anhydride. CO2H OH salicylic acid 2g 0.014 mole O O O CH3 H2SO4 ethyl acetate CO2H O O acetyl salicylic acid acetic acid CH3 O + H3C + H3C OH acetic anhydride 5 mL 0.05 mole The limiting reagent is salicylic acid. The theoretical yield of acetyl salicylic acid is 2.52 g. Physical Data:* mp MW salicylic acid 157-9˚ 138 acetyl salicylic acid 135-6˚ 180 acetic anhydride — 102 acetic acid — 60 sulfuric acid — 98 ethyl acetate — 88 *Data from the CRC‚ 70th ed. bp — — 138˚ 117-8˚
Premium Acetic acid Aspirin
* Benzaldehyde * Acetone * Sodium Nitroprusside Test – Test for presence of acetone * -Wine red solution * Iodoform Test – Test for Methyl Ketones * Acetone – positive * Ethyl methyl ketone – positive * Ethyl acetate * Special test for Benzaldehyde * Formation of crystals * Molisch Test – General test for Carbohydrates * Violet ring (2nd layer) * Glucose – positive * Starch - positive
Premium Carboxylic acid Oxygen Alcohol
e dominant position in world menthol production. 90% crop of India‚ grown in Uttar Pradesh‚ rest 10% in Punjab‚ Haryana and Rajasthan. Recently‚ Mentha Herb was developed in Madhya Pradesh & Gujarat but in little quantity Uses and Application Menthol mint essential oil is the main source of natural menthol. The dementholised oil (DMO) is reconstituted to produce oil similar to Mentha piperita oil. Many dozens of terpenes present in the essential oil are valuable compounds that find uses in
Premium Menthol
1. Introduction Plumbago zeylanica L. belonging to the family Plumbaginaceae is an important plant of medicinal value. In the Arabian Peninsula‚ it is mainly distributed over Oman‚ Yemen and the Southwestern region of Saudi Arabia. The use of the roots of P. zeylanica for treating skin problems has been recorded by early Muslim physicians. P. zeylanica is greatly valued in Ayurveda for treatment of cough‚ asthma and gastrointestinal disorders. In Sushrutha Samhitha it has been described as antiseptic
Premium Uric acid Uric acid Antioxidant
Abstract: In this lab‚ the chemical components of Excedrin and Tylenol‚ two common‚ over-the-counter analgesic drugs‚ were determined by utilizing the technique of thin-layer chromatography‚ or TLC. The active ingredients of Excedrin were caffeine‚ acetaminophen‚ and aspirin with Rf values of 0.11‚ 0.38‚ and 0.61‚ respectively. The lone active ingredient of Tylenol was acetaminophen with an Rf value of 0.39. The elution sequence obtained in the experiment is as follows: ibuprofen (least polar)
Premium
about 10 minutes. Next‚ 4- bromophenylacetic acid was added to the flask and the mixture was refluxed for about 50 minutes at about 80°C. TLC was used to monitor the reaction progress every 15 minutes. A relatively non-polar solvent system of 25% ethyl acetate/ 75% hexanes was used as the mobile phase. Each plate contained a starting material (4-bromophenylacetic acid)‚ a reaction mixture spot‚ and a co-spot. The TLC at 15 minutes showed the starting material to have an Rf of about 0.12 and reaction
Premium Oxygen Carbon Carbon dioxide
reaction. If the bromine reacted with the alkene the bromine would discolor from orange and turn clear. Experiment Part A) Solubility of Alkanes: 1 mL of nine solvents (water‚ methanol‚ n-butanol‚ ethylene‚ glycol‚ acetone‚ hexane‚ toluene‚ ethyl acetate‚ and dichloromethane.) was added to nine sample vials. Each vial then had 0.5 mL of the alkane decalin added to each one. The mixtures were stirred to determine if the materials dissolved. If the material was insoluble it was heated with an
Premium Solvent Solubility
ISOLATION OF TRIMYRISTIN FROM NUTMEG ABSTRACT The purpose if the experiment was to extract the Trimyristan from ground nutmeg using extraction‚ distillation and recrystallization procedures. This experiment involves extraction and separation techniques that yield a purified product. The product was extracted and a distillation process was used to remove any remaining solvent. The recrystallization of the sample in turn produced a pure sample‚ which was proven using the known melting
Premium Distillation Solvent Temperature
steam distillation using a microscale distillation apparatus and isolate a natural product from cloves. Introduction By performing steam distillation we can isolate eugenol at lower temperature than its usual boiling point of 248 degree Celsius. Eugenol belongs to a category called essential oil. Many of these compounds are used as flavoring and perfumes and in the past were considered the essence of plant from which they were derived. Structure of eugenol (clove oil) and eugenol acetate:
Premium Distillation Essential oil Solvent
Introduction Esters are in a lot of natural products like flowers‚ spices and fruits. They are usually used in artificial flavorings. Carboxylic esters help amplify the sensory effect of esters. Isopentyl acetate is made from the direct esterification of acetic acid and isopentyl alcohol. The direct esterification of acetic acid and isopentyl alcohol is an equilibrium reaction that shifts the product to the side by using the excess of one of the starting reagents. Acetic acid usually used in excess
Premium Chemistry Solvent Acetic acid