting‚ New Orleans‚ LA‚ March 23−27‚ 2003; American Chemical Society: Washington‚ DC‚ 2003; CHED-1277. (2) Swearingen‚ L.; Florence‚ R. T. The Solubility of Sodium Bromide in Acetone. J. Phys. Chem. 1934‚ 39 (5)‚
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1. What is the ideal solvent for crystallization of a particular compound? What is the primary consideration in choosing a solvent for crystallizing a compound? volatile in order to be easily removed from the purified crystals. In selecting a solvent consider that like likes like. Polar compounds dissolve polar compounds and non-polar compounds dissolve non-polar compounds. Solvent will dissolve a large amount of the impure compound at temperatures near the boiling point of the solvent the compound
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