In this experiment‚ the production of a Grignard reagent (phenylmagnesium bromide) was performed from a bromobenzene reactant combined with magnesium and ether. Phenylmagnesium bromide was then transformed into a tertiary alcohol called triphenylmethanol‚ through addition of another compound called benzophenone‚ as well as additional ether. The end product of triphenylmethanol was analyzed via NMR and IR. Figure 1: Preparation of the Grignard agent by combining bromobenzene with magnesium and ether
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LIMITING REAGENT Practice Problems 1. At high temperatures‚ sulfur combines with iron to form the brown-black iron (II) sulfide: Fe (s) + S (l) ( FeS (s) In one experiment‚ 7.62 g of Fe are allowed to react with 8.67 g of S. a. What is the limiting reagent‚ and what is the reactant in excess? b. Calculate the mass of FeS formed. 2. Arcylonitrile‚ C3H3N‚ is the starting material for the production of a kind of synthetic fiber acrylics) and can be made from
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Preparation of the NaOH Solution Mass of NaOH before standing = NaOH before standing (g) – beaker (g) = 111.490 g – 110.970 g = 0.520 g Mass of NaOH after standing = NaOH after standing (g) – beaker (g) = 111.500 g – 110.970 g = 0.530 g Standardization of the NaOH solution TRIAL I Volume of NaOH solution = Final reading of buret - Initial reading of buret = 13.80 mL – 0.00 mL = 13.80 mL Converting the Volume (mL) to Volume (L) Volume (liters) = Volume (mL) x
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Abstract: The main objective of this Lab‚ is to experiment with stoichiometric measurements‚ since it is one of the most important subjects in chemistry. In addition‚ stoichiometric measurement is widely used in chemistry‚ because it indicates the proportion of mass in which various substances react. By examining one specific example of stoichiometric determination‚ which is: “Stoichiometry and limiting reacting”‚ we found out the different mass proportions in which substance react. In this case
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Abstract: The purpose of this lab is to prepare phenylmagnesium bromide‚ a Grignard reagent‚ and react it with benzophenone to give triphenylmethanol. Once made‚ the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone‚ benzophenone. The result is an alkoxide that is then protonated to give the alcohol‚ triphenylmethanol. The purity of the final product will then be considered by melting point and IR spectroscopy. Final purified triphenylmethanol weighed 8.02 grams
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Chemistry 101 Lab 7 Determination of % NaHCO3 in Alka Seltzer Tablets Names ____________________________and ___________________________ Date ____________________________ Objectives: (1) To determine the amount of NaHCO3 in Alka Seltzer tablets by observing the amount of CO2 produced from the acid-base reaction of HCO3- with acetic acid (in vinegar). (2) To study the concept of limiting reactant. Background: Alka Seltzer is an effervescent tablet that contains aspirin
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Experiment #8: Limiting Reactant Abstract In chemical reactions‚ the significance of knowing the limiting reactant is high. In order to increase the percent yield of product‚ increasing the limiting reactant‚ possibly‚ is the most effective. In this experiment we were able to calculate limiting reactants from the reaction of CaCl2. 2H2O + K2C2O4.H2O(aq). As a group‚ we obtained our salt mixture of calcium chloride and potassium oxalate‚ and weighed the mixture. We were able to make an aqueous
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Drain cleaner is mostly made up of the strong base NaOH but also has other substances in it to efficiently clean a lodged pipe such as aluminum‚ sodium nitrate‚ and sodium chloride. All the homeowner ahs to do while using drain cleaner is to pour I down the clogged drain and maybe run some water‚ inside the pipe the chemicals go to work for you. But even though it sounds simple precaution must be taken in order to prevent injury to our body. NaOH must be produced correctly before it can be used
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Lab Report for the Limiting Factors of the Cedar Glade Mrs. Hall Introduction: In the wild‚ populations are normally controlled by limiting factors that are either biotic or abiotic. These prevent the population from continually growing and reaching their carrying capacity. This experiment will teach one what it is like to study real populations and to help one use and learn the meanings of certain words. Hypothesis: Investigation 1: If both the male and female owl hunt both 2 times a
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Formula: for NaoH N NaoH = grm KHP / ml NaoH x KHp /1000ml Formula: for HCL (NV) HCL = (NV) NaoH or N HCL V HCL = N NaOH V NaoH N HCL = VNAOH (NNaoH) / VHCL (for more info page 62-63 of the photocopy) KHP = Potassium hydrogen phthalate = KHC8H4O4 = Mw - 204.23 Trial 1: NNaoH = 1grm / 20.6 x 204.23 /1000 = 1grm / 4.21 = 0.24 normal NHCL = 20.6 (0.24) / 39.5 = 4.94 / 39.5 = 0.125 or 0.13 Trial 2: NNaoH = 1grm / 20.8 x 204.23 /1000
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