represents one of the most promising options for the use of conventional fossil fuels. In the first step of this experimental research‚ edible rice bran oil used as test material and converted into methyl ester and non-edible jatropha vegetable oil is converted into jatropha oil methyl ester‚ which are known as biodiesel and they are prepared in the presence of homogeneous acid catalyst and optimized their operating parameters like reaction temperature‚ quantity of alcohol and the catalyst requirement
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a solution α-naphthol 1a‚ 4-methylbenzaldehyde 2a and tert-butyl isocyanide 3a in EtOH was magnetically stirred at 45 C for 12 hours under an oxygen atmosphere with an equimolar ratio of the three reactants. TLC monitoring of the reaction mixture exhibited formation of a new product‚ which was purified (Table 1‚ entry 1). Identification of its structure by NMR spectroscopy revealed that it was 2-(4-methylbenzoyl)-1-naphthyl N-(tert-butyl)carbamate (4a). Next‚ in order to improve the yield of 4a‚
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The Equilibrium Constant of an Ester Hydrolysis Reaction CHM 152LL Section 33263 March 28‚ 2014 John Weide Abstract: The purpose if this experiment is to determine the equilibrium constant of an unknown alcohol. In this experiment unknown alcohol number three and unknown ester number three were used. The equilibrium constant was found by titrating a series of reactions containing H2O‚ HCl‚ and the unknown ester with only the last solution containing the unknown alcohol
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Title: Esterification Objective: To recover and calculate the percentage yield of substance by esterification. Introduction: When a carboxylic acid reacts with an alcohol‚ the products are water and ester. The overall reaction is reversible and slow‚ as soon as the products begin to form‚ hydrolysis a reverse reaction of esterification occurs. To ensure the reaction is complete an acid catalyst is commonly used. The catalyst is usually concentrated sulphuric acid. This experiment covered 4
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Steam Distillation of Lemongrass Oil I. Introduction When a mixture of cyclohexane and toluene is distilled‚ the boiling point of these two miscible liquids is between the boiling points of each of the pure components. By contrast‚ if a mixture of benzene and water (Immiscible liquids) is distilled‚ the boiling point of the mixture will be found below the boiling point of each pure component. Since the two liquids are essentially insoluble in each other‚ the benzene molecules in a droplet of
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April 04‚ 2014 Fisher Esterification Introduction: Esters are one of the most common derivatives of carboxylic acids and are widely distributed in both nature and industry. A Fischer Esterification is the formation of an ester and water from alcohol and an acid. It is the simplest means of synthesizing an ester and requires the reaction of a carboxylic acid and an alcohol. The general reaction of Fischer esterification is‚ CH3CO2H + ROH ↔ CH3CO2R + H2O (reaction1) CH3COOH + ROH ↔
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Assignments in Science Class X (Term II) 4 Carbon and its Compounds IMPORTANT NOTES 9. Unsaturated organic compounds : Organic compounds in which a double or a triple bond exists between two carbon atoms in a carbon chain‚ are called unsaturated organic compounds. 10. Hydrocarbons : Organic compounds which contain only carbon and hydrogen atoms are called hydrocarbons. 11. Straight chain hydrocarbons : Hydrocarbons‚ in which all the carbon atoms are linked to one another in a straight chain
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moves slowly through the packed column. In this experiment‚ an adsorption chromatography column was constructed using silica gel as the adsorbent. A 50:50 mixture of ferrocene and acetylferrocene was then separated using the eluents hexane and tert-butyl methyl ether (TBME). The less polar ferrocene was attracted to the less polar hexane‚ so as the hexane passed through the stationary phase‚ the ferrocene moved with it and the acetylferrocene was left behind. When TBME was passed through the stationary
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leaving groups (anions i.e. Cl-‚ RO-‚ RCO2-) = unstable - starting carbonyl compound with good leaving group = unstable (makes a Tetrahedral intermediate then collapses to form the starting carbonyl group) i.e. Grignard reagent added to an ester
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Hexadecane(1)‚ 2-[4a‚ 8-Dimethyl-3‚4‚4a‚5‚6-hexahydro-napthalene-2-yl]-prop-2-en-1-ol(2)‚ Heptadecane(3)‚ Benzene‚ [1-butylheptyl]-(4)‚ Benzene‚ [1-methyldecyl]-(5)‚ Oxirane‚ tetradecyl-(6)‚ Hexadecanoic acid‚ methyl ester(7)‚ Hexadecanoic acid‚ ethyl ester(8)‚ 9‚12‚15- Octadecatrienoic acid‚ ethyl ester‚ [Z‚Z‚Z]-(9)‚ Lupeol (11) . The ethanolic extract of the aerial parts showed the most promising activity among selected four solvents against clinically isolated pathogenic bacterial strains. The Ethanol:water
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