"Esterification octyl acetate" Essays and Research Papers

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    EXERCISE 11 Synthesis of Aspirin (Acetylsalicylic Acid from Salicylic Acid) RAQUID‚ Rency J Group 5 18L I. Introduction Due to the demand of certain reagents in the laboratory in order to perform and conduct further experiments or produce essential compounds‚ chemists continuously develop organic synthesis. This process aims to prepare and synthesize desired organic compounds from commercially or readily available ones by providing the simplest route in synthesizing the compound

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    Synthesis of Aspirin

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    Sypnopsis In this experiment‚ acetylsalicylic acid was synthesized from the acidification of salicylic acid and acetic anhydride. The objective was to convert a specific amount of salicylic acid into the same amount of aspirin that was high in purity. Furthermore‚ the other objectives were to enable students to conduct the synthesis of aspirin‚ reinforce skills or recrystallisation and the technique of melting point determination. The amount of each compound should be the same because there is

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    the crystals form they are then filtered and left to dry out. There mass is measured and recorded then the yield is calculated. Introduction: Purpose: The aim of this experiment is to synthesize the common pain killer aspirin through an esterification reaction between Salicylic Acid and Acetic Anhydride; using sulfuric acid as a catalyst (4). Background: Aspirin is one of the

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    Paper

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    obtained in paste tank is fed to esterification reactor by screw pump. The esterification reaction is carried out under pressure and at high temperature of 265 deg C . Mole ratio of 1:1.19 is maintain in the reactor. Theoretical mole ratio requirement is 1: 1.01 Monomer is the product of esterification reaction. Water is evolved in the esterification process as byproduct The water is distilled off by distillation column and send to ETP for further treatment Esterification reaction dose not required

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    Chemistry notes

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    9.3 – The Acidic Environment: Δ. Construct word and balanced formulae equations of all chemical reactions as they are encountered in this module: NOTE: In chemistry‚ [x] means “concentration of x” in moles per litre (mol/L). EG: [H3O+] means “concentration of H3O+ ions” in mol/L. BASIC reactions to remember: Acid reactions: acid + base salt + water acid + metal salt + hydrogen gas acid + carbonate carbon dioxide gas + salt + water Formation of hydronium: H+ + H2O H3O+ Reactions of

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    functional groups present in the compound. n-heptane‚ pentene‚ benzene‚ heptanol‚ sec-butanol‚ phenol‚ acetyl chloride‚ buteraldehyde‚ benzaldehyde‚ 2-butanone‚ propanoic acid‚ sucrose‚ diethyl ether‚ butyl bromide‚ acetonitrile‚ L-alanine‚ n-amyl acetate‚ benzene sulfonyl chloride and aniline were used as test compounds. Observations were noted‚ such as changes in color and product formation. Iodine test‚ bromine test‚ Baeyer Test‚ Chloroform and aluminum chloride‚ fuming sulfuric acid‚ acetyl

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    Labreport

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    Background: Benzocaine | | C9H11NO2  | Reaction scheme for Fischer Esterification of p-aminobenzoic acid: Synthesis of Benzocaine.3 In 1890‚ a chemist named Ritsert‚ was the first to synthesis benzocaine and introduced it in the market in 1902. Benzocaine is a pain reliever and has many active over-the-counter ingredients. It is also used as a lubricant and topical anesthetic on intratracheal catheters and pharyngeal and nasal airways to obtund the pharynegeal and tracheal reflexesl.2 Sodium

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    INDUSTRIAL ATTACHMENT REPORT

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    CHAPTER ONE 1.0 INTRODUCTION This report is a practical experience acquired by me in the course of my industrial training at Druckfarben Nigeria Limited (DFN) under the student industrial work experience scheme (SWIES). In the earlier stage of science and technology education in Nigeria‚ students were from their respective institutions without any technical knowledge or working experience. It was in this view that students undergoing science and technology related courses were mandated in different

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    Benzocaine Ir Analysis

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    Benzocaine is the ethyl ester of paraaminobenzoic acid and as an ester it can be classified by Fischer esterification. Fischer esterification reactions typically include a carboxylic acid and alcohol as well as a dehydrating agent . Since esterification reactions are slow‚ a catalyst is required. The addition of the catalyst maximizes the yield of product (benzocaine) from the esterification since the reaction is reversible which means it tends to result in a low yield of product. For the synthesis

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    Experiment # 45: Benzocaine Abstract The local anesthetic‚ benzocaine‚ was synthesized via the esterification of p-aminobenzoic acid with ethanol. The percent yield of crude product was determined to be 21% and the melting point was recorded at 86.2°C ± 0.2°C‚ with a 6.3% error from 92°C‚ the literature melting point of pure benzocaine. The crude product was then recrystallized to improve the purity of benzocaine and 57.4% was recovered. The new melting point range was measured at 89.1°C ±

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