Oxidation of an Alcohol: Oxidizing Methoxybenzyl Alcohol to Methoxybenzaldehyde Using Phase-Transfer Catalysis PURPOSE OF THE EXPERIMENT Oxidize methoxybenzyl alcohol to methoxybenzaldehyde‚ using sodium hypochlorite as the oxidizing agent and tetrabutylammonium hydrogen sulfate as the phase-transfer catalyst. Monitor the progress of the reaction by thin-layer chromatography. BACKGROUND REQUIRED You should be familiar with extraction‚ evaporation‚ and thin-layer chromatography techniques
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Name: __________________________________ Teacher: ________________________________ DO NOT OPEN THE EXAMINATION PAPER UNTIL YOU ARE TOLD BY THE SUPERVISOR TO BEGIN Chemistry 2202 FINAL EXAMINATION June 2010 Value: 100% General Instructions This examination consists of two parts. Both parts are contained in this booklet and further general instructions are provided on appropriate pages. Part I – Multiple Choice (40%) Select the letter of the correct response from those provided. EITHER
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neutral pink Co Solution and the blue CoCl4‚ HCl solution. During the flame test‚ there was no change‚ which ruled out Ba‚ Ca‚ Cu‚ K and Na. From all of these observations‚ there was no doubt that my cation was Co (II). To figure out my anion‚ the AgNO3 test proved to be very helpful. At first‚ it looked as if there was no precipitate formed but when you look closer you can see that there actually is some precipitate at the bottom. This showed that the solution was white and sparingly soluble. Looking
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Name: Allison Bynum Date:6/17/14 Exp 8: Ionic Reactions Lab Section: 75426 Data Table: Record your observations in the following table Na3PO4 NaI Na2SO4 NaCl NaHCO3 Na2CO3 NaOH Co(NO3)2 Created a musty looking cloud that later turned dye to a purple shade No change‚ brought out pink very slightly No change No change Created a cream looking liquid‚ did not mix with pink substance Darkened color‚ changing to more of a purple tint as time passes on. Immediately turned
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1. Add a small piece of zinc into a test tube 2. Add about 5 mL of CuSO4 to the same test tube 3. Observe the reaction for 2-3 minutes 4. Record Observation 5. Clean workstation * Workstation 7: 1. Combine 5-8 drops of AgNO3 and CaCl2 in a test tube 2. Observe reaction for 2-3 minutes 3. Record Observations 4. Clean Workstation * Workstation 8: 1. Combine 4-5 drops of CaCl2 and NaPO4 in a test tube 2. Observe reaction for 1 minute 3. Record
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Lab Report Layout and Template The lab report will be 4-8 pages‚ typed‚ double spaced‚ in 12 pt Times New Roman font. The sections within the lab report should be as follows (and numbered accordingly): Title Page 1.0 Introduction 2.0 Synthesis of a Cobalt Complex 3.0 Percent Halide Analysis of Cobalt Complex 4.0 Preparation and Standardization of a 0.3 M Hydrochloric Acid solution 5.0 Percent Ammonia Analysis of Cobalt Complex 6.0 Preparation and Standardization of a 0.1 M Sodium Thiosulfate
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SYNTHESIS AND CHEMISTRY OF K2S2O8 ABSTRACT In this experiment‚ a sample of K2S2O8 was prepared by the electrolysis of an aqueous solution of H2SO4 and K2SO4. The peroxodisulfate anion‚ S2O82-‚ was also observed for its ability to serve as a counterion for precipitation by preparing a copper (II) complex by reacting hydrated copper (II) sulfate with ammonium peroxodisulfate in the presence of pyridine. This same ability‚ coupled with its strong oxidizing ability allowed for stabilization of
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Reactivity of Halide Ions PURPOSE The purpose of this experiment is to observe the reactions of halide ions with different reagents by mixing them together. Materials 0.1 M AgNO3 0.1 M NaCl 0.1 M NaF 0.2 M KBr 0.2 M Na2S2O3 3% Starch Solution 4.0 M NH3 (aq) 5% NaClO (commercial bleach) 24 – well microplate thin – stemmed pipettes‚ 12 Safety DATA |PARTS |INITIAL MASS |FINAL MASS |CHANGE IN MASS | |
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AS TRANSITION COURSE SUMMER 2012 PART 1: MEASURING AMOUNT OF SUBSTANCE MASS VOLUME MOLAR MASS AVOGADRO [pic] CONCENTRATION ATOM ION MOLECULE COURSE OUTLINE OCR Chemistry A Unit 1 – Autumn Term 2012 • Atoms and Electron Structure • Moles‚ Equations and Acids • Structure and Bonding • Redox‚ Group 2 and Group 7 Unit 1 Exam – January 2013 – 1 hour – 90 UMS – 30% of total Unit 2 – Spring Term 2013 • Basic Concepts
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displaces another less active element in a compound (i.e. Zn (s) + CuSO4 (aq) ZnSO4 (aq) + Cu (s)). Double displacement are similar to single displacement reactions however two elements are displaced instead (they switch compounds‚ observe: KCl (aq) + AgNO3 (aq) AgCl (s) + KNO3 (aq)). A neutralization reaction double displacement reaction that occurs between an acid and base when they are combined (i.e. H2SO4 (aq) + 2NaOH (aq) Na2SO4 (aq) + 2H2O (aq)). Combustion reactions are examples of spontaneous
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