are immiscible and all are flammable. Tests for active unsaturation indicate that hexane‚ heptane‚ cyclohexane‚ benzene and toluene are saturated while cyclohexene is actively unsaturated. Hexane‚ heptane‚ benzene‚ and toluene are classified as aliphatic while cyclohexane‚ and cyclohexene are aromatic. All are not oxidized except for cyclohexene. I. Introduction Hydrocarbons are compounds that contain only carbon and hydrogen. Hydrocarbons can be aromatic or aliphatic
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Dehydrating Cyclohexanol • Introduction The purpose of the lab experiment is to prepare cyclohexene from cyclohexanol through an acid-catalyzed dehydration. In order to produce the cyclohexene from cyclohexanol‚ an elimination reaction was performed. First by protonating the oxygen of the alcohol and creating an oxonium ion we replaced the poor leaving group (OH) into a better leaving group (OH2+). Second‚ dehydrating the cyclohexanol using phosphoric acid and sulfuric acid as acid catalysts
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Yılgör Experiment date:06.12.2010 Report Date: 20.12.2010 ABSTRACT In this experiment‚ the purpose was to investigate E1 elimination mechanism with the reaction of cyclohexanol to cyclohexene. The reaction was acid catalyzed dehydration of alcohol and with catalyst sulfuric acid cyclohexene was obtained from cyclohexanol. And the product was obtained from the simple distillation and later it was reacted with bromine and potassium permanganate. The observations and results were all recorded
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Dehydration of Alcohols Abstract The dehydration of cyclohexanol to cyclohexene can be done through fractional distillation. Once the fraction has been collected it must then be dried. The dried distillate is finally tested to determine whether or not it has been dehydrated. The three tests used were infrared spectroscopy‚ Bromine chemical test and Bayer’s chemical test. The infrared spectroscopy showed a large narrow peak at 3062.12(cm-1) and 3020.71(cm-1) which indicates that there is a double
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Mario Troncoso 20025019 Dehydrating Cyclohexanol Structure/MSDS: Anhydrous calcium chloride—irritant and hygroscopic (calcium chloride) cyclohexanol—irritant and hygroscopic (cyclohexanol) cyclohexene—flammable and irritant (cyclohexene) Sulfuric acid—toxic and oxidizer (Sulfuric acid) phosphoric acid—corrosive (phosphoric acid) Results/Data: End product weighed 0.109g of cyclohexane and tested positive with bromine test Discussion: In order to perform
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NORTHERN CARIBBEAN UNIVERSITY DEPARTMENT OF BIOLOGY‚ CHEMISTRY and ENVIRONMENTAL SCIENCE LABORATORY MANUAL Instructor: Dr. M. Wilson CHEM401: BIOCHEMISTRY for NURSES Prepared by: Oreane Collins CHEMISTRY LABORATORY REGULATIONS AND SAFETY PRECAUTIONS Reference: http://www.sciencebyjones.com/safety_rules.htm Thanks to the Flinn Scientific Safety Rules for much of the below. General Guidelines 1. Conduct yourself in a responsible manner at all times
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Synthesis of Cyclohexanol Author: Ahmed Ayyash 06/06/13 Introduction: In this experiment‚ cyclohexanol was prepared from an initial cyclohexene. However‚ this occurred over a number of steps‚ these are out lined below. 1. Cyclohexene + aqueous acid cyclohexyl cation 2. cyclohexyl cation + hydrogen sulphate + water protonated cyclohexanol + cyclohexyl hydrogen sulphate 3. cyclohexyl hydrogen sulphate protonated cyclohexanol + HSO4 4. protonated cyclohexanol + HSO4
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Formation of an Alkene by Alcohol Dehydration Lab Report Balanced Chemical Equation for the Main Reaction Mechanism The acid-catalyzed dehydration of secondary and tertiary alcohols involves non-isolable carbocation intermediaries. In the first step of the of the reaction mechanism below‚ a phosphoric acid catalyst adds a proton to the oxygen atom of the alcohol to form an oxonium ion. The OH is converted to a better leaving group as the positive charge on the oxygen weakens the carbon-oxygen
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carbon-carbon double bonds are positioned next to one another‚ a conjugated diene is formed. Conjugated dienes undergo a cycloaddition reaction with certain double bonds to afford cyclohexenes and related compounds. The reaction is named Diels-Alder. The Diels-Alder reaction is between 1‚3-butadiene and ethylene to produce cyclohexene + dienedienophile. The mechanism of the Diels-Alder reaction is classified as a [4+2] cycloaddition reaction‚ because one reactant (the diene)‚ contributes four carbon atoms
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Arranged a fractional distillation apparatus used a 100mL round-bottomed flask for the solution and used a 50mL round- bottomed flask cooled in ice an ice bath as the receiver of the reaction. The 65% sulfuric solution was prepared in a clean 125mL Erlenmeyer flask it contained 20.0 mL of deionized water and 20mL of concentrated sulfuric acid was added carefully with some swirling in between. The diluted acid was cooled with an ice water bath to 20-25ºC. to the cooled sulfuric acid cyclohexanol was
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