Weighed accurately about 25.0 mg of baclofen and transferred to 25 ml volumetric flask. Added 20 ml of a 0.001 M aqueous hydrochloric acid solution and sonicated to dissolve and degassed. The resultant solution diluted up to the mark with diluents to obtain 1000 μg/ml. Further stock solution was used to prepare plasma standards to construct the calibration curve. C. Pre-chromatographic isolation of baclofen from plasma Prior to chromatography‚ baclofen from plasma constituents was isolation by adding
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Name: Bulose Sihle Student Number: 209504496 Date of Practical: 11 April 2013 Inductively Coupled Plasma – Atomic Emission Spectroscopy Aim The aim of this practical was to use an ICP-OES to perform a multi-elemental analysis of different types of tea. The elements that were analysed in the tea were copper‚ iron‚ manganese and magnesium. The sample is introduced into the plasma as an aerosol. Argon gas flows through three concentric quartz tubes in the plasma torch. This argon gas transports
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concentration of solute‚ the more light will be absorbed and a higher reading will be obtained on the spectrometer. Procedure: Part A: 1. Obtain 10.0 ml measuring (MoHr) pipet and two cuvettes from a storeroom. 2.Pipet 7.0ml of 0.5M HNO3 into blank cuvette. 3.Into other pipet 4.00 mL of A and 3.00mL of B 4. Cover mouth of pipet w/plastic wrap place thumb on top of plastic and carefully shake. 5. Before placing cuvette into compartment wipe with chem tissue.
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Description Table salt Piece of string Isopropyl (rubbing) alcohol Tap water Paper‚ 5 cm x 5 cm for weighing chemicals Beaker‚ 100 mL‚ glass Cylinder‚ 25 mL 25-mL volumetric flask Pipet‚ Serological-2mL Bulb‚ Rubber Goggles-Safety Scale-Digital-500g Test Tube (1)‚ 13 x 100 mm Bolt‚ Metal – Small Magnet bar Pipet‚ Empty Short Stem 2 Discussion and Review In this experiment you will learn the techniques for using several pieces of laboratory equipment and become familiar with
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We had to dilute the stock solutions to a specific molarity for the experiment. Using the same method‚ an unknown solution called “120x” was titrated to find its percentage of oxalic acid. Introduction The purpose of the experiment was to use volumetric analysis‚ a chemical analysis involving measuring a liquids volume to
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repeatedly measure out small volumes of solutions A–I. The burette made the task convenient‚ and it is a precise instrument. | 250 cm3 volumetric flask | I needed to make up a specific volume of a standard solution. The volumetric flask has a low error. | 100 cm3 volumetric flask | I needed to make up a specific volume of a standard solution. The volumetric flask has a low error. | Top pan balance | I needed to accurately weigh out small amounts of solid when making up my solutions. | 25
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Concentration of Ammonia in Window Cleaner Solution Design (D) Aim To determine the concentration of ammonia‚ NH3‚ in the commercial window cleaner solution Background Window cleaner contains ammonia‚ NH3‚ a weak base‚ which helps remove dirt from glassware. The concentration of ammonia in the window cleaner solution varies by brands. Titrating the window cleaner solution with an acid of known concentration allows us to calculate the concentration of the ammonia in that brand of window cleaner solution
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Since the Grignard reagent can easily react with water‚ all glassware including the 25 ml round bottom flask‚ magnetic stir bar‚ 3 and 5 ml conical vial‚ 50 mL Erlenmeyer flask‚ claisen adapter‚ drying tube and 5 glass pasteur pipets were first added to a 250mL beaker and placed in the oven for 30 minutes. After the completion of the thirty minutes‚ 0.150 g of shiny magnesium turnings and a stir bar was first added to the round bottom flask and the claisen adapter along with the drying tube packed
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emptied and weight of granules was calculated by subtracting weight of each empty shell from each capsule weight. Average weight was determined and an accurately weighed quantity of granules equivalent to 10 mg of DAB was transferred into 10 ml volumetric flask and dissolved in 5 ml of DMSO and sonicated for 10 minutes. Then the volume is made up to mark with the DMSO and filtered through whatmen filter paper. Further the filtrate was diluted with DMSO to get final concentrations within linearity
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Period 1 11/7/13 Chapter 35 Discussion Background: Potassium permanaganate is widely used as an oxidizing agent in volumetric analysis. In acid solution‚ MnO4- ion undergoes reduction to Mn2+ this is the equation: 8H+(aq) + Mno4-(aq) + 5e- Mn2+(aq) + 4H2O Since the KMnO4 – ion is violet and the Mn2+ ion is nearly colorless‚ the end point titrations using KMnO4 as the titrant can be taken as the first pink color that appears in the solution (and stays without disappearing).
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