Introduction to Microscale Laboratory Niki Gharavi *‚ Minh Nguyen San Jose City College ABSTRACT: The objective of the experiment was to be introduced to working with the lab equipment‚ specifically heating and measuring‚ and to be able to create some of the apparatus that future experiments will require. Heating methods used were an aluminum block‚ a sand bath‚ and a water bath. The aluminum block heated most quickly while the others were more stable. Regarding the measurement of water‚ the less
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Jessica Robins Lab 3: Properties of Organic Compounds Introduction Distillation is a physical process used to separate chemicals from a mixture by how easy they vaporize. The temperature rises unit it reaches the temperature of the lowest boiling substance in the mixture while the other contents of the mixture remain in their original phase (until the most volatile substance has all boiled off) as it’s heated. Hot vapor results and passes into a condenser and is then converted to a liquid
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Exercise 1 Polymers – An introduction to Organic Chemistry Group 3 Jude Marchoni C. Tampus Meryl Marie Susan Chua Pearl Pontillas Paolo Pepito Gaia Casas I. Abstract: (Paolo) In this experiment we will be testing what would happen to the polymer when we add borax to it. A polymer is a compound made up of large molecules often in a solid state. Polymers are chemically formed by 100 to 10‚000 small molecules called "monomers". Monomers occur in molecular units or patterns
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Experiment 6 titled “Organic Chemistry” and the purpose of this lab is to get familiar with some organic functional group and test certain reactions of selected functional groups. To do the first part of the experiment (combustion test)‚ instructor demonstration in hood‚ and record the observation. Part A (combustion of toluene) pour 1 milliliter of toluene into a evaporating dish and ignite it with a flaming wood splint. Most importantly put the flame with a watchglass. Part B (combustion of ethyl
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Physical Properties of Organic Molecules Abstract Identifying the physical properties of compounds can be useful in several ways. It helps us to determine the structure of certain compounds‚ the purity of substances and if a substance is not pure we can figure out how to separate contaminating substances from a compound. In this experiment‚ I learned how to determine a solid’s melting point and why some melting point ranges may be broader than others.
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Microscale Crystallization of Sulfanilamide Purpose The purpose of the experiment was to use the crystallization technique to purify the solute sulfanilamide using 95% ethanol as the solvent‚ to calculate the amount of sulfanilamide that was recovered‚ and to determine the purity of the final product. Introduction In this experiment‚ recrystallization will be the method used to purify the solute sulfanilamide using ethanol as the solvent. Based on the solubility curve on the solubility
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Chem 2203 Sec 026 27/September/2013 Experiment 3B: Fractional Semi-microscale Distillation Separation of Hexane and Toluene. Objective: The main goal of this lab is to learn how separation of binary liquid mixtures is performed. Especially when the two liquids have boiling points varying by about 30° C. Hexane can be separated from toluene in this experiment because of the difference in their boiling points. Since toluene has a higher boiling point‚ it will left at the bottom while the hexane
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Microscale Crystallization – Craig Tube For this experiment‚ we had to find the percent recovery and melting point of pure sulfanilamide from impure sulfanilamide using the crystallization technique. To start‚ .1004 grams of impure sulfanilamide was put into a Craig tube with enough ethyl alcohol to barely pass the top of the sulfanilamide. The Craig tube was put into a stone block until boil‚ then check to see if the solid material had dissolve. With the addition of two more drops from a supply
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electronic instrument‚ the result that was achieved in this experiment was met due to the presence of esters in the graph in Figure 5; with a peak of 1297.89 at 1300-1100. There is also a match of 35.48 with ethyl salicylate. The objective‚ which is to create aspirin‚ has been completed due to the results shown by the data provided by an electronic instrument.A recommendation would be a more exact amount of reactants to be used. In this experiment‚ there was an excess of water and more acetic anhydride
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Organic Chemistry Laboratory – CH 200L (2012 – 2013) 2B-Ph Group 9 Experiment 10 Identifying Carboxylic Acids and Derivatives Through Classification Tests Bianca Therese Rivera‚ Camille Aliana Rivera‚ Zarah Mae Roxas‚ Ma. Rosario Teresa Saylo‚ Jean Darlene Semilla and Adrian Yu Department of Pharmacy‚ Faculty of Pharmacy University of Santo Tomas‚ Espana Street‚ Manila 1008 Date Submitted: September 13‚ 2012 ------------------------------------------------- Abstract Carboxylic acid derivatives
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